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针对岩矿测试中传统手段无法直接获取岩心样品内部特定矿物颗粒的空间分布、含量等信息,文章利用不同密度的矿物对X射线具有不同衰减系数这一特性,研究了不同测定条件下黄铁矿、黄铜矿和沥青铀矿的灰度变化特征,并通过灰度特征确定了区分3种矿物的最佳测量条件。通过测定包括沥青铀矿在内的多种常见的单矿物灰度特征,研究了沥青铀矿对各种常见矿物的识别率。研究结果表明,除方铅矿、重晶石等矿物外,其余常见矿物对沥青铀矿的识别率优于95%。通过模拟岩心测定结果表明,X-CT技术对沥青铀矿识别结果与真实值基本一致。该研究对无损条件下直观了解岩心内部目标矿物的空间赋存状态以及为数字岩心提供了技术支撑。 相似文献
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应用轻便X射线荧光仪和X射线荧光测井仪,在我国某锑矿上进行了试验.对锑矿粉末样品、锑的化探样品、原始产状锑矿X射线取样、块状岩心及充满泥浆的锑矿钻孔进行了分析测量,并与化学分析比较,结果十分一致.特别是在消除基体效应方面取得了良好的效果. 放射性同位素X射线荧光技术在地质勘探工作中应用的特点是:仪器轻便,射线防护简单,操作容易,便于现场使用,测量速度快,对样品中元素含量能进行定量或半定量测定.在普查找矿阶段,可用来对某些地质远景地段进行及时检查,从而加速岩体评价.在化探工作中,可对中等强度以上的化探分散晕异常地段和水系底部沉积物的淘洗重矿物进行半定量或定量测量, 相似文献
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研究了高纯锗γ能谱仪测定铀矿地质试样中铀、钍、镭、钾的测量条件，解决了高含量样品的测量准确度问题，确定了最佳工作条件，提高了分析精度。经标准物质和生产样品验证，分析结果满足铀矿地质样品分析规范要求。 相似文献
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μ-XRF技术在黄龙铺钼(铀)矿床铀矿物学研究中的应用 总被引：1，自引：0，他引：1
东秦岭碳酸岩型钼成矿带是全球最大的钼成矿带。该带内的黄龙铺矿床是中国最早发现的碳酸岩型钼矿床之一。最近的野外地质调查发现,部分钼矿石具有较高的放射性异常,但其放射性元素的赋存形式和矿物学特征尚不明确。本文借助聚毛细管微束X射线荧光光谱分析(μ-XRF)分析速度快、原位无损、高灵敏度的分析优势,快速查明铀矿物的空间位置,再结合扫描电镜分析(SEM)和X射线能谱分析(EDS),确定铀矿物的种类及其次生变化。研究表明:黄龙铺矿床高放射性矿石中主要的铀矿物为钛铀矿、铌钛铀矿和晶质铀矿,它们与方解石、长石、黄铁矿、辉钼矿和黄铜矿呈共生关系。矿石中铀矿物后期均遭受氧化性流体改造,发生了明显的蚀变,钛铀矿蚀变之后转变为含Nb的钛铁氧化物,铌钛铀矿和晶质铀矿蚀变后矿物内部形成大量空洞,流体来源可能为大气降水。背散射电子(BSE)图像上灰度差异明显,暗示着矿物中元素分布的不均一性。 相似文献
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《矿物岩石》2014,(4)
以北祁连锆英石(776Ma±10Ma)为研究对象,利用60 Co源γ射线辐照装置对其进行γ射线辐照。借助偏反多功能显微镜、阴极发光、背散射电子、电子探针对样品微观形貌进行观察与分析,并对样品产出的地质背景和化学成分进行研究,并利用X射线衍射、激光拉曼光谱和红外光谱等表征手段对γ射线辐照前后样品的物相、结构进行测试分析。并对样品产出的地质背景和化学成分进行研究,明确放射性核素固化介质备选矿物锆英石的特征结构变化及抗γ射线辐照能力。结果表明:北祁连所产出的锆英石系变质成因,经约7.76×108 a的地质演变后,对UO2和ThO2的包容量仍为0.118%,晶胞参数较标准样品发生了10-3 nm量级的微小变化。样品经576kGy的γ射线辐照后晶胞参数较辐照前发生了10-4 nm量级的变化,辐照后样品结构的无序程度略显增强。锆英石在包容一定量U和Th的情况下具有较好的抗γ射线辐照结构稳定性。 相似文献
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在铀矿航空γ能谱测量和地面放射性普查工作的基础上,通过对铀矿异常进行地表揭露和钻探工程验证,发现了芒和特铀矿床。铀矿床类型为湖沼相砂岩型沉积矿床,含铀矿岩石为古近系粉砂岩,铀矿化具有放射性强度较弱、铀含量较高和矿化分布不均匀的特点。深入分析铀矿放射性强度弱的原因,采用放射性测量结合化学样品分析的方法,能够提高找矿效率。 相似文献
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《地质科技情报》2016,(6)
钻孔岩心高光谱技术是高光谱遥感技术的延伸运用方向,它将高光谱遥感矿物填图技术应用于深部钻孔岩心蚀变信息的提取,为深部地质研究提供了新的思路与方法。在遥感技术系统的基础之上建立了钻孔岩心高光谱技术系统体系,并以Hyspex钻孔岩心高光谱采集系统为例,对我国南方某火山岩型铀矿勘查区钻孔岩心高光谱数据进行了处理和示范性应用。岩心高光谱数据预处理包括辐射校正、反射率计算和光谱去噪3个步骤,之后的蚀变信息提取包括端元光谱识别和光谱匹配填图2个步骤。利用处理之后的岩心蚀变矿物全孔编录结果,进行了蚀变矿物空间分带规律分析和蚀变矿物组合划分,并对钻孔蚀变信息反映的深部流体环境进行了分析和反演,结合钻孔地质资料,发现该钻孔铀矿化富集部位处于蚀变矿物酸碱性发生突变的地球化学障部位这一特征。最后,对钻孔岩心高光谱技术的特点及优势进行了总结,其能够为深部矿产资源勘查提供有效技术支撑,值得进一步推广应用。 相似文献
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A method has been developed to determine the state of disequilibrium and uranium content in geological samples using low energy gamma scintillation spectrometry. Ore standards in radioactive equilibrium were prepared in different concentrations and their low energy spectra were compared with those of chemical uranium standards of the same concentrations. The standards were analysed carefully for their U contents using X-ray fluorescence and high resolution gamma spectrometers. Counts of the complex peak under which 63 keV and 93 keV photopeaks take place in ore spectra were compared with the counts in corresponding channels of chemical uranium spectra. For standards in equilibrium it was found that (26 ± 2)% of the counts under complex peak came from Th-234 and also there was a constant relation between Th-234 (63 keV and 93 keV) and Pb-210 (47 keV) counts. The technique was applied to the geological samples for which eU concentrations had been measured previously by means of high energy gamma spectroscopy in the same laboratory. 相似文献
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A. R. Ramsden B. L. Dickson R. L. Meakins 《Australian Journal of Earth Sciences》2013,60(3-4):285-296
The Toolebuc Formation, which is a potentially important source of oil shale in the Eromanga Basin of NW Qld, exhibits a marked gamma‐ray response that has long beeen used as a stratigraphic marker. At Julia Creek, a large area of the Formation contains low‐grade oil shale that is accessible to mining. Detailed investigation, by gamma‐ray spectrometry and neutron activation analysis, of drill core samples from this deposit and from the type section of the Toolebuc Formation at Boulia (BMR Boulia 3A stratigraphic drill hole) show that the Toolebuc gamma‐ray anomaly in the northern Eromanga Basin is due to the presence of uranium. Analyses for organic carbon and phosphorus show that the uranium is associated primarily with organic matter in the oil shales and with phosphatic skeletal fish debris in the accompanying coquinites. Drill core samples from Tibooburra, N.S.W. were also analysed (BMR Urisino‐1 stratigraphic drill hole) to investigate whether the gamma‐ray anomalies observed in the Bulloo Embayment on the southern margin of the Eromanga Basin (possibly correlative with the Toolebuc Formation) might also be indicative of oil shale. The results show that the much weaker anomaly at this locality is due principally to potassium and reflects the presence of an argillaceous siltstone within glauconitic sandstones. 相似文献
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Relation between source rock properties and wireline log parameters: An example from Lower Jurassic Posidonia Shale, NW-Germany 总被引：1，自引：0，他引：1
The relationships between source rock quality and wireline log parameters were established for the Lower Jurassic Posidonia Shale, the most prolific petroleum source rock of Central Europe. Wireline logs used are the gamma ray spectrometry, density, sonic and various resistivity logs. The organic geochemical parameters considered include the organic carbon content, hydrogen index, and the hydrocarbon potential expressed by pyrolysis yield. The case history presented is based on a continuous core through the entire Posidonia Shale interval from a location where this source rock is immature. Care was taken to detect and to avoid samples and log values influenced by bore hole roughness and fractures. Fair correlations were observed only between uranium content from gamma ray spectrometry log and organic carbon content. No correlation was recognized between uranium content and kerogen type as defined by hydrogen indices. For various reasons density, sonic, and resistivity logs did not provide useful data in this study.Three rock units with irregular, high and low uranium contents could be differentiated. Possible causes for this tripartition are different environments during deposition and postdepositional redistribution of uranium during early diagenesis and in association with fractures. 相似文献
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车载台式能量色散X射线荧光光谱仪在地球化学勘查现场分析中的应用 总被引：10，自引：10，他引：0
充分发挥小型实验室设备的功能以提高现场快速分析的能力。在内蒙和新疆两地覆盖区的钻探现场,采用车载化台式偏振能量色散X射线荧光光谱仪,对由轻便钻采集的覆盖层和基岩样品进行了贱金属分析。共采集、制备和分析了约400件钻探样品,采用能量色散X射线荧光光谱法、波长色散X射线荧光光谱法和电感耦合等离子体质谱法对这些样品进行比对分析。现场分析数据与实验室分析数据(各方法的平均值)的比对结果表明,K、Ca、Ti、V、Cr、Mn、Fe、Ni、Cu、Zn、Ga、As、Rb、Sr、Y、Zr、Nb、Ba、Pb、Th等20余种元素的分析数据的一致性良好;含量超过10μg/g时,除了V和Ba外,其他元素的平均相对偏差均小于25%。在现场作为质控样品分析4个地质标准物质GBW07301～GBW07304,测定结果表明,除了低含量的Cu和Ga外,上述其他18种元素均符合地质行业标准地质矿产实验室测试质量管理规范(1∶20万)规定的误差要求。应用研究表明,设计的仪器车载化方案可行,现场分析方法快速、准确,适用于野外钻探、化探等急需现场数据支持的工作。 相似文献
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Chemical and radiometric analyses have been made on core samples from 15 drill holes intersecting the Toolebuc Formation at Julia Creek. The holes are located in the vicinity of the St Elmo Structure and include intersections of a potentially economic oil shale deposit west of this structure as well as non‐economic mixed coquinite/shale intersections to the east. The gamma ray activity of the formation is due largely to uranium in the shales. Wire‐line gamma ray logs, available for eight of these holes, reflect the distribution of organic carbon. Despite this, there is poor correlation between uranium and organic carbon in the oil shales as a result of remobilization of uranium from organic matter into phosphate during diagenesis. In consequence wire‐line gamma ray logs have no potential for evaluating oil yield. Density, on the other hand, is a good indicator of oil potential. On a hole by hole basis, the correlation between uranium and organic carbon in the formation ranges from 0.22 west of the St Elmo Structure (the potential oil shale resource) to 0.95 east of the structure. This reflects a systematic change in sedimentology from oil shale that is thick and well separated from coquinite (low correlation) to laterally equivalent but finely interbedded coquinite and shale (high correlations). Such trends could be used in exploratory drilling to indicate favourable areas elsewhere in the Toolebuc Formation. 相似文献
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“煤铀兼探”“油铀兼探”是当今的研究热点,利用煤、油气田钻井的测井资料评价铀资源潜力是尚待解决的难题。以鄂尔多斯盆地彭阳铀矿区为例,开展基于自然伽马测井数据的铀资源评价方法探索。根据彭阳铀矿区砂岩型铀储层自然伽马异常响应显著的特性,通过对比分析9个验证孔中定量伽马和油田钻孔中自然伽马测井数据,研究彭阳铀矿区矿层定量伽马值的自然伽马测井回归模型,研发矿层平米铀量筛选计算程序。初步建立基于自然伽马测井信息的区域铀矿层识别和品位评价方法,研究成果精度与实测数据吻合,解决了难以高效利用常规煤、油气田测井资料进行铀矿层识别和品位评价的问题。该成果可为鄂尔多斯盆地铀资源调查和潜力评价提供有效的技术支持。 相似文献
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花岗伟晶岩型铀矿床是一种重要的铀矿化类型,其矿化层严格受到花岗伟晶岩脉控制,矿化层围岩为片岩、片麻岩和混合岩等。花岗伟晶岩脉由硅质物肢结,坚硬质密,不透水,其测井结果表现为高电阻和高自然伽玛特征。而其围岩片岩、片麻岩和混合岩层理和解理非常发育,并富含层间水,测井结果表现为低自然伽玛、低电阻和低自然电位异常特征。花岗伟晶岩型铀矿含矿层与其围岩物性差异较大,利用地球物理测井参数的差异来评价岩矿层和铀成矿规律显然是一种较好的铀矿勘查工作方法。FD--3019伽玛定量测井是铀矿钻探勘查定量解释必不可少的一项基本测井工作;2007年以前花岗伟晶岩型铀矿钻探勘查没有尝试用电阻率、自然电位等综合测井参数评价预测铀矿化情况,实践结果证明通过综合测井曲线解释能够更准确的预测花岗伟晶岩脉的展布规律,科学划分钻孔地质剖面,为花岗伟晶岩型铀矿勘查评价和预测提供可靠依据,并且及时准确的指导野外生产和钻探设计工作。 相似文献
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为扩大粤北花岗岩型铀矿找矿成果,以青嶂山矿集区1:5万210Po测量数据为依据,研究了210Po法在粤北花岗岩型铀矿找矿中的异常特征及应用效果。结合研究区地质特征,应用趋势面分析等数理统计方法对数据进行处理,结果表明:趋势面分析消除了不同铀含量的地质背景对提取210Po异常的影响;210Po法与地面伽马能谱、氡气测量、 AMT组合应用对寻找花岗岩区深部隐伏矿体具有良好的效果,多种测量方法均出现峰值的部位,为含矿构造带或铀矿体产出部位;经钻探工程验证,在210Po法及相关方法异常区揭露到铀矿工业矿段,210Po法在粤北花岗岩型铀矿勘查中具有较大的指导意义。 相似文献
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A low-energy gamma ray spectrometric set-up for determination of uranium, thorium and potassium in rock and soil samples is described. The procedure described exploits the fact that a large proportion of gamma quanta produced in the Th and U decay series have energies of less than 1 MeV. The instrumental parameters such as sensitivity and detection limits for the low-energy region have been studied. The measuring conditions were optimized by suitably minimizing the background and by increasing the overall sensitivity with the help of proper geometry of measurement and sample parameters. High sensitivity and low detection limits for U and Th can be achieved using low-energy gamma ray spectrometry. The method provides a rapid analysis with a counting time of the order of a few minutes for each sample. 相似文献