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1.
Abstract— Based on recent progress in simulating space weathering on asteroids using pulse‐laser irradiation onto olivine and orthopyroxene samples, detailed analyses of two of the A and R type asteroid reflectance spectra have been performed using reflectance spectra of laser‐treated samples. The visible‐near‐infrared spectrum of olivine is more altered than that of pyroxene at the same pulse‐laser energy, suggesting that olivine weathers more rapidly than orthopyroxene in space. The same trend can be detected from reflectance spectra of the asteroids, where the more olivine an asteroid has, the redder its 1 μm band continuum can become. Comparison of the 1 μm band continuum slope and the 2/1 μm band area ratio between the asteroids and olivine and pyroxene samples (including the laser‐treated ones) suggests that asteroids may be limited in the degree of space weathering they can exhibit, possibly due to the short life of their surface regolith. Their pyroxenes may also have a limited chemical composition range. Fitting the visible continuum shape and other parts of the spectra (especially the 2μm part) has been impossible with any combination of common rock‐forming minerals such as silicates and metallic irons. However, this study shows, for the first time, excellent fits of reflectance spectra of an A asteroid (Aeternitas) and an R asteroid (Dembowska), including their visible spectral curves, band depths and shapes, and overall continuum shapes. Our results provide estimates that Aeternitas consists of 2% fresh olivine, 93% space‐weathered olivine, 1% space‐weathered orthopyroxene, and 4% chromite, and that Dembowska consists of 1% fresh olivine, 55% space‐weathered olivine, and 44% space‐weathered orthopyroxene. These results suggest that space weathering effects maybe important to the interpretation of asteroid reflectance spectra, even those with deep silicate absorption bands. Modified Gaussian model deconvolutions of the laser‐irradiated olivine samples show that their identity as olivine remained. The most recent submicroscopic mineralogical analyses have revealed that the laser‐irradiated olivine samples contain nanophase iron particles similar to those in space‐weathered lunar samples.  相似文献   

2.
The surfaces of small bodies in the outer Solar System are rich in organic compounds and carbonaceous refractories mixed with ices and silicates. As made clear by dedicated laboratory experiments space weathering (e.g. energetic ion bombardment) can produce red colored materials starting from bright and spectrally flat ices. In a classical scenario, the space weathering processes “nurture” alter the small bodies surface spectra but are in competition with resurfacing agents that restore the original colors, and the result of these competing processes continuously modifying the surfaces is supposed to be responsible for the observed spectral variety of those small bodies. However an alternative point of view is that the different colors are due to “nature” i.e. to the different primordial composition of different objects. In this paper we present a model, based on laboratory results, that gives an original contribution to the “nature” vs. “nurture” debate by addressing the case of surfaces showing different fractions of rejuvenated vs. space weathered surface, and calculating the corresponding color variations. We will show how a combination of increasing dose coupled to different resurfacing can reproduce the whole range of observations of small outer Solar System bodies. Here we demonstrate, for the first time that objects having a fully weathered material turn back in the color–color diagrams. At the same time, object with the different ratio of pristine and weathered surface areas lay on specific lines in color–color diagrams, if exposed to the same amount of irradiation.  相似文献   

3.
R. Brunetto  F. Romano  S. Fonti  V. Orofino 《Icarus》2006,180(2):546-554
Laser irradiation experiments have been performed on powdered silicates (othopyroxene, clinopyroxene, and olivine) using a nanosecond pulse UV excimer laser (193 and 248 nm) to simulate the effects of space weathering induced on minor bodies of the Solar System by micrometeorite bombardment. We have used different fluences (from 0.05 to 2 J/cm2) to weather the samples, experimenting below and above the ablation threshold. All the irradiated materials have shown reddening and darkening of their UV-vis-NIR reflectance spectra. In addition we have found that: (1) below ablation threshold, weathering effects increase with increasing number of laser pulses, and with increasing fluence, confirming that a thermal process is active; (2) above ablation threshold, weathering is much stronger and efficient than in the previous case, and is independent on the number of pulses. We show that astrophysical time-scales, i.e. times necessary to obtain similar effects on planetary objects, are of about 108 yr for both olivine and pyroxene in the case of ablation. The time grows up to 1010 yr in the case of thermal effects. We infer that micrometeorite bombardment can be rightly simulated by laser irradiation only considering congruent laser ablation.  相似文献   

4.
Ion irradiation experiments have been performed on silicates (bulk samples) rich of olivine, pyroxene, and serpentine to simulate the effects of space weathering induced on asteroids by solar wind ions. We have used different ions (H+, He+, Ar+, Ar2+) having different energies (from 60 to 400 keV) to weather the samples, probed by Raman spectroscopy and UV-vis-NIR reflectance spectroscopy. All the irradiated materials have shown reddening and darkening of reflectance spectra in the 0.25-2.7 μm spectral range. We have found that the increase of the spectral slope of the continuum across the 1-μm band is strongly related with the number of displacements caused by colliding ions because of elastic collisions with the target nuclei. The spectral slopes have been compared, at increasing ion fluence, with those from irradiated Epinal meteorite. We show that formation of nuclear displacements by solar wind ion irradiation is a physical mechanism that reddens the asteroidal surfaces on a time-scale lower than 106 years.  相似文献   

5.
We performed ion irradiation of mineral samples with 50 keV He+, aimed to investigate ion irradiation effects on diagnostic spectral features. Reflectance spectra of samples in 0.375–2.5 μm are measured before and after ion irradiation. Silicates, including Luobusha olivine, plagioclase and basaltic glass, have shown reddening and darkening of reflectance spectra at the VIS–NIR range. Olivine is more sensitive to ion irradiation than plagioclase and basaltic glass. Irradiated Panzhihua ilmenite exhibits higher reflectance and stronger absorption features, which is totally different from lunar soil and analog silicate materials in other experiments. Using continuum removal and MGM fit, we extracted and compared absorption features of olivine spectra before and after irradiation. Ion irradiation can induce band strength decrease of olivine but negligible band centers shift. We estimate band centers shift caused by ion irradiation are quite limited, even less than variations due to chemical composition in silicates. It provides one possible explanation for no systematic shift in band positions in lunar soil. Irradiated Luobusha olivine spectrum matches spectra of olivine-dominated asteroids. Our results suggest space weathering should be new clues to explain the subtle difference between A-type asteroid spectra and laboratory spectra of olivine.  相似文献   

6.
Space weathering is an important surface process that occurs on the Moon and other airless bodies, especially those that have no magnetic field. The optical effects of the Moon's space weathering have largely been investigated in the laboratory for lunar samples and lunar analogues. However, duplication of pristine regolith on Earth is not possible. Here we report on space weathering from the unique perspective of the "Yutu" rover, which was part of the Chang'e-3(CE-3) mission, building on our previous work.Measurement of the visually undisturbed uppermost regolith as well as locations that have been affected by rocket exhaust from the spacecraft by the Visible-Near Infrared Spectrometer(VNIS) revealed that the returned samples provide biased information about the pristine lunar regolith. The uppermost surficial regolith is much more weathered than the regolith immediately below, and the finest fraction is rich in space weathered products. These materials are very dark and attenuated throughout the visible and near-infrared(VNIR) wavelengths, hence reducing the reflectance and masking the absorption features. The effects on the spectral slope caused by space weathering are wavelength-dependent: the visible and near-infrared continuum slope(VNCS) increases while the visible slope(VS) decreases. In the visible wavelengths, the optical effects of space weathering and Ti O_2 are identical: both reduce albedo and blue the spectra. This suggests that a new Ti O_2 abundance algorithm is needed. Optical maturity indices are related to composition and hence only locally meaningful. Since optical remote sensing can only sense the uppermost few microns of regolith and since this surface tends to be very weathered, the interpretation of surface composition using optical remote sensing data needs to be carefully evaluated. Sampling the uppermost surface is suggested.  相似文献   

7.
The absorption features of olivine in visible and near-infrared(VNIR) reflectance spectra are the key spectral parameters in its mineralogical studies. Generally, these spectral parameters can be obtained by exploiting the Modified Gaussian Model(MGM) with a proper continuum removal. However, different continua may change the deconvolution results of these parameters. This paper investigates the diagnostic spectral features of olivine with diverse chemical compositions. Four different continuum removal methods with MGM for getting the deconvolution results are presented and the regression equations for predicting the Mg-number(Fo#) are introduced. The results show that different continua superimposed on the mineral absorption features will make the absorption center shift, as well as the obvious alterations in shape,width and strength of the absorption band. Additionally, it is also found that the logarithm of a second-order polynomial continuum can match the overall shape of the spectrum in logarithmic space, and the improved regression equations applied to estimate the chemical composition of olivine-dominated spectra also have a better performance. As an application example, the improved approach is applied to pulse laser irradiated olivine grains to simulate and study the space weathering effects on olivine diagnostic spectral features.The experiments confirm that space weathering can make the absorption band center shift toward longer wavelength. Therefore, the Fo# estimated from remote sensing spectra may be less than its actual chemical composition. These results may provide valuable information for revealing the difference between the spectra of olivine grains and olivine-dominated asteroids.  相似文献   

8.
Abstract— We present combined multi‐spectral imager (MSI) (0.95 μm) and near‐infrared spectrometer (NIS) (0.8–2.4 μm) observations of Psyche crater on S‐type asteroid 433 Eros obtained by the Near‐Earth Asteroid Rendezvous (NEAR)—Shoemaker spacecraft. At 5.3 km in diameter, Psyche is one of the largest craters on Eros which exhibit distinctive brightness patterns consistent with downslope motion of dark regolith material overlying a substrate of brighter material. At spatial scales of 620 m/ spectrum, Psyche crater wall materials exhibit albedo contrasts of 32–40% at 0.946 μm. Associated spectral variations occur at a much lower level of 4–8% (±2–4%). We report results of scattering model and lunar analogy investigations into several possible causes for these albedo and spectral trends: grain size differences, olivine, pyroxene, and troilite variations, and optical surface maturation. We find that the albedo contrasts in Psyche crater are not consistent with a cause due solely to variations in grain size, olivine, pyroxene or lunar‐like optical maturation. A grain size change sufficient to explain the observed albedo contrasts would result in strong color variations that are not observed. Olivine and pyroxene variations would produce strong band‐correlated variations that are not observed. A simple lunar‐like optical maturation effect would produce strong reddening that is not observed. The contrasts and associated spectral variation trends are most consistent with a combination of enhanced troilite (a dark spectrally neutral component simulating optical effects of shock) and lunar‐like optical maturation. These results suggest that space weathering processes may affect the spectral properties of Eros materials, causing surface exposures to differ optically from subsurface bedrock. However, there are significant spectral differences between Eros' proposed analog meteorites (ordinary chondrites and/or primitive achondrites), and Eros' freshest exposures of subsurface bright materials. After accounting for all differences in the measurement units of our reflectance comparisons, we have found that the bright materials on Eros have reflectance values at 0.946 μm consistent with meteorites, but spectral continua that are much redder than meteorites from 1.5 to 2.4 μm. Most importantly, we calculate that average Eros surface materials are 30–40% darker than meteorites.  相似文献   

9.
Hayabusa‐returned samples offer a unique perspective for understanding the link between asteroids and cosmomaterials available in the laboratory, and provide insights on the early stages of surface space weathering. This study characterizes the mineralogy and the extent of space weathering of the three Itokawa particles RA‐QD02‐0163, RA‐QD02‐0174, and RA‐QD02‐0213 provided by JAXA to our consortium. We report here a series of results based on nondestructive analyses through visible‐near‐infrared reflectance and Raman spectroscopy. Results were obtained on the raw particles, both in their original containers and deposited on diamond windows. Identification of the minerals, characterization of their elemental compositions, and measurements of their relative abundances were led through Raman spectroscopy in punctual and automatic mode. Reflectance spectra in the visible and near‐IR wavelengths constrain the mineralogy of the grains and allow direct comparison with the surface of Itokawa. The spectra reflect the extent of space weathering experienced by the three particles. Particle RA‐QD02‐0163 consists of a heterogeneous mixture of minerals: olivine (Fo76) dominates an assemblage with both Ca‐rich (En50, Wo50) and Ca‐poor (En85) pyroxenes. The elemental compositions of the silicates are consistent with those previously reported for distinct Hayabusa particles. Particles RA‐QD‐0174 and RA‐QD02‐0213 are solely composed of olivine, whose chemical composition is similar to that observed in RA‐QD02‐0163. It has been previously shown that the S‐type asteroid 25143 Itokawa is a breccia of poorly equilibrated LL4 and highly equilibrated LL5 and LL6 materials. The three particles studied here can be related to the least metamorphosed lithology (LL4) based on the high forsterite content of the olivine. Neither carbonaceous matter nor hydrated minerals were detected through Raman on the three allocated particles. The NIR‐VIS reflectance (incidence = 45°, light collection at e = 0°) spectra of the three particles, in particular the 1 μm band, are consistent with the presence of both olivine and pyroxene detected via Raman. The spectra of particles RA‐QD02‐0163 and RA‐QD02‐0213 are also fully compatible with the ground‐based observations of asteroid (25143) Itokawa in terms of both spectral features and slope. By contrast, particle RA‐QD02‐0174 has a similar 1 μm band depth but higher (redder) spectral slope than the surface of Itokawa. This probably reveals a variable extent of space weathering among the regolith particles. RA‐QD02‐0174 may contain a higher amount of nanophase metallic iron and nanophase FeS. Such phases are products by space weathering induced by solar wind, previously detected on other Itokawa particles.  相似文献   

10.
This project examines the different approaches which deal with the theory of radiative transfer on atmosphereless bodies. We present the relative merits of two scattering theories based on the equivalent slab model: the extensively used Hapke theory (Hapke 1981, J. Geophys. Res.86, 3039-3054) and the Shkuratov theory (Shkuratov et al. 1999, Icarus141, 132-155). We found that their main difference is the role of the phase function of individual particles of regolith, which is predicted (and generally forward directed) in the case of the Shkuratov model instead of being a free parameter as formulated in the Hapke model. We also emphasize that different assumptions as to the manner in which different constituents are physically mixed in either model have a substantial effect on the synthetic spectra inferred. This leads to a significant extension of the validity of Hapke's or similar practical approaches to areas where these approaches are valid.We used two objects (the Centaurs 5145 Pholus and 8405 Asbolus) as examples. Previous modeling of the spectra of these two bodies with the Hapke approach gave suspect results in terms of the derived grain sizes, which were smaller than the wavelength, violating key assumptions of the model (Cruikshank et al. 1998, Icarus135, 389-407 for Pholus; Barucci et al. 2000, Astron. Astrophys.357, L53-56 for Asbolus). We considered several different types of powdered surfaces to interpret the surface composition of these two Centaurs. The effect of fine-scale contamination of water ice grains by small amounts of carbon and/or tholins is also explored. We can explain the strong red color and the rich near-infrared spectral signatures of Pholus using a five-component surface (contaminated water ice, amorphous carbon, Titan tholin, olivine, and methanol ice) where the grain sizes are consistent with the model assumptions. These components are similar to those inferred by Cruikshank et al. (1998), but we obtain very different grain sizes and relative abundances. For example, we obtain a relative abundance of water ice on the surface of Pholus of about 40% instead of 6% found with the Hapke model. Organic and carbonaceous components change by similar amounts. In the case of Asbolus, a tholin and amorphous carbon areal mixture can reproduce the spectrum, with water remaining at 9% or less. Using the albedo published by Fernandez et al. (2002, Astron. J.123, 1050-1055) which is higher than most workers assume for Centaurs and Kuiper belt objects, a surface composition similar to that of Pholus is found. It appears that model-based uncertainties in relative compositions must be regarded with more attention.  相似文献   

11.
The surfaces of airless bodies, such as the Moon and asteroids, are subject to space weathering, which alters the mineralogy of the upper tens of nanometers of grain surfaces. Atom probe tomography (APT) has the appropriate 3‐D spatial resolution and analytical sensitivity to investigate such features at the nanometer scale. Here, we demonstrate that APT can be successfully used to characterize the composition and texture of space weathering products in ilmenite from Apollo 17 sample 71501 at near‐atomic resolution. Two of the studied nanotips sampled the top surface of the space‐weathered grain, while another nanotip sampled the ilmenite at about 50 nm below the surface. These nanotips contain small nanophase Fe particles (~3 to 10 nm diameter), with these particles becoming less frequent with depth. One of the nanotips contains a sequence of space weathering products, compositional zoning, and a void space (~15 nm in diameter) which we interpret as a vesicle generated by solar wind irradiation. No noble gases were detected in this vesicle, although there is evidence for 4He elsewhere in the nanotip. This lunar soil grain exhibits the same space weathering features that have been well documented in transmission electron microscope studies of lunar and Itokawa asteroidal regolith grains.  相似文献   

12.
Mineral mapping of the lunar surface is critical to understanding the Moon’s geological diversity and history, yet the global lunar abundance of minerals has not been mapped using hyperspectral data. The Interference Imaging Spectrometer (IIM) of Chang’E-1 mission obtained hyperspectral data of the global lunar surface within the wavelength of 480–960 nm in which major minerals can be discriminated by faint differences in 32 contiguous hyperspectral bands. The effect of space weathering produces multiple endmembers of lunar minerals by obscuring the pure spectra of minerals in different levels. In this study, the distributions of plagioclase, clinopyroxene and olivine on the global lunar surface were mapped with IIM hyperspectral data based on the modified Multiple Endmember Spectral Mixture Analysis (MESMA) method considering the space weathering effect. The distribution of lunar space weathering levels was retrieved as a byproduct of mineral mapping. The mineral mapping results were compared with recent mapping results. Although the wavelength of IIM is limited, it shows that our results are basically consistent with the recent research at both global and local scales. The distribution of space weathering levels is also consistent with the map of optical maturity parameter (OMAT) in most parts of the global lunar surface, especially in the highlands. This study demonstrates that the modified MESMA method is an effective approach to quantitative mapping of the lunar minerals and space weathering levels using hyperspectral data. In the future, more minerals can be mapped with higher accuracy if hyperspectral data with a wider spectral range are used based on the method proposed in this study.  相似文献   

13.
Abstract— We report the mineralogy and oxygen isotopic compositions of FeO‐rich silicates in the Sahara 97159 EH3 chondrite. This component is referred to as FeO‐rich because it contains substantially more FeO than the characteristic FeO‐poor silicates in the highly reduced enstatite meteorites. These FeO‐rich silicates are mostly low‐Ca pyroxene (Fs5–35) and their compositions suggest an origin under more oxidizing conditions, like those for the ordinary chondrites. However, the mafic silicates in ordinary and carbonaceous chondrites are dominantly olivine, and the FeO‐rich silicates in the E chondrites are less commonly olivine. The oxygen isotopic compositions of the FeO‐rich silicates are indistinguishable from those of FeO‐poor silicates in Sahara 97159. These observations suggest that both the FeO‐rich silicates and the FeO‐poor silicates in EH chondrites formed from the same oxygen reservoir where redox conditions varied widely.  相似文献   

14.
Since their formation in the outflows of evolved stars, materials suffer in space deep chemical and physical modifications. Most abundant elements (C, N, O, Mg, Si, S and Fe) are present in dust as refractory chemical species. Among them silicates are one of the main constituents. Spectroscopic observations in various astronomical environments have shown that magnesium rich silicates are present both in amorphous and in crystalline form. An accurate interpretation of these observations requires studies on the formation of silicate dust in the atmospheres of giant stars and their evolution in the interstellar medium until their inclusion in protoplanetary disks.Many theoretical works have described the chemical and physical evolution of solids in space and their link to observable optical properties. Laboratory studies of cosmic dust analogues are needed to investigate these processes experimentally.In this work, experiments aimed at simulating the formation of silicates in space are presented. In particular, the laser ablation technique is used to produce amorphous silicates with various Si-Mg-Fe content. The analysis of their thermal evolution is presented.  相似文献   

15.
We report an unexpected variability among mid-infrared spectra (IRTF and Spitzer data) of eight S-type asteroids for which all other remote sensing interpretations (e.g. VNIR spectroscopy, albedo) yield similar compositions. Compositional fitting making use of their mid-IR spectra only yields surprising alternative conclusions: (1) these objects are not “compositionally similar” as the inferred abundances of their main surface minerals (olivine and pyroxene) differ from one another by 35% and (2) carbonaceous chondrite and ordinary chondrite meteorites provide an equally good match to each asteroid spectrum.Following the laboratory work of Ramsey and Christensen (Ramsey, M.S., Christensen, P.R. [1998]. J. Geophys. Res. 103, 577-596), we interpret this variability to be physically caused by differences in surface particle size and/or the effect of space weathering processes. Our results suggest that the observed asteroids must be covered with very fine (<5 μm) dust that masks some major and most minor spectral features. We speculate that the compositional analysis may be improved with a spectral library containing a wide variety of well characterized spectra (e.g., olivine, orthopyroxene, feldspar, iron, etc.) obtained from very fine powders. In addition to the grain size effect, space weathering processes may contribute as well to the reduction of the spectral contrast. This can be directly tested via new laboratory irradiation experiments.  相似文献   

16.
The impact threat of some near-Earth Asteroids (NEAs) drives our need to understand their mineral compositions. Quantitative mineral abundances based on reflectance spectroscopy are of great significance for studying the compositions of NEAs. In this study, we constrained the surface mineralogy of (99942) Apophis based on multiple diagnostic spectral parameters. The influence of non-mineral component factors (e.g., space weathering, phase angle, and surface temperature) on diagnostic spectral parameters was evaluated. We established the connection between Apophis and corresponding meteorite analog. Our results show that the abundances of olivine and pyroxene on the surface of Apophis are 53.4 ± 6 wt% and 35.6 ± 2 wt%, respectively. The 1 μm band width is basically unaffected by phase-angle changes and is less affected by temperature variations. Low temperature has more obvious effects on the 1.25/1 μm band depth ratio (BDR 1.25) based on the present data. When the phase angle ranges from 60° to 120°, the BDR 1.25 changes significantly with the increase or decrease of phase angle. In terms of spectral characteristics, the best meteorite analog of Apophis is LL chondrite, confirming earlier interpretations. Mineral analyses based on multiple diagnostic spectral parameters provide more consistent results. Knowledge of the surface compositions of Apophis can also inform optimum or possible defense strategies for it and other NEAs.  相似文献   

17.
Following the work of Rivkin et al. (Rivkin, A.S., Thomas, C.A., Trilling, D.E., Enga, M., Grier, J.A. [2011]. Icarus 211, 1294–1297) and Thomas et al. (Thomas, C.A., Rivkin, A.S, Trilling, D.E., Enga, M., Grier, J.A. [2011a]. Icarus 212, 158–166), we investigate space weathering trends in the Koronis family using the larger sample size of the Sloan Digital Sky Survey Moving Object Catalog. We confirm the trend in spectral slope seen in our earlier work and extend our results by investigating the trend in band depth (i ? z color index) to show that Koronis family asteroids smaller than 4 km show the transition from fresh Q-type to weathered S-type surfaces.  相似文献   

18.
M.J. Loeffler  R.A. Baragiola 《Icarus》2008,196(1):285-292
We present quantitative laboratory studies that simulate the effect of redeposition of impact-ejecta on mineral surfaces. We produced deposits of natural olivine (Fo90) and forsterite on olivine and forsterite powder samples by ns-pulsed laser ablation. The deposits produce changes in the optical reflectance (0.66-2.5 μm). We show that significant darkening and reddening of the surface occurs when the deposit is olivine but not if it is forsterite. This is attributed to the formation of metallic iron nanoparticles in the olivine deposits. We also characterized structural and chemical changes using scanning electron microscopy, transmission electron microscopy, and X-ray photoelectron spectroscopy (XPS). In situ XPS measurements show that the olivine deposits are reduced, with 50% of the iron becoming metallic. Transmission electron microscope studies confirm the presence of 2-3 nm crystalline iron nanoparticles in the olivine deposits. The scanning electron microscope shows that both olivine and forsterite deposits smoothen the topography of the powder surface, which could have effects on processes such as exosphere-surface interactions and sputtering. We conclude that the effect of coatings produced by micrometeorite impacts will not be uniform on airless bodies but will depend on the composition of the terrain.  相似文献   

19.
Silicates are one of the principal components present in Solar System objects.Silicates evolve in space modifying their physical properties according to theastronomical environments they go through. To characterise the nature of TNOsin the framework of the formation and evolution of the Solar System, experimentson structural transitions of silicates have been performed in the laboratoryto simulate some of the processing suffered by the dust. The infrared spectralproperties of possible silicate candidates thought to be present in TNOs have beenstudied. The results of thermal annealing of amorphous silicates and amorphisationof crystalline forsterite (pure-Mg olivine) by ion irradiation are presented. Theobservable properties of TNOs surfaces are inferred.  相似文献   

20.
Space weathering is now commonly accepted to modify the optical and magnetic properties of airless body regoliths throughout the Solar System. Although the precise formation processes are not well understood, the presence of ubiquitous sub-microscopic metallic iron (SMFe) grains in lunar soils and corresponding spectral analyses have explained both the unique optical and magnetic properties of such soils. More recently, a variety of ion irradiation, laser melting and vaporisation and impact experiments have been shown to reproduce these effects in the laboratory. Such experiments are crucial to the study of the formation of SMFe under controlled conditions. To date, more emphasis has been placed on optical analyses of laboratory samples, as these address directly the mineralogical interpretation of remote sensing data. However, the magnetic analyses performed on the Apollo and Luna samples have provided useful qualitative and quantitative evaluation of regolith metallic iron content. These techniques are reviewed here, demonstrated on pulsed laser irradiated olivine powder, and their utility for determining the quantity and size distribution of this metallic iron discussed. Ferromagnetic resonance, multi-frequency magnetic susceptibility, vibrating sample magnetometry and thermomagnetic measurements were carried out. Each showed trends expected for the conversion of paramagnetic Fe2+ in olivine to fine-grained Fe0, with some grains in the superparamagnetic size range. Although evidence for superparamagnetic iron was found, the quantity of sub-microscopic metallic iron produced in these experiments proved insufficient to make conclusive measurements of either the quantity or size distribution of this iron. Improvements to both the experimental and analytical procedures are discussed to better enable such measurements in the future.  相似文献   

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