共查询到20条相似文献，搜索用时 484 毫秒
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提出了Tamm溶液提取-石墨炉原子吸收光谱法对土壤样品中有效钼的测定方法。有效钼标准曲线的相关系数为0.9995,方法检出限为0.005 mg/kg,定量限为0.018 mg/kg;采用有证标准物质对方法适用性进行了考察,本方法测定值与认定值基本一致,且相对误差(RE)不大于4.17%,相对标准偏差(RSD)不大于7.87%,本方法检出限低、精密度和正确度较好,满足土壤样品测试工作的要求,简化了工作流程,提高了工作效率,适用于批量土壤样品中有效钼的测定。 相似文献
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断续流动氢化物发生-原子荧光光谱法测定地球化学样品中的痕量锗 总被引：5，自引：0，他引：5
采用断续流动进样方式的原子荧光仪测定地质样品中的痕量锗,方法测定检出限为0.07×10-6,测定范围0.2μg/g～100μg/g,相对标准偏差小于7.45%,样品加标回收率为96.7%～105.0%,经标准样品验证,方法准确可靠。 相似文献
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本文通过阐述用过氧化钠碱熔法处理矿样,以盐酸—柠檬酸—过氧化氢混合酸液提取样品,可有效避免硅胶的产生和钼、钨酸沉淀的生成。选择Mo 202.031nm、W207.912 nm、Cu 324.754nm、Pb 220.353nm、Zn 213.856nm谱线作为钼钨铜铅锌的分析线,用ICP-AES光谱法测定。各元素检测限分别为钼0.005μg/mL,钨0.010μg/mL,铜0.012μg/mL,铅0.018μg/mL,锌0.006μg/mL。通过对标准物质试样测试,待测元素含量值与认定值相符。该方法精密度、准确度良好,可适用于生产中同时对大批量矿石中钨钼铜铅锌含量的快速测定。 相似文献
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采用氢氟酸-盐酸-硝酸-硫酸四酸溶矿,建立了电感耦合等离子体发射光谱仪法(ICP-AES)同时测定钒钛磁铁矿、钛铁矿中铝、钙、镁、钾、钠、锰、钛、铬、锶、锌和钒11种元素的方法。对最佳仪器条件及分析谱线进行了优化筛选,并探讨了4种消解方法及酸度对测定的影响。实验结果表明:ICP-AES法测定钒钛磁铁矿、钛铁矿中铝、钙、镁、钾、钠等元素,与原子吸收光谱法、分光光度法、滴定法、重量法等单一元素测定方法相比较,具有检出限低、灵敏度高、测量范围宽、操作简便,适合大批量样品测定等突出优点。方法准确度(RE)小于10%,元素精密度(RSD,n=12)为0.68%~5%。采用国家一级标准物质进行了方法验证,取得了令人满意的结果。 相似文献
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采用HCl-HNO3-HF-H2SO4溶矿,利用电感耦合等离子体发射光谱仪内标法（ICP—AES）测定,建立了钛铁矿、钒钛磁铁矿中铜、钴、镍、锰、钒、铬等元素的同时测定方法。对电感耦合等离子体发射光谱仪测定的最佳仪器条件及分析谱线进行了选择,并对钛、铁基体的影响以及采用Y内标元素消除基体的影响进行了研究。实验结果表明：采用内标法能够消除基体对被测元素的影响,改善分析准确度和精密度,与经典分光光度法和原子吸收法相比较,具有检出限低、灵敏度高,操作简便、快速等突出优点。方法经国家一级钒钛磁铁矿标准物质验证,测定值与标准值吻合。 相似文献
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红藻石和蓝藻石概念及分类归属的综述和修订 总被引：1，自引：0，他引：1
在分析和总结前人对红藻石和蓝藻石研究成果基础上,结合岩石薄片显微镜下观察实例,发现在以往碳酸盐岩颗粒分类中没有红藻石和蓝藻石的合适位置.鉴于红藻石重要的成因意义和造礁作用,有必要明确红藻石的概念和归属.珊瑚藻本身极易钙化,经生物矿化作用最终保存下来的珊瑚藻屑一直放在生物碎屑中,而红藻石是由非固着的珊瑚藻构成的钙质独立结... 相似文献
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即将到来的新世纪,是一个全新的网络化的市场时代。网络营销是每一个商家的必然选择。网络市场在经过了3个阶段的演变后,将会有较大发展。它具有无店铺经营的若干基本特征,具有发展公共关系等多种功能。 相似文献
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动力及环境集中监控系统应用中问题的分析及建议 总被引：2，自引：0，他引：2
介绍了通讯专网机房集中监控系统的整体情况,组网方式,重点讨论了动力及环境集中监控系统在使用过程中存在的一些问题,提出了改进建议,最后对监控系统的管理问题提出了看法. 相似文献
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村镇社区作为我国社会的基层组织,是社会生活最基本的环境载体,村镇社区对地方病、传染病防治工作的开展对城市社会医疗卫生工作的良性运行具有重要的影响.计算机、网络、数据库等技术的发展,为提高村镇社区地方病、传染病的防治管理水平提供了有效的途径.从村镇社区实际出发,设计了基于Java Applet的电子地图应用程序JAEMA,在此基础上,采用轻量级设计模式,综合运用Struts+Spring+Hibernate框架构建了村镇社区地方病、传染病防治咨询系统EIPCAS,为提高村镇社区地方病、传染病防治水平提供有效的技术支撑和决策支持. 相似文献
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Mollisols properties and changes in Ukraine and China 总被引：4，自引：2，他引：2
Soils are the foundation of civilizations and the basis for human food production.Mollisols in Ukraine and Northeast China are two out of the four major Mollisol regions in the world.The natural areas from which Mollisols developed are the prairies and steppes that experience temperate and freezing conditions.This review paper introduces the general climate,vegetation,and topography of Mollisols regions in Ukraine and Northeast China,analyzes their properties,including soil texture,soil organic matter content,soil bulk density,pH,cation exchange capacity and other chemical properties,and compares the property changes and management practices of Mollisols in relation to sustainable grain production. 相似文献
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张兴旺 《成都信息工程学院学报》2006,21(1):96-100
在简单分析“T”形天线和地波传输特点的基础上,以行业标准中对NDB覆盖半径和覆盖区中最小场强为切入点,运用电磁波传输和天线与地网的工程公式,探索了NDB天线和地网的设计原理和计算方法.据此建立相应的数学模型. 相似文献
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根据在激光原理与激光技术课程建设和教学改革实践中的体会,从课程建设和教改的必要性、课程内容体系改革、教学手段和方法改革、课堂教学模式的探索和实践、大力培养学生科研意识和创新精神、完善课程考核模式等方面作了详细分析和阐述. 相似文献
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Pak-TaoLeung CarlH.Gibson 《中国海洋湖沼学报》2004,22(1):1-23
Turbulence is defined as an eddy-like state of fluid motion where the inertial-vortex forces of the eddies are larger than any of the other forces that tend to damp the eddies out. Energy cascades of irrotational flows from large scales to small are non-turbulent, even if they supply energy to turbulence. Turbulent flows are rotational and cascade from small scales to large, with feedback. Viscous forces limit the smallest turbulent eddy size to the Kolmogorov scale. In stratified fluids, buoyancy forces limit large vertical overturns to the Ozmidov scale and convert the largest turbulent eddies into a unique class of saturated, non-propagating, internal waves, termed fossil-vorticity-turbulence. These waves have the same energy but different properties and spectral forms than the original turbulence patch. The Gibson (1980, 1986) theory of fossil turbulence applies universal similarity theories of turbulence and turbulent mixing to the vertical evolution of an isolated patch of turbulence in a stratified fluid as its growth is constrained and fossilized by buoyancy forces. Quantitative hydrodynamic-phase-diagrams (HPDs) from the theory are used to classify microstructure patches according to their hydrodynamic states. When analyzed in HPD space, previously published oceanic datasets showed their dominant microstructure patches are fossilized at large scales in all layers. Laboratory and field measurements suggested phytoplankton species with different swimming abilities adjust their growth strategies by pattern recognition of tur-bulence-fossil-turbulence dissipation and persistence times that predict survival-relevant surface layer sea changes. New data collected near a Honolulu waste-water outfall showed the small-to-large evolution of oceanic turbulence microstructure from active to fossil states, and revealed the ability of fossil-density-turbulence patches to absorb, and vertically radiate, internal wave energy, information, and enhanced turbulent-mixing-rates toward the sea surface so that the submerged waste-field could be detected from a space satellite (Bondur and Filatov, 2003). 相似文献
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Bertrand's law that the plant can't live in lack of some indispensable element, appropriate amount of the element will make the plant thrive but excessive amount of it will make the plant poisoning and even die was obtained through the study on the biologic adaptability in laboratory for the indispensable element manganese by G. Bertrand. E. D. Weinberg developed Bertrand's law as that certain amount of manganese was appropriate for the growth of some bacteria but not for the form of bacteriophage.The double threshold contents of elements indispensable for the organisms and their physiological effects can be extended to different hydrogeochemical zones of hydrogeological unit. Some elements are lack in the hydrogeochemical zone, in which the elements leaching and transfer are very strong the biological physiological effect is negative to the elements content. However, in the elements enrichment area caused by leaching and concentrating by evaporation or environmental pollution, the biological physiological effects are positive to the element content. The elements content in other areas which are in between two above types is appropriate for the organisms.From the hydrogeochemical study in Liliu , Shanxi province we obtained that the rate of KBD, IDD and dental caries are resulted from deficiency of elements Se, I and F in water (soil), respectively, the rate of diseases above is inversely related with the element content, while in the zone with excessive fluorine caused by enrichment and leaching, the rate of endemic fluorosis is positive to the fluorine content. 相似文献