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1.
使用感量校正多测片再生(SMAR)法对新疆昆仑山北坡的12个黄土样品的细颗粒混合矿物和细颗粒石英进行了等效剂量(De)的测量.测试结果显示,该地区黄土的[ post-IR]OSL和OSL信号强度相对于黄土高原的样品偏低,初步认为与物源不同及粉尘堆积和堆积后经受的风化作用微弱有关.细颗粒混合矿物的IRSL等效剂量值基本上小于其细颗粒石英OSL的,反映出长石存在明显的异常衰减现象;[post-IR] OSL信号主要来自于长石,用于测年需谨慎;细颗粒石英OSL更适合用于对该地区黄土的测年.  相似文献   

2.
使用感量校正多测片再生(SMAR)法对新疆昆仑山北坡的12个黄土样品的细颗粒混合矿物和细颗粒石英进行了等效剂量(De)的测量.测试结果显示,该地区黄土的[ post-IR]OSL和OSL信号强度相对于黄土高原的样品偏低,初步认为与物源不同及粉尘堆积和堆积后经受的风化作用微弱有关.细颗粒混合矿物的IRSL等效剂量值基本上...  相似文献   

3.
郑州邙山马兰黄土的光释光(OSL)测年初步研究   总被引：6，自引：1，他引：5  
对郑州市西北邙山黄土塬赵下峪(34°58'N,113°22'E)剖面上部马兰黄土(厚约87m)不同层位的24个样品作了细颗粒(4-11μm)组分红外释光(IRSL)测年,其中8个样品同时进行了细颗粒组分绿光释光(GLSL)测年。样品的IRSL和GLSL信号强度都在Daybreak1100TL/OSL检测系统中测量。该系统的本底计数为70-80光子/秒。被检测的IRSL和GLSL波长分别为340-480nm和340±25nm;激发光束波长分别为880±80nm和514±14nm,功率为18mW和15-16mW。所有样品的等效剂量都用再生释光法测定;环境剂量率是通过测定样品的铀、钍和钾含量,按Aitken(1985)的转换系数确定的,考虑了含水量的影响及宇宙射线的贡献。从这批样品的光释光测年结果可得以下初步认识:
(1)8个样品细颗粒组分的IRSL和GLSL测定的等效剂量和年龄值,除1个样品外,都在1-2σ范围内一致。这可能提供了沉积物光释光测年可靠性的一种自检方法。(2)邙山剖面马兰黄土不同层位段的沉积速率变化十分显著,从0.4m/ka到5.6m/ka,并与剖面上质量磁化率测定值的变化大致相吻合。该剖面马兰黄土至少有4个快速堆积层(沉积速率>3m/ka),其磁化率低而变化小;3个缓慢堆积层(沉积速率<0.5m/ka),其磁化率大或变化显著,它们之间有一系列过渡层。(3)邙山马兰黄土大体可三分即上部(L1-1)埋深2.7-27.5m,中部(L1-2)埋深27.5-57.9m)和下部(L1-3)埋深57.9-87.9m。它们的形成年代分别为10.8-36.2ka B P,36.2-70.3ka B P和70.3-80.2ka B P。较详细的黄土-古土壤序列年代表将在文中讨论   相似文献   

4.
使用钾长石进行释光测年时,由于长石的释光信号存在异常衰减,会导致沉积事件年龄的低估。对中国北方4个全新世样品分别使用石英和钾长石矿物组分释光测年,通过测量钾长石的衰退系数(g值)对钾长石使用再生剂量法获得的表征年龄进行了校正。发现对于本文所研究的年轻样品钾长石表征年龄与石英年龄相比系统偏小约2％～9％,钾长石校正年龄与石英年龄相比则严重偏大约16％～40％,表明使用g值无法校正年轻样品的钾长石年龄。对于年轻样品,钾长石IRSL信号异常衰减现象对测年结果的影响是可以忽略的。  相似文献   

5.
从湖南省北部赤山岛枫树嘴旧石器遗址剖面第2、第3和第4考古层位采集的3个沉积物样品中提取的细粒混合矿物,尝试对其红外释光(IRSL)信号进行研究。实验表明,虽然长石IRSL信号很弱,但仍可以测得信噪比足够高的红外激发后高温红外激发释光(post-IR IRSL)信号。与此同时,样品存在明显的红外激发后蓝光释光(post-IR OSL)信号,并且样品的IRSL与post-IR OSL信号均以快组分为主,这为该地区沉积物利用长石光释光信号定年提供了新的可能。鉴于长石IRSL信号较弱,根据剂量恢复实验结果,本研究采用post-IR IRSL SAR法(50℃红外激发后270℃高温红外激发,pIRIR270℃)进行等效剂量测量,同时也应用post-IR OSL SAR法定年进行比较。实验结果表明,细粒混合矿物的pIRIR270℃等效剂量分别为418.8±13.2 Gy、562.3±18.2 Gy和694.8±17.9 Gy,相对应的post-IR OSL SAR等效剂量结果为345.0±29.4 Gy、409.6±33.7 Gy和424.7±32.2 Gy。假设强烈化学风化未对沉积物的剂量率造成很大影响,基于长石pIRIR270℃信号的释光年龄为89±6 ka、118±8 ka和152±9 ka,比前人所得的石英OSL SAR法年龄老30%~55%(约20~55 ka)。通过对比不同测量条件下获得的等效剂量值来评估长石IRSL信号是否存在晒退问题,没有发现长石post-IR IRSL信号存在晒退不完全的证据。根据本研究post-IR IRSL SAR法测年结果,赤山岛枫树嘴旧石器遗址似阿舍利技术类型的石器出现在倒数第二次冰期(MIS 6)后期至末次间冰期(MIS 5)前期,比湖南道县福岩洞现代人类牙齿化石年龄(80~120 ka)稍老。作为似阿舍利技术石器制造者的赤山岛古人与福岩洞现代人的关系将是我国旧石器时代考古学和古人类学研究的一个重要课题。  相似文献   

6.
黄土高原马兰黄土粘土矿物的定量研究   总被引：4，自引：0，他引：4  
张永双  曲永新 《地质论评》2004,50(5):530-537
本文在回顾和总结中国西北黄土粘土矿物研究进展的基础上,提供了采用现代X-射线衍射(XRD)定量测试技术(包括粘土矿物样品处理和全自动数据处理技术)对陕北晋西12个县市马兰黄土粘土矿物定量研究的最新结果。测试结果表明,马兰黄土的主要粘土矿物为伊利石／蒙脱石混层矿物(相对含量为60％～70％),而不是以往所认为的伊利石。伊利石在黄土中主要呈两种形式存在,即单矿物伊利石和伊／蒙混层矿物中的伊利石。研究还发现,各地马兰黄土粘土矿物组成变化不大,但在神木、河曲、偏关一带伊／蒙混层比有局部增高的现象。根据扫描电子显微镜观察,黄土中粘土矿物不是以单粒形式存在,而主要是以集粒粘附物的形式包裹在碎屑颗粒表面。黄土中粘土矿物组成及其存在形式一方面可以充分揭示黄土物源区的表生化学环境特征;另一方面,伊／蒙混层矿物作为一种广泛分布的膨胀性粘土矿物和它在黄土粘土矿物中所占地位,对于认识马兰黄土在水作用下的湿陷变形和强度衰减的本质具有重要意义。  相似文献   

7.
一、前言 二十年代末以来,许多学者曾对马兰黄土进行过研究。岩石、古生物地层证据表明,马兰黄土系晚更新世的风成堆积。但迄今没有提出过可靠的年龄数据。本文采用热释光法测定了甘肃境内马兰黄土底部年龄,目的是了解不同地点马兰黄土堆积的起始年龄。  相似文献   

8.
新疆黄土岩石磁学特征与地层性质的对应关系具有鲜明的区域特征.本文选取沙湾黄土剖面进行较为系统的岩石磁学分析.研究结果表明,沙湾剖面的磁性矿物组成与黄土高原及新疆北部其他黄土剖面相似,以亚铁磁性矿物(如磁铁矿、磁赤铁矿)为主要的载磁矿物,同时含有一定量的不完全反铁磁性矿物(如赤铁矿、针铁矿)和顺磁性矿物.假单畴(PSD)和多畴(MD)为样品的主要磁畴特征,部分土壤样品中磁性矿物磁畴状态表现为单畴(SD).进一步分析发现,磁化率与地层对应关系较为复杂,剖面3m以上地层中的磁化率及其他相关磁学参数与成壤强度呈现正相关关系,全新世以来发育的古土壤中磁化率值较高,细颗粒磁性矿物含量也较高;而3m之下地层中磁学参数显著表现为风力强度驱动变化模式.古风场强度的变化可能对剖面整体磁学性质具有一定的影响,成壤作用受到风动力条件的制约,主要决定了较细颗粒磁性矿物的含量变化.xARM/SIRM参数与磁化率相比对地层成壤强度的指示作用更为明显.  相似文献   

9.
使用SEM、EDS、IR、XRD等仪器,分析了马兰黄土的物化组成、表面结构及表面位浓度和阳离子交换容量等特征,并利用这些数据建立了马兰黄土-Cr(Ⅲ)的水岩相互作用模型及变初始浓度、去碳酸岩盐以及形态提取实验。通过对比模拟结果与实验结果,验证模型的可靠性,并初步获取了马兰黄土与水溶液中Cr(Ⅲ)作用过程中所发生的相关反应及其强度。结果显示,在实验浓度(1～100mg/L)范围内,该模型能够很好地描述马兰黄土与水中Cr(Ⅲ)的反应过程,其模型精度达90%。本成果将进一步丰富马兰黄土与Cr(Ⅲ)水岩相互作用的机理研究。  相似文献   

10.
赵华  卢演俦  张金起  王宏 《地质科学》2002,37(2):174-183
对天津大直沽ZH2钻孔晚第四纪沉积物岩芯12个样品的红外释光(IRSL)测年及沉积物记录的环境变化研究结果表明:1)细颗粒(4～11μm)多测片的红外释光(IRSL)技术对水悬浮沉积物的年龄测定有着巨大的潜力,渤海湾西岸全新世环境变化的IRSL年代可与14C年代相对比;2)大直沽ZH2孔所在地未见晚更新世海侵,并在距今约30 ka至约10 ka期间处于沉积间断状态,距今9.5 ka开始发生海侵,距今5.1 ka发生海退,距今4.4 ka海水已退出ZH2孔所在地,距今2 ka左右已有人类活动.  相似文献   

11.
Optically stimulated luminescence (OSL) dating of polymineral fine-grained loess samples collected from the southern Loess Plateau of China was conducted using the single-aliquot regenerative-dose (SAR) protocol. A ‘Double-SAR’ procedure in which aliquots are subjected to both infrared (IR) and blue stimulations was used, and two sets of equivalent dose (D e ) determinations were produced. These doses are assumed to be predominantly related to the feldspathic and quartz fine grain populations, respectively. The results revealed that the OSL ages estimated by infrared stimulated luminescence (IRSL) signals and those estimated by [post-IR] stimulated luminescence ([post-IR] OSL) signals disagreed. Specifically, the ages estimated using the IRSL signals were smaller than those estimated using [post-IR] OSL signals. The results of an anomalous fading test of the two types of OSL signals revealed that the [post-IR] OSL signals from the etched sub-sample (by H2SiF6 and HF) and the un-etched sub-sample did not fade significantly. However, the IRSL signals from the un-etched sub-sample showed obvious signs of fading. These findings indicate that the lower age estimated by IRSL is due to the anomalous fading of feldspar IR signals in the polymineral fine grains. For samples collected from greater than 100 cm, the estimates of their OSL ages using two types of luminescence signals generally agreed with their pre-estimated ages, especially those of the [post-IR] OSL signals. However, for the three samples that were collected from a depth of less than 100 cm, their OSL ages were remarkably underestimated, possibly due to the enhanced human activity (such as soil cultivation) that has occurred in the region since 3000 a B.P.  相似文献   

12.
Buylaert, J.‐P., Huot, S., Murray, A.S. & Van den haute, P.: Infrared stimulated luminescence dating of an Eemian (MIS 5e) site in Denmark using K‐feldspar. Boreas, 10.1111/j.1502‐3885.2010.00156.x. ISSN 0300‐9483. Infrared stimulated luminescence (IRSL) dating of K‐feldspars may be an alternative to quartz optically stimulated luminescence (OSL) dating when the quartz OSL signal is too close to saturation or when the quartz luminescence characteristics are unsuitable. In this paper, Eemian (MIS 5e) coastal marine sands exposed in a cliff section on the coast of southern Jutland (Denmark) are used to test the accuracy and precision of IRSL dating using K‐feldspars. This material has been used previously to test quartz OSL dating ( Murray & Funder 2003 ): a small systematic underestimation of <10% compared to the expected age of ～130 ka was reported. In our study, a single‐aliquot regenerative‐dose (SAR) IRSL protocol is used to determine values of equivalent dose (De) and the corresponding fading rates (g values). A significant age underestimation (of up to ～35%) is observed; this is attributed to anomalous fading. Using a single site‐average fading rate of 3.66 ± 0.09%/decade to correct the IRSL ages for all samples provides good agreement between the average fading‐corrected K‐feldspar age (119 ± 6 ka) and the independent age control (132–125 ka). This is despite the reservations of Huntley & Lamothe (2001) that their fading correction method is not expected to work on samples older than ～20–50 ka. This fading‐corrected feldspar result is not significantly different from the overall revised quartz age (114 ± 7 ka) also presented here. We conclude that fading‐corrected IRSL ages measured using K‐feldspar may be both precise and accurate over a greater age range than might be otherwise expected.  相似文献   

13.
天山乌鲁木齐河源末次冰期冰川沉积光释光测年   总被引：6，自引：5，他引：1  
乌鲁木齐河源地区是中国冰川遗迹保存最丰富、地貌最典型的区域之一,是根据冰川遗迹重建第四纪冰川历史的理想地区。大量的研究工作以及技术测年结果也使其成为试验冰川沉积光释光（optically stimulated luminescence,OSL）测年可行性的理想地点。共采集了6个冰碛及上覆黄土样品用于光释光测年。提取38~63 μm的石英颗粒,运用SAR-SGC法测试等效剂量。各种检验表明测试程序是适用的。通过地貌地层关系、重复样品、已有年代的对比等方法,检验该地冰川沉积OSL测年的可行性。结果表明,OSL年代结果与地貌地层新老关系非常吻合,与已有的其他测年技术的年代结果也具可比性,表明这些样品的OSL信号在沉积之前晒退较好,OSL年代是可信的。冰川观测站侧碛垄的OSL年代为14.8±1.2 ka;9号冰川支谷口附近冰碛的OSL年代为13.5±1.1 ka和17.2±1.3 ka;上望峰冰碛的OSL年代为20.1±1.6 ka。综合OSL年代结果与此前其他测年结果,这几套冰碛垄形成于深海氧同位素MIS 2阶段应该是比较统一的认识。上望峰冰碛上覆黄土的OSL年代（10.5±0.8 ka）也印证了该结论。OSL年代指示上望峰冰碛对应于末次冰期最盛期,冰川观测站和9号冰川支谷谷口冰碛对应于晚冰期。下望峰冰碛的OSL年代为36.3±2.8 ka,对应于MIS 3阶段。下望峰冰碛的形成时代,仍有待更多沉积学以及测年工作进一步确定。  相似文献   

14.
《Quaternary Science Reviews》2003,22(10-13):1131-1138
In this investigation we evaluate several proposed optically stimulated luminescence single-aliquot regeneration (OSL SAR) procedures to determine which technique has the greatest potential to yield accurate ages for samples collected from tuff-derived alluvial sediments within the narrow, sharply incised canyon systems of the Pajarito Plateau of northern New Mexico. The SAR data collection methods evaluated are: infrared-stimulated luminescence (IRSL), post-IR blue-OSL, IRSL with TL annealing cycles on polymineral fine-grains, and blue-OSL on quartz fine sand. A single-grain laser luminescence (SGLL) procedure for quartz sand is also evaluated. Age estimates obtained from these methods are compared with radiocarbon, soil PDI (profile development index), and IRSL multi-aliquot additive dose (MAAD) age constraints. Our results indicate that the modal De of quartz sand SGLL dose distributions yield ages that are consistent with radiocarbon and PDI age constraints for the tuff derived sediments in this investigation and appears to be the most promising method for studies in this area. Additionally, two fine-grained polymineral methods, IRSL SAR and traditional IRSL MAAD, produced ages that were generally in agreement with the SGLL ages and with available 14C and PDI age constraints. At the present stage of research, we advocate using quartz sand SGLL in conjunction with IRSL SAR or even IRSL MAAD for polymineral fine-grains to provide the most robust and reliable luminescence age data sets for tuff-derived sediments.  相似文献   

15.
The loess–palaeosol sequence of Batajnica (Vojvodina region, Serbia) is considered as one of the most complete and thickest terrestrial palaeoclimate archives for the Middle and Late Pleistocene. In order to achieve a numerical chronology for this profile, four sets of ages were obtained on 18 individual samples. Equivalent doses were determined using the SAR protocol on fine (4–11 μm) and coarse (63–90 μm) quartz fractions, as well as on polymineral fine grains by using two elevated temperature infrared stimulation methods, pIRIR290 and pIRIR225. We show that the upper age limit of coarse quartz OSL and polymineral pIRIR290 and pIRIR225 techniques is restricted to the Last Glacial/Interglacial cycle due to the field saturation of the natural signals. Luminescence ages on coarse quartz, pIRIR225 and pIRIR290 polymineral fine grains are in general agreement. Fine quartz ages are systematically lower than the coarse quartz and pIRIR ages, the degree of underestimation increasing with age. Comparison between natural and laboratory dose response curves indicate the age range over which each protocol provides reliable ages. For fine and coarse quartz, the natural and laboratory dose response curves overlap up to ~150 and ~250 Gy, respectively, suggesting that the SAR protocol provides reliable ages up to c. 50 ka on fine quartz and c. 100 ka on coarse quartz. Using the pIRIR225 and pIRIR290 protocols, equivalent doses up to ~400 Gy can be determined, beyond which in the case of the former the natural dose response curve slightly overestimates the laboratory dose response curve. Our results suggest that the choice of the mineral and luminescence technique to be used for dating loess sediments should take into consideration the reported limited reliability.  相似文献   

16.
Despite numerous palaeoenvironmental investigations of loess–palaeosol sequences across the Carpathian Basin, well-dated high-resolution records are scarce. This paper presents a new high-resolution chronology for the loess-palaeosol sequence at Surduk (Serbia), based on optically stimulated luminescence (quartz) and post-infrared infrared stimulated luminescence (polymineral) dating. The presented record spans 53–19 ka, with primary loess deposition occurring after 52±2 ka, and differs from previously published chronologies that relied on less precise and now superseded dating protocols. Based on the new chronology, mass accumulation rates (MARs) for Surduk were constructed and compared with sites in the Carpathian Basin. The results demonstrate that accumulation periods across this area are not consistent in timing or rates. The high-resolution dating strategy identifies a disturbance in sediment deposition that occurred after 45±2 ka and implies that site contains a hiatus. Finally, we show samples that failed routine dose recovery and preheat plateau tests, and had low fast ratios. Supported by bulk sample geochemical analysis it is proposed that a potential abrupt source shift, during the Last Glacial Maximum, may be the cause of the anomalous luminescence behaviour.  相似文献   

17.
We tested the suitability of the fine‐grained quartz (4–11 μm) Optical Stimulated Luminescence (OSL) and thermally‐transferred OSL (TT‐OSL), and the fine‐grained polymineral (4–11 μm) post‐infrared IRSL (post‐IR IRSL or pIRIR) signals for dating samples from aeolian‐lacustrine deposits from the Xiaochangliang archaeological profile in the Nihewan Basin, China; these deposits include material from the Jaramillo subchron (c. 1.0 Ma). In the upper aeolian section, the OSL and pIRIR290 ages are consistent with each other, and show that the upper 8.8 m was deposited between c. 0.3 and c. 140 ka. The luminescence ages indicate a major discontinuity in deposition between the aeolian and the older lacustrine deposits. Below this hiatus at 9.4 m (i.e. in the lacustrine sediments) all three signals are found to be in field saturation (no further systematic increase in burial dose with depth) despite the TT‐OSL signal (apparent mean burial dose ~880 Gy) being well below saturation on the laboratory growth curve. This is in contrast to the pIRIR290 signal, which saturates in the field at a level consistent with laboratory saturation. This results in a practical upper limit to the measured burial dose of ~900 Gy (2D0). Thus for the TT‐OSL and pIRIR290 signals, the upper limits for dating lacustrine deposits are <260 ka and c. 240 ka, respectively. These results have major implications for the appropriate future application of these signals. The ages of our lacustrine samples cannot be regarded as necessarily accurate ones; nevertheless, these ages provide the first long series absolute chronology for study of local palaeolithic and geomorphic evolution history aside from the magnetostratigraphical results available before this research.  相似文献   

18.
The continuing development of analytical methods for investigating sedimentary records calls for iterative re-examination of existing data sets obtained on loess-palaeosol sequences (LPS) as archives of palaeoenvironmental change. Here, we re-investigate two LPS (Hecklingen, Zilly) in the northern Harz foreland, Germany, being of interest due to their proximity to the Scandinavian Ice Sheet (SIS) and the position between oceanic climatic influence further west and continental influence towards the east. First, we established new quartz OSL and polymineral IRSL chronologies. Both methods show concordant ages in the upper part of the Hecklingen profile (~20–40 ka), but in the lower part IRSL underestimates OSL ages by up to ~15 ka for the period 40–60 ka. Interpretations hence refer to the OSL data set. Second, we applied Bayesian age-depth modelling to data sets from Hecklingen to resolve inversions in the original ages, also reducing averaged 1σ uncertainty by ~19% (OSL) and ~12% (IRSL). Modelled chronologies point out phases of increased (MIS 2, early MIS 3) and reduced (middle and late MIS 3) sedimentation, but interpretation of numerical rates is problematic because of intense erosion and slope wash particularly during MIS 3. Finally, previously obtained grain-size data were re-investigated by end member modelling analyses. Three fundamental grain-size distributions (loadings) explain the measured data sets and offer information on intensity and – combined with modelled OSL ages – timing of geomorphic processes. We interpret the loadings to represent (i) primary loess accumulation, (ii) postdepositional pedogenesis and/or input of aeolian fine fractions, and (iii) input of coarse aeolian material and/or slope wash. The applied modelling tools facilitate detailed understanding of site-formation through time, allowing us to correlate a strong peak in mean grain size at ~26–24 ka to the maximum extent of the SIS and increased influence of easterly winds.  相似文献   

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