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1.
Usually, multiple-grain aliquots are used for electron spin resonance (ESR) dating of sediments. However, this approach excludes the ability of detecting insufficient bleaching, as would be the case when measuring several single aliquots or single grains. In this paper, we present preliminary results of single-grain ESR dating experiments on three different sedimentary deposits (fluvial, fluvio-aeolian and desert aeolian), ranging in age between 100 ka and 2 Ma. Titanium-related impurity centres (Ti–Li and Ti–H) were measured in a Q-band ESR spectrometer for estimating equivalent doses (De) of individual quartz grains (0.5–1 mm). Both additive and regenerative dose methods were used. The resulting De plots show a large scatter in De—from 100 Gy to more than 600 Gy—for the fluvial sample, probably reflecting different bleaching histories of the grains. On the contrary, a clear plateau can be observed in De for sands with a strong aeolian component. Preliminary single-grain ESR ages are in relatively good agreement with independent estimates, the best results being obtained for the desert aeolian sample (200 ka). It is concluded that ESR has a promising potential for estimating large naturally accumulated doses of well-bleached sediments. Nevertheless, the method is challenged by several experimental difficulties, such as long measurement times, excessive errors, and presumably a complex interrelationship between Ti–Li and Ti–H components.  相似文献   

2.
Modern and known-age Pleistocene fluvial sediments were investigated by optical dating of quartz to test the suitability of the approach for dating deposits from the deeply incised Middle Rhine Valley. Samples from modern flood sediments revealed skewed distributions indicating different residual levels of equivalent dose (De) within the different aliquots. Nevertheless, a substantial number of aliquots from the modern deposits reflect De values close to zero. For the Pleistocene samples, optical ages are in general consistent with age control given by the presence of the Laacher See Tephra and radiocarbon dating. However, some samples overestimate the known age by a few thousand years when using the arithmetic mean. This is apparently explained by including aliquots in the determination of mean De where the optical signal was incompletely bleached at deposition. The most difficult issue in this context is identifying a suitable approach that can distinguish between the variability of De due to partial bleaching and microdosimetry. However, even when considering these limitations it appears that optical dating will by a quite suitable method to date Pleistocene sediments from such a complex fluvial environment, especially when focusing on a precision scale beyond a few thousand years.  相似文献   

3.
Glacifluvial deposits along an ice-marginal zone in Småland, southern Sweden, have been dated using post-IR blue OSL. To test for incomplete bleaching, we adopted two strategies: analysis of modern analogues and small-aliquot dose distributions. Samples of modern fluvial sediments show no significant incomplete bleaching; they yield equivalent doses of only 0.5–2 Gy (0.25–4% of our glacifluvial sediment doses). Small-aliquot dose distributions do not provide any evidence for incomplete bleaching.

The sediments are believed to have been deposited during deglaciation and appear to fall into two age groups: 19–25 ka (mainly sandur sediments) and 33–73 ka (mainly deltaic sediments). Compared to the expected ages (13–15 ka), even the younger glacifluvial OSL ages appear up to 10 000 years (25 Gy) too old. The ages are nevertheless stratigraphically consistent and correspond between sites; we deduce that the 19–25 ka ages are true deposition ages. For glacifluvial sedimentation to take place on the South Swedish Upland at this time either a very early deglaciation is required, or alternatively ice-free conditions just prior to the LGM. The deltaic sediments (33–73 ka) were most likely not significantly bleached during deposition and thus they date events prior to the latest ice advance.  相似文献   


4.
Fossil oyster reefs are indicators of past sea levels, and their formation is usually dated by means of radiocarbon. However, radiocarbon dating of the shells from coastal areas may be complicated by the varying sources of carbon. Here we applied optical dating methods to date the samples from above and below a fossil oyster bed in a section on the coast of Bohai Bay, China. The optical ages of the sediments were used to constrain the oyster bed. Single-aliquot regenerative-dose procedures using the OSL signal from fine grain quartz, the IRSL and post-IR OSL signals from polymineral fine grains were employed to determine equivalent dose (De). The behaviors of the different luminescence signals from quartz and polymineral grains during De measurements were examined. The results showed that the quartz OSL signal is more reliable than the polymineral IRSL and post-IR OSL signals with respect to dating for these coastal samples. The optical ages indicated that the oyster reef formed between ca. 6.2 and 5.0 ka.  相似文献   

5.
Linking the timing of glacial episodes and behaviour to climatic shifts that are documented in ice and marine sedimentary archives is key to understanding ocean-land interactions. In the NW Scottish Highlands a large number of closely spaced (‘hummocky’) moraines formed at retreating glacier margins. Independent age control on one palaeo-glacier limit is consistent with the timing of Younger Dryas (YD) glaciation in the area, but adjacent glacier lobes have remained undated due to the lack of sites and material for 14C dating. Direct dating of ice-marginal moraines using optically stimulated luminescence (OSL) techniques has never been attempted before in Scotland, but if successful, they may be the most appropriate methods for constraining the age of sediment deposition in the absence of organic material. Coarse-grained quartz and K-feldspar minerals from supraglacial sheet flow deposits and glacilacustrine sediments within ice-marginal moraines were analysed using the single-aliquot regenerative-dose (SAR) protocol. Independent age control and clear geomorphological relationships indicate that all samples should yield YD or post-Last Glacial Maximum (LGM) ages. Quartz OSL shine down curves showed low luminescence sensitivity, significant medium-to-slow components, a weak fast component, and scattered SAR data; Linearly Modulated-OSL (LM-OSL) measurements confirmed that the fast component was weak or absent. In contrast, feldspar infrared stimulated luminescence (IRSL) was highly sensitive with excellent SAR data. However, SAR data from 3 mm diameter aliquots of feldspar (200 grains) give higher than expected equivalent doses (De) by an order of magnitude. SAR measurements of small clusters of feldspar grains (ranging from 1–8) considerably broaden the apparent De distribution, but even the lowest value is about 2–3 times the expected De. Two possibilities arise to explain the quartz and feldspar data: (1) that glacial sequences in the NW Highlands re-work inherited (older) glacial deposits and that some of the pre-Devensian existing glacial landforms have only been modified during Devensian glaciation; or (2) that the sedimentary processes operating in these ice-marginal environments are not conducive to adequate bleaching of quartz and feldspar grains. Our study implies that ice-proximal supraglacial sediments from this region in NW Scotland reflect older ages of deposition, but dating YD sediments has not been possible.  相似文献   

6.
Post-depositional mixing or exhumation is common in surficial sediments, yet may be unobservable from field evidence. However, any disturbance may have significant consquences in terms of establishing a reliable luminescence age determination. Optically stimulated luminescence (OSL) measurements, particularly measurements at the single grain level, can be used to gain an insight into both contemporary and past post-depositional processes.

This paper examines sites from Texas and Florida (USA) with independent chronological control to demonstrate the potential effects of varying degrees of bioturbation on OSL. Results show that contemporary soil forming processes clearly impact on the palaeodose (De) replicate distributions which are measured in order to derive an OSL age. Significant levels of scatter and apparently zero dose grains are observed in the upper-most sediments; declining with depth from the surface. De replicates from undisturbed and fully bleached sediments are unskewed, show low overdispersion (OD) and comparable single grain and single aliquot OSL ages. Bioturbated sediments, however, may show highly skewed multi-model De distributions with higher OD values, zero dose grains at depth, and significant diffences between single grain and single aliquot results. True burial ages may be derived from minimally bioturbated sediments through the application of statistical analysis such as finite mixture modelling to isolate De components. However, for significantly bioturbated sediments, the latter approach, even at the single grain level, produces inaccurate ages. In such cases we argue that additional evidence (both dating and contexual) may be required to identify with confidence the burial De population.  相似文献   


7.
The southern coastline of South Africa exhibits extensive aeolianites and spectacular barrier dunes; the ages and palaeoenvironmental significance of which have, until recently, received limited attention. We present preliminary results for samples taken from a single 6.5 m section in the seaward barrier dune near to the town of Wilderness. The reliability of these ages has been investigated using a series of dose recovery and pulsed irradiation experiments, as well as through analyses of single aliquot and single grain De distributions. Results indicate that the SAR protocol is providing accurate and precise De determinations and that adequate sensitivity correction is being made. The application of pulsed irradiations does not result in significant changes in the dose–response curves or averaged De's. Single grain De distributions are broad, with significant levels of overdispersion, which may reflect beta dose heterogeneity effects.

Peaks in aeolian activity date to 157–154 and 140–125 ka, with a slower rate of deposition recorded from 115 to 85 ka. Brief phases at 40 and 21 ka are also identified. Some ages, notably those from OIS 3 and OIS 2, are surprising from a geomorphological perspective, given the likely distance of the dune from the shoreline at such times, although they are not inconsistent with evidence from the east coast of South Africa. The results reveal multiple phases of Late Quaternary barrier dune accumulation, and suggest that aeolian activity in this region has been episodic and potentially more complex than previously thought.  相似文献   


8.
Many of the small-scale arroyo systems found across southern Colorado contain well-preserved sedimentary records of prehistoric fluvial erosion and aggradation epicycles. In the following paper, we date a set of 50 ephemeral fluvial samples from four southern Colorado arroyo systems using a combination of single-grain and single-aliquot OSL techniques. Analysis of the sample De distribution characteristics reveals that these arroyo sediments were subjected to a diverse array of bleaching conditions prior to deposition. The use of appropriate burial dose estimation procedures is therefore deemed vital to ensuring that accurate age estimates are produced for each of these samples. In this study we apply the formal ‘age model’ decision procedures of Bailey and Arnold [Statistical modelling of single-grain quartz De distributions and an assessment of procedures for estimating burial dose. Quaternary Science Reviews, in press.] and Arnold [2006. Optical dating and computer modelling of arroyo epicycles in the American Southwest. D.phil. Thesis, University of Oxford, unpublished] to our fluvial sample dataset in order to enable a more objective selection of appropriate burial dose estimates. The resultant OSL chronostratigraphies are examined and discussed. These formal decision procedures yield sample ages that are stratigraphically consistent for 94% of the 50 fluvial samples examined. The resulting OSL ages also display a greater degree of stratigraphic consistency in comparison to those ages that would have been generated by simply applying a single type of age model to all samples.  相似文献   

9.
The Starmoen dune field is part of a larger aeolian system in the Jømna and Glomma river valleys in southeastern Norway. It is believed to have formed just after the last deglaciation in the area, but no absolute ages have been available to support this. Here, we present a set of quartz optically stimulated luminescence (OSL) ages from the aeolian sediments and the underlying glacifluvial deposits. The results show that the main dune-building phase was a short-lived event ∼10 ka ago, likely with a duration less than a few hundred years. This suggests a rapid stabilisation of an initially unstable environment in newly deglaciated terrain. A much younger event with limited and surficial reworking of sand is dated to 770 ± 110 years ago, and the modern age of an active dune provide additional OSL quality control. Age overestimation is found for glacifluvial sediments, probably due to incomplete bleaching as indicated by e.g. scattered dose distributions from small aliquots. OSL measurements were conducted using coarse quartz grains (180–250 m), which show a dominance of a fast signal component.  相似文献   

10.
Optically stimulated luminescence of fine silt quartz was investigated to establish chronologies for lake sediments from the British Isles. Feldspar contamination and its potential effects on equivalent dose (De) determination were examined. A new feldspar contamination test based on the thermal quenching of quartz OSL and thermal assistance of feldspar OSL identified feldspar contamination in samples being treated for 20 min in 20% hydrofluoric acid. Feldspar component monitoring based on the post-IR OSL/OSL ratio was not sufficiently sensitive to monitor a feldspar component, but is a good indicator whether a standard SAR procedure can be applied successfully, despite the presence of feldspar. Based on these results we used a modified SAR protocol including a 100 s IRSL stimulation at 50 °C before OSL readout. This protocol could overcome any malign effects of feldspar even for a feldspar bearing polymineral sub-sample.  相似文献   

11.
In this study we report on optical stimulated luminescence (OSL) ages of quartz extracted from a sedimentary record in the N-Oman mountain range. Equivalent dose (DE) distributions derived from single aliquot measurements (SAR) of small aliquots (ca. 200 grains) were investigated to test whether the skewness and broadness of the dose distribution can be used as criteria for the identification of insufficient bleaching. Furthermore, the methods proposed by Lepper and McKeever [2002 An objective methodology for dose distribution analysis. Radiation Protection Dosimetry 101 (1–4), 349-352]. Singhvi [Juyal, N., Chamyal, L.S., Bhandari, S., Bushan, R., Singhvi, A.K., in press. Continental record of the southwest monsoon during the last 130 ka: evidence from the southern margin of the Thar Desert, India. Quaternary Science Review] and Fuchs and Lang [2001 Fuchs, M., Lang, A., 2001. OSL dating of coarse-grain fluvial quartz using single-aliquot protocols on sediments from NE Peloponnese, Greece. Quaternary Science Review 20, 783–787.] to derive DE's from insufficiently bleached sediments were compared. At first, the investigations were carried out on artificially bleached, irradiated and mixed quartz material from the Oman study area to simulate insufficiently bleached sediments. Then, the various statistical methods for identifying insufficient bleaching and DE derivation were applied to the natural samples from the study area, where 18 samples were measured. For the identification of insufficient bleaching the preferential parameter is the broadness of a distribution. For DE calculation, both the Singhvi method and the Fuchs and Lang method produce similar results, which are consistent with the stratigraphic order. A drawback of both methods is their sensitivity to low outliers. The Lepper and McKeever method was not applied to the natural samples, due to limitations in its application to a small number of aliquots and due to the ambiguous identification of the rising limb of the dose distributions.  相似文献   

12.
There are only a few luminescence dating studies of loess sediments in Japan, but interleaved with these deposits are many well-described tephras of known age based on 14C and fission track analysis; these independent age controls provide an opportunity to test the reliability of loess luminescence ages. This study provides such a comparison at two sites in central Honshu, the largest island in the Japanese archipelago. Samples were collected from sequences of interleaved volcanic tephra and loess deposited on a Middle Pleistocene river terrace in the Niigata Prefecture and on an Early to Middle Pleistocene dissected fluvial surface at in the Tochigi Prefecture, Honshu. Equivalent doses (De) were estimated from fine grains (4–11 μm) using both polymineral IR-OSL and (post-IR) blue-OSL, and quartz blue-OSL. The blue-stimulated luminescence signals could be represented by up to three exponentially decaying components; only the most light sensitive of these components was used in the final De estimation. Almost all the estimates of De from polymineral IR-OSL are smaller than those from polymineral (post-IR) blue-OSL and quartz blue-OSL, whereas the latter two are in good agreement. The blue-light stimulated luminescence ages using the most light sensitive component are shown to be in good agreement with the independent control, up to 500 ka. Although the IR-OSL signals underestimate the known age, a simple laboratory fading test is found empirically to correct for this underestimation. We conclude that the most rapidly blue-stimulated luminescence signals from quartz extracted from our loess samples give reliable ages, and that future loess dating studies should concentrate on these signals.  相似文献   

13.
Quartz optically stimulated luminescence (OSL) forms the basis for the chronology of Weichselian ice advances in Arctic Eurasia developed over the last few years. There is almost no age control on this chronology before 40 ka, except for some marine sediments correlated with marine isotope stage (MIS) 5e on the basis of their palaeofauna. Results from more southern latitudes have shown that dose estimates based on quartz OSL and the single aliquot regenerative (SAR) dose procedure may underestimate the age of MIS 5e deposits. Here we use the same method to date well-described marine sediments, thought to have been deposited during the very beginning of the Eemian interglacial at 130 ka, and exposed in two sections on the river Sula in northern Russia. Various quality-control checks are used to show that the OSL behaviour is satisfactory; the mean of 16 ages is 112±2 ka (σ=9 ka). This represents an underestimate of 14% compared to the expected age, a discrepancy similar to that reported elsewhere. In contrast to SAR, the single aliquot regeneration and added (SARA) dose procedure corrects for any change in sensitivity during the first OSL measurement. The SARA results are shown to be 10% older than those from SAR, confirming the geological age estimate and suggesting that SAR ages may underestimate older ages (larger doses), despite their good performance in the younger age range.  相似文献   

14.
This study reports on the first investigation into the potential of quartz luminescence dating to establish formation ages of ferruginous duricrust deposits (ironstones) of the Xingu River in Eastern Amazonia, Brazil. The studied ironstones comprise sand and gravel cemented by goethite (FeO(OH)), occurring as sandstones and conglomerates in the riverbed of the Xingu River, a major tributary of the Amazon River. The Xingu ironstones have a cavernous morphology and give origin to particular habitat for benthic biota in an area that hosts the largest rapids in Amazonia. So far, the Xingu ironstones have uncertain formation ages and their sedimentary origin is still poorly understood. In this way, seven samples of ironstones distributed along the lower Xingu River were collected for optically stimulated luminescence (OSL) dating of their detrital quartz sand grains. Additionally, the organic content of some samples was dated by radiocarbon (14C) for comparison with quartz OSL ages. The luminescence ages of the sand-sized quartz grains extracted from the ironstones were obtained from medium (100–300 grains) and small (10–20 grains) aliquots using the single aliquot regenerative-dose (SAR) protocol. Equivalent doses (De) distributions have varied overdispersion (OD) both for medium size aliquots (OD = 19–58 %) and small size aliquots (OD = 29–76 %). No significant trend was observed between De and aliquot size. The studied ironstones grow over the riverbed, but stay below or above water throughout the year due to the seasonal water level variation of the Xingu River. However, the effect of water saturation in dose rates is reduced due to relatively low porosity of ironstones. Water saturated dose rates (dry sample dose rates) range from 2.70 ± 0.21 (2.79 ± 0.22) Gy/ka to 12.34 ± 0.97 (13.26 ± 1.12) Gy/ka, which are relatively high when compared to values reported for Brazilian sandy sediments elsewhere (∼1 Gy/ka). Samples with high overdispersion (>40 %) are mainly attributed to mixing of grains trapped in different time periods by goethite cementation. The obtained OSL ages for water saturated (dry) samples range from 3.4 ± 0.3 (3.3 ± 0.4) ka to 59.6 ± 6.0 (58.1 ± 6.4) ka, using De determined from medium size aliquots and dose response curves fitted by an exponential plus linear function. Radiocarbon ages of the bulk organic matter extracted from selected ironstone varied from ca. 4 cal ka BP to ca. 23 cal ka BP. Significant differences were observed between OSL and radiocarbon ages, suggesting asynchronous trapping of organic matter and detrital quartz within the ironstone matrix. These late Pleistocene to Holocene ages indicate that ironstones of the Xingu River result from an active surface geochemical system able to precipitate goethite and cement detrital sediments under transport. The obtained ages and differences between OSL and radiocarbon ages point out that the ironstones have multiphase and spatially heterogeneous growth across the Xingu riverbed. Our results also expand the application of luminescence dating to different sedimentary deposits.  相似文献   

15.
Endorheic basins, filled by a rhythmic stratification of fluvio-lacustrine sediments, are useful archives for studying the interaction of palaeoenvironment and prehistoric development. Archaeological evidence indicates an occupational maximum during the Early to Mid-Holocene humid phase that can be linked to geochronological dates. A wadi has cut these sediments and a wadi profile of about 6 m was sampled for luminescence dating.

Palaeodose estimates are based on single aliquot measurements of the sand-sized quartz fraction using the regenerative dose technique. The comparison of equivalent dose results from different aliquot sizes (<100 and >1000 grains) provides interesting insights into heterogeneous degrees of bleaching. Problems arising from substantial variations in environmental dose rates of such heterogeneous sediments are discussed.

The luminescence ages indicate two major phases of deposition, both of Holocene age. The lower 2 m of sediments were deposited about 9400 years ago. The sedimentation of the upper 2 m started about 7200 and terminated around 6300 years ago. Radiocarbon ages of charcoals contained in the upper part of the section disagree with that OSL dating. This discrepancy is explained by re-deposition of the charcoal fragments.  相似文献   


16.
The effect of weathering on optically stimulated luminescence dating   总被引：2，自引：0，他引：2  
Optically stimulated luminescence (OSL) dating was applied to quartz samples recovered from the gravel sediments of deformed marine terrace at the Suryum site, southeastern Korea, but has yielded stratigraphically inconsistent ages. Micromorphological, chemical, and mineralogical analyses of the gravels indicate the possible influence of chemical weathering on the apparent OSL ages. In the course of weathering after emerging from beach environments, originally permeable gravels underwent infilling by halloysite-rich clays in their voids, export and import of radioactive elements, and loss of mechanical strength with the creation of a porosity within pebbles. Calculation based on the evolution of the weathering profile showed a severe fluctuation of dose rate caused by the change of water content and radioactive element concentrations. Samples recovered from the weathering profile inevitably include quartz grains derived from mechanically weakened pebbles or illuviated from the upper layer, making it difficult to determine the equivalent dose (De) values of exclusively depositional quartz sands. Quantitative evaluation of the change of fabric and chemistry of the sediments on the basis of pedologic insight significantly aids in the derivation of OSL ages consistent with geomorphology and other independent age controls.  相似文献   

17.
A comparative study using quartz optically stimulated luminescence (OSL) and feldspar post-infrared infrared stimulated luminescence (post-IR IRSL) was undertaken on Quaternary fluvial sediments from an unnamed tributary of the Moopetsi River in South Africa. The aim is to assess whether the post-IR IRSL signal can be used to date incompletely bleached sediments. Several post-IR IRSL signals using varying stimulation and preheat temperatures were investigated; of these the post-IR IRSL225 signal was deemed most appropriate for dating because it bleached most rapidly. The feldspar post-IR IRSL225 equivalent dose (De) values from this site are consistently larger than those from quartz OSL, probably due to differences in the bleaching characteristics of the two signals. Additionally, the post-IR IRSL225 De values within a sample showed less variation in precision than the quartz De data, possibly due to greater averaging between grains in the feldspar small aliquots. The agreement between ages based on the OSL and post-IR IRSL225 signals was better for younger samples (<20 ka) than for older ones (>50 ka); the cause of this variation is unclear.  相似文献   

18.
OSL dating of sediments from deserts in northern China   总被引：2，自引：0，他引：2  
Aeolian samples from deserts in northern China were studied using the optically stimulated luminescence (OSL) of quartz and potassium (K) feldspar separates. K-feldspar has shown advantages over quartz for dating samples younger than 100 years, due to its more homogeneous equivalent dose (De) values, higher internal dose rate and higher luminescence sensitivity to dose. Without additional measurements, the luminescence characteristics of quartz obtained in De determination procedures can be used to reveal the source material and/or quartz thermal history for the deserts in northern China. The results indicated that the duration of paleosol formation in desert areas reflects regional paleoenvironments.  相似文献   

19.
The numerical dating of megaflood sediments is a worldwide challenge, a fact that has impeded a full understanding of Late Quaternary dam-outburst flood processes that occurred along the river courses of the Tibetan Plateau. Optically stimulated luminescence (OSL) dating has been widely used on such sediments. Due to their short transportation distances prior to deposition, the OSL signals of megaflood sediments are often partially bleached, resulting in age overestimations. Here, we report on a comparison of OSL ages obtained using both quartz (4–11 μm FG; 90–125, 180–250 μm CG) and K-feldspar (180–250 μm CG) extracted from sediments taken from the Binghong-Bingnong Neolithic-Bronze Age site on the second Jinshan River terrace (T2), in Yunnan Province, southwestern China. Contrary to previous experience suggesting that CG fractions are usually better bleached than FG fractions prior to deposition, our results showed that the OSL ages for the FG quartz fraction were generally younger than those for the CG fraction. This would suggest that the two fractions may have come from different sources, and may have been subject to different geomorphological processes prior to deposition. FG quartz fractions may be suitable to define the maximum age of sediments located in alpine gorge regions. CG quartz fractions can be used by applying the minimum age model (MAM) to select relatively well-bleached grains yielded ages close to the ‘true’ burial ages of the sediments. The results showed that the post-IR IRSL225 ages of single grain K-feldspar were overestimated by > 3 ka, suggesting K-feldspar may not be suitable dating material for megaflood sediments <30 ka. The OSL dates suggest that the T2 terrace was formed ∼8.4 ka, that aeolian sediments were deposited during ∼2.6–1.5 ka, and that the megaflood event occurred after ∼1.5 ka.  相似文献   

20.
The Altyn Tagh Fault(ATF)is one of the most prominent active strike-slip faults in the India-Eurasia collision. Fresh features of surface ruptures, which are attributed to seismic events taking place in the last millennium, are identified at several sites along the Che'erchen River to Qingshui River section on the central part of ATF. Accurate chronology of these earthquake events would help understand the spatial-temporal relationship of the recent earthquakes. However, great difficulties are encountered. The central ATF is located in the arid area, and the vegetation cover is so limited that rare organic materials appropriate for radiocarbon dating can be found in the sediments. Luminescence dating technique may serve as an alternative to directly determine the burial ages of the earthquake related sediments. The optically stimulated luminescence(OSL)signal of quartz, which has been widely employed for luminescence dating, displays unwanted charateristics for accurate dating. Firstly, the quartz OSL signal is not sensitive to irradiation, which leads to low signal-to-noise ratio or even no measurable quartz OSL signal. Secondly, the targeted samples of the last millennium are very young, and the radiation dose received during the burial is expected to be less than 3~4Gy, which futher deteriorates the signal-to-noise ratio of the quartz OSL signal. Therefore, quartz OSL signal is not appropriate for dating the sediments relevant to the recent earthquakes on ATF.
The infrared stimulated luminescence(IRSL)signal of potassium feldspar is an alternative, and it is in usual an order of maginitude more sensitive to raidation than the quartz OSL signal. The enhanced signal-to-noise ratio makes it applicable to young samples. The post-IR IRSL signal has been successfully applied to date the sediments beyond the Holocene, however, the relatively slow bleaching of the post-IR IRSL signal poses challenges on applying it to young sediments, especially for the sediments deposited during the last millennium. In this study, we investigated the feasibility of using post-IR IRSL signal from potassium feldspar to date the earthquake events of the last millennium by employing modern sag pond deposits with different sorting and expected equivalent dose(De)of 0Gy. Choosing an appropriate measurement procedure and identifying the well bleached pottassium feldspar grains are essential for post-IR IRSL dating of young sediments. The non-fading characteristic of the post-IR IRSL170 signal measured at 170℃ following a prior IR stimulation at 110℃ was verified by employing the De plateau test with respect to the signal integration interval and IR stimulation temperature together. Reducing the amount of potassium feldspar grains mounted on an aliquot would help reveal the among grains variation of bleaching level of post-IR IRSL170 signal before depostion and identify the most sufficiently bleached grains. Therefore, the post-IR IRSL170 De values of 2mm aliquots were measured for three samples with different sedimentary textures. The median of De distribution of well sorted and stratified sag pond deposits is consistent with the minimum De value inferred from the minimum age model(MAM-3) and finite mixture model(FMM), while for the poorly sorted deposits, the median is significantly overestimated compared with the minimum De values from the MAM-3 and the FMM. The minimum De values of 0.6~0.8Gy of all three samples are consistent with the unbleachable residual dose previously reported for post-IR IRSL signals measured at similar temperature for well bleached samples. It implies that by combined use of small aliquot and statistical age models, the well-bleached potassium feldspar grains could be identified. Such an intrinsic unbleachable component needs to be properly corrected when earthquake events of last millennium are to be dated in this area. Otherwise, the post-IR IRSL170 age would be overestimated by 200~300a.
The post-IR IRSL170 procedure investigated in this study is not only applicable for dating the paleoearthquake events along the Altyn Tagh Fault, but also with great potential to be applied to other tectonically active area. With consideration of the potential variability in post-IR IRSL signal characteristics of potassium feldspar grains from different origins, the signal stability needs to be routinely inspected. The modern analog sample would also be informative for justifying the measurement procedure and analytical method employed.  相似文献   

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