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1.
The acquisition of a gyroremanent magnetization (GRM) by single-domain (SD) greigite particles during alternating-field (AF) demagnetization is demonstrated. Previous palaeomagnetic studies failed to identify the presence of authigenic greigite in the glacio-marine clays studied. These clays formed the subject of an earlier debate about the validity of a Late Weichselian geomagnetic excursion (the Gothenburg Flip) in southern Sweden. The greigite carries a stable chemical remanent magnetization (CRM), which coexists with a detrital remanent magnetization (DRM) carried by magnetite. AF demagnetization could not isolate the primary remanence in the sediments where magnetite and greigite coexist, due to the overlapping coercivity spectra of the two minerals and the inability to determine the time lag between sediment deposition and CRM formation. Thermal demagnetization removed the CRM at temperatures below 400 C, but this method was hindered by the unconsolidated nature of the sediments and the formation of secondary magnetic minerals at higher temperatures. The results suggest that the low-coercivity DRM carried by magnetite was mistaken for a 'viscous' component in the earlier studies. Hence the former debate about the record of the Gothenburg Flip may have been based on erroneous palaeomagnetic interpretations or non-reproducible results. AF demagnetization procedures applied to samples suspected of bearing SD magnetic particles (such as greigite) should be carefully selected to recognize and account for GRM acquisition.  相似文献   

2.
Summary. Using natural volcanic rocks which acquired thermoremanence (TRM) in known fields, reliability of various palaeointensity methods using alternating field (AF) demagnetization were evaluated. Natural remanence (NRM), TRM and anhysteretic remanences (ARM's) before and after heating were stepwisely AF demagnetized following Shaw's method.
It was found that the coercivity spectra of TRM and ARM in these samples are very similar, and that even when changes occurred during heating, the changes for two remanences are quite similar in many samples. Therefore, Shaw's method of palaeointensity determination, which incorporates ARM checks to the conventional comparison of NRM and TRM coercivity spectra, gives results as reliable as those obtained by the Thellier method. Many examples were demonstrated in which TRM and ARM intensities changed substantially by heating, but without changes in the shape of their coercivity spectra. Such changes cannot normally be detected and erroneous palaeointensities with apparent internal consistency would be obtained by usual AF demagnetization methods.
Although ARM is quite similar to TRM, the rate of acquisition of ARM and TRM in weak fields varies by a factor of five among the present samples. To determine palaeointensities from the linear relation between ARM and TRM, it is necessary to determine experimentally the relative acquisition rate of these remanences. Therefore, methods based only on NRM-ARM relations would not give palaeointensities with acceptable errors.  相似文献   

3.
The intensity of rotational remanent magnetization (RRM) acquired by single-domain greigite at a rotation frequency of 5 rps was combined with measurements of anhysteretic remanent magnetization (ARM) to calculate the effective biasing field ( Bg ) that produced the RRM. Samples of single-domain greigite had Bg values between -137 and -84 μT, and a MDFRRM of c. 80 mT. By contrast, a suite of natural and synthetic ferrimagnetic iron oxide samples, including single-domain magnetite and y Fe3O4 tape particles, acquired Bg values between -3 and -14 μT, and MDFRRM ranged between 43 and 68 mT (when RRM was acquired). Multidomain magnetite did not acquire a RRM. Bg values at 5 rps were calculated from previously published data for magnetite particles of different grain sizes, which revealed a minimum Bg value of -24 μT and a MDFRRM of 57 mT for the finest fraction (0.2-0.8 μm in diameter). In a geological example, measurements of Bg and MDFRRM were used to detect the presence of greigite in a 4 m long Late Weichselian sediment core. Variations in inclination, declination and the intensity of the natural remanent magnetization (NRM) correlate with changes in magnetic mineralogy.  相似文献   

4.
The magnetic behaviour of hydrothermally synthesized greigite was analysed in the temperature range from 4 K to 700 °C. Below room temperature, hysteresis parameters were determined as a function of temperature, with emphasis on the temperature range below 50 K. Saturation magnetization and initial susceptibility were studied above room temperature, along with X-ray diffraction analysis of material heated to various temperatures. The magnetic behaviour of synthetic greigite on heating is determined by chemical alteration rather than by magnetic unblocking. Heating in air yields more discriminative behaviour than heating in argon. When heated in air, the amount of oxygen available for reaction with greigite determines the products and magnetic behaviour. In systems open to contact with air, haematite is the final reaction product. When the contact with air is restricted, magnetite is the final reaction product. When air is excluded, pyrrhotite and magnetite are the final reaction products; the amount of magnetite formed is determined by the purity of the starting greigite and the degree of its surficial oxidation. The saturation magnetization of synthetic greigite is virtually independent of temperature from room temperature down to 4 K. The saturation remanent magnetization increases slowly by 20–30 per cent on cooling from room temperature to 4 K. A broad maximum is observed at ~10 K which may be diagnostic of greigite. The coercive and remanent coercive force both increase smoothly with decreasing temperature to 4 K. The coercive force increases from ~50 mT at room temperature to approximately 100–120 mT at 4 K, and the remanent coercive force increases from approximately 50–80 mT at room temperature to approximately 110–180 mT at 4 K.  相似文献   

5.
Repeated laboratory-induced weak mechanical shocking ( c .  0.57  kg  m  s−1 ) of marine sandstone samples showing drilling-induced remanence, from commercial bore cores from the North Sea and Prudhoe Bay, causes increases in their low-field susceptibility ( χ ) and their ability to acquire an isothermal remanent magnetization (IRM). These enhancements are reduced by some 20 per cent by AF demagnetization in 100  mT. Doubling the intensity of the shock doubles the susceptibilities and IRMs acquired. The susceptibility increase ceases after 300 to 400 shocks for the North Sea samples and 20 to 30 shocks for those from Prudhoe Bay, while the IRM saturates after 800–1000 and 30–50 shocks respectively. Continental, haematite-bearing sandstones from commercial bore cores with no drilling-induced remanence subjected to the same shocks do not show these effects. Differences in the magnetic mineralogy of shocked and unshocked marine samples suggest that the magnetic enhancement is predominantly due to the creation of pyrrhotite by shock-induced irreversible crystallographic changes in iron-bearing sulphides. When shocked during commercial drilling, these new ferromagnetic minerals acquire strong chemical (crystalline) remanences, associated with a wide spectrum of grain sizes, in the magnetic field of the drill string, and these are resistant to both thermal and AF demagnetization. Similar processes are likely in any situation involving the shock of physically metastable iron-bearing minerals, particularly anoxic sediments. A 5  cm non-magnetic collar between the drill stem and crown should drastically reduce the magnetic intensity of this effect under commercial conditions, but would not prevent its occurrence.  相似文献   

6.
Summary. In palaeomagnetic studies of volcanic rocks it is often considered that, if the direction of NRM does not change much and the intensity de-creases gradually and smoothly during ac cleaning, then the remanent magnetization is stable and chiefly composed of TRM. This argument is extended as a consistency check to detect unwanted effects during laboratory heating. A simple procedure which employs orientated samples and a short heating (15 min) for TRM acquisition in the laboratory has been used for determining the ancient geomagnetic field intensity using seven volcanic rocks of Late Cenozoic age from central Mexico. The main reliability tests are based on the stability of direction, the close correspondence of the entire coercitivity spectra of both NRM and TRM to ac demagnetization, the low scatter of TRM directions, close correspondence of the TRM directions and the direction of the laboratory magnetic field, proportionality of TRM intensities to applied field, susceptibility comparison before and after heating, and the within-unit consistency of palaeointensity determinations.  相似文献   

7.
Magnetic remanence acquisition in Finnish lake sediments   总被引：2，自引：0，他引：2  
Summary. Magnetic studies have been carried out on organic sediments from five Finnish lakes to determine the carrier(s) of the stable NRM and to find how the remanence is acquired. Single or pseudo-single domain 'magnetite' is thought to carry the NRM. It was found that drying and cooling sediment samples resulted in a loss of NRM which was attributed to the misalignment of small magnetic particles. Low-field experiments were carried out on sediment samples in different physical states and from the results of these investigations it was concluded that post-depositional processes are important in the acquisition of an NRM. Stabilization of magnetic grains is thought to be due to the growth of gels in the organic sediment rather than to dewatering.  相似文献   

8.
In this paper, the mechanisms of low-temperature demagnetization of remanence in multidomain magnetite are considered. New experimental observations of the behaviour of the saturation isothermal remanence, thermoremanence and partial thermoremanence at low temperatures are presented. The results show that there are two main contributions to this low-temperature demagnetization. The first and predominant contribution (type-1 demagnetization) is due to 'kinematic' domain state reorganization and occurs throughout cooling from room temperature to the Verwey transition, T v , at 120–124  K. The second contribution arises from the change in anisotropy from cubic to monoclinic at T v , which changes the overall domain structure of the grain. On warming in zero field, some domain walls will not return to their original positions but will take up a position that leads to a lower net remanence (type-2 demagnetization). In stoichiometric magnetite, demagnetization does not occur at 130  K at the isotropic point, T k , contrary to some previous predictions. In non-stoichiometric magnetite, the influence of the Verwey transition is greatly reduced, and anomalous behaviour is observed at T k .  相似文献   

9.
Summary. This study covers detailed thermal, chemical and alternating field demagnetization from 50 sites distributed through all units of the Longmyndian sedimentary succession (with the exception of the Stretton Shales), and eight sites in the tuff bands comprising the Batch Volcanics. The resultant effect of treatment is to remove a low blocking temperature steep component and isolate a coherent remanence direction D = 116°, I = 76° the total NRM is composite and not an adequate indicator of the palaeofield. Chemical demagnetization indicates that both hematite and magnetite grains contribute to this component and these two phases are magnetized in the same direction. A negative fold test shows that this remanence was acquired during or after the Longmyndian folding. Formation of the major magnetic constituent, authigenic magnetite, is linked to dewatering during rapid uplift following the folding which is dated by both the Rb–Sr and fission track methods at c . 525 Ma. The study defines a palaeopole of this age remote from the later APW path for Britain and links the Late Precambrian–Lower Cambrian path defmed from basement rocks of England and Wales with the Ordovician and younger results. Palaeomagnetic results from tuff bands within the sediments and Lower Silurian age intrusions cutting the outcrop are also reported.  相似文献   

10.
A newly developed field distribution measuring system based on a high- T c SQUID has been employed in the study of magnetic mineral distribution in several Permian sedimentary rocks. The instrument consists of a small, 1.4×1.4 mm sized YBaCu-oxide SQUID magnetic field sensor that is operated in a thin-walled dewar, so that the sample's surface, at room temperature, can be scanned at a distance of only ∼1.5 mm. The samples were subjected to a saturation remanence perpendicular to the surface and the scanning measurements in zero field reveal that the magnetization might be carried by only a small part of a sample, in one case associated with secondary oxide phases. High-resolution magnetic scans can aid in the interpretation of the magnetic remanence acquisition process.  相似文献   

11.
Summary. A theoretical investigation of the way in which an isotropic rock containing single-domain particles acquires both IRM and ARM (or TRM) has indicated that stationary single-axis alternating field (af) demagnetization with the af axis at an angle to the remanence vector should produce progressive angular changes in a single-component remanence as demagnetization proceeds. Just before the remanence is completely removed it should lie at 90° to the af axis irrespective of the original orientation of the remanence (apart from 0°). Experimental observations on a rock sample support these deductions.
This analysis has been extended to investigate the way in which ARM (or TRM) and IRM are demagnetized by static three-axis demagnetization methods which are used by some workers in palaeomagnetism. Theory, in conjunction with the use of a numerical model, predicts that an ARM or TRM should not undergo significant direction changes when these methods are applied but an IRM should undergo progressive direction changes as demagnetization proceeds, usually moving until it makes an angle of cos−1 (1/3) with each of the three af axes just before it is removed. Confirmation that such changes do occur have been obtained by experiments on a rock sample. The relative merits of static and tumbling af demagnetization methods are also discussed.  相似文献   

12.
The palaeomagnetic standard technique of stepwise thermal demagnetization (STD), long regarded as unreliable for oceanic basalts that have undergone low temperature alteration, has recently been applied in a number of studies to characterize the natural remanent magnetization (NRM) of such rocks. In order to better understand STD data of oceanic basalts, and to possibly identify the magnetominerals that are carrying the NRM, we have carried out a number of continuous and STD experiments on seven oceanic basalt samples. During continuous thermal demagnetization (CTD), a sample is heated to a certain temperature and its NRM is measured during heating and subsequent cooling. Even when CTD reveals only titanomaghemite unblocking at 400°C as the remanence carrier, STD behaviour can be very complex and unblocking is observed at temperatures of up to 500°C and higher. CTD also allowed to identify a partial or full self-reversal of NRM due to interaction between two types of magnetominerals in one sample. The higher degree of maghemitization of smaller titanomaghemite grains with respect to larger ones, which are less efficient in carrying the remanence, was seen for three samples by a shift of 80°C between the strong field thermomagnetic curve and the NRM measured at elevated temperature. In several cases, the identification of the NRM-carrying magnetomineral was not possible from CTD data due to the ambiguity of Curie temperatures in the titanomagnetite/titanomaghemite system.  相似文献   

13.
In the pseudo-Thellier method for relative palaeointensity determinations (Tauxe et al. 1995) the slope of the NRM intensity left after AF demagnetization versus ARM intensity gained at the same peak field is used as a palaeointensity measure. We tested this method on a marine core from the Azores, spanning the last 276  kyr. We compared the pseudo-Thellier palaeointensity record with the conventional record obtained earlier by Lehman et al . (1996 ), who normalized NRM by SIRM. The two records show similar features: intensity lows with deviating palaeomagnetic directions at 40–45  ka and at 180–190  ka. The first interval is associated with the Laschamps excursion, while the 180–190  ka low represents the Iceland Basin excursion (Channell et al. 1997). The pseudo-Thellier method, in combination with a jackknife resampling scheme, provides error estimates on the palaeointensity.
  Spectral analysis of the rock magnetic parameters and the palaeointensity estimates shows orbitally forced periods, particularly 23  kyr for climatic precession. This suggests that palaeointensity is still slightly contaminated by climate. Fuzzy c -means cluster analysis of rock magnetic and geochemical parameters yields a seven-cluster model of predominantly calcareous clusters and detrital clusters. The clusters show a strong correlation with climate, for example samples from detrital clusters predominantly appear during rapid warming. Although both the pseudo-Thellier palaeointensity m a and fuzzy clusters show climatic influences, we have not been able to find an unambiguous connection between the clusters and m a .  相似文献   

14.
Summary. The Breggia gorge (Ticino, Switzerland) provides a continuous outcrop of Mesozoic limestones covering the time between the Lower Jurassic and Upper Cretaceous. The Jurassic section from the Lower Pliens-bachian to Aalenian is well dated by ammonites. The limestones of these stages are a good quality recorder of the polarity of the geomagnetic field during this time interval. More than 500 cores have been drilled along a 120 m thick section with a median distance between cores of about 20 cm. Detailed thermal and af demagnetization and further rock magnetic studies were used to determine the characteristic NRM direction for each sample. Initial NRM intensities and low field susceptibilities reflect variations in oxidation potential and sedimentation rate during carbonate deposition. The Breggia section covers an estimated 12Myr of Lower to Middle Jurassic time during which more than 60 distinct reversals of the geomagnetic field are recorded. This corresponds to a comparatively high mean reversal frequency of about 5 reversals Myr−1. The Breggia polarity zonation can be correlated with the nearby section at Alpe Turati (Como, Italy) and comparable polarity patterns are recognized in other biostratigraphically well-dated magnetostratigraphic profiles from Hungary and Umbria (Italy).  相似文献   

15.
The remanent magnetic properties of an 88  m bore core are unrelated to either the dolomite content or the sedimentological textures and are considered to be carried primarily by biogenetic magnetite that was cemented in during very early diagenesis. Individual readings represent time intervals of c . 720 ± 32  yr and, after 40  mT partial demagnetization, they provide an almost continuous record of averaged geomagnetic secular variations over a period of some 3.17  Myr. The magnitude of directional secular variation is twice that of the present day, despite being smoothed, and the secular variations appear to grade into polarity transitions, suggesting no difference in their mechanisms. The rates of change in direction between subjacent levels in the core have a log-normal distribution which extends smoothly beyond 90° and has a median value of 13°/700  yr, the same as for unsmoothed European secular variation during the last 2000  yr. The intensity of remanence, after 40  mT partial demagnetization, appears to provide a reasonable approximation to geomagnetic field intensity. This tends to be weaker when the direction is moving faster, reflecting averaging, but is unrelated to the distance of the vector from the mean direction; that is, it depends on the rate of change and not on the virtual pole latitude. The virtual poles, after correction for tectonic rotations about horizontal and vertical axes, have latitudes that form a strongly platykurtic Fisherian distribution, while their longitudes have a circular distribution on which are superimposed two Gaussian peaks, 180° apart. This bore core thus provides detailed information of smoothed geomagnetic secular variation in the Lower Cretaceous (127 ± 3  Ma) which shows clear regularities in behaviour, some related to changes in the Earth's orbital parameters.  相似文献   

16.
Summary. After thermal and alternating field (AF) cleaning, the characteristic high blocking temperature A component of natural remanent magnetization (NRM) of the Tudor gabbro of southern Ontario has a mean direction D = 326°, I =–46° ( k = 132, α95= 4.8°, N = 8 sites). The corresponding palaeopole, 133°E, 12°N ( dp = 4°, dm = 6°), confirms the palaeopole 137°E, 17°N (α95= 8.4°) reported earlier by Palmer & Carmichael, based on AF cleaning only. The A NRM has unblocking temperatures > 515–525°C which exceed the estimated 500°C peak temperature reached locally during ∼ 1050 Ma Grenvillian regional metamorphism. The A NRM therefore predates metamorphism and is probably a primary thermoremanence (TRM). The age of the Tudor NRM has previously been taken to be about 675 Ma, but recent 40Ar/39Ar dating by Baksi has shown that this is the time of post-metamorphic cooling to 200–250°C. Hornblendes record initial cooling of the intrusion to 590±20°C at 1110 Ma and this is the best estimate of the age of the A remanence. Successful Thellier-type palaeointensity determinations on 11 Tudor samples confirm that the A NRM is a TRM and indicate a palaeofield at this time of 18–27 μT, about 50–70 per cent of the present field intensity at 27° magnetic latitude. The anomalous Tudor A palaeopole, which lies well to the west of both 1000–800 Ma Grenvillian palaeopoles and 1100–1050 Ma poles from Interior Laurentia, is interpreted as recording divergence between Grenvillia and Interior Laurentia just before the Grenvillian orogeny, rather than a post-metamorphic extension of the apparent polar wander path as previously assumed.  相似文献   

17.
Calcite and sedimentary fills in fractures cutting the Upper Devonian carbonates in the Holy Cross Mountains (HCM) were dated palaeomagnetically by comparison with the apparent polar wander path (APWP). Haematite-bearing calcite possessed well-defined components of natural remanent magnetization (NRM), which were preserved under thermal demagnetization to temperatures of approximately 500 °C, when specimens disintegrated. Although not completely demagnetized, some specimens revealed a stable NRM component before destruction, thus making a component analysis possible. Five components were determined using density point distribution and cluster analysis. One has a mean that is similar to the present-day local geomagnetic vector. The remaining four components yielded palaeomagnetic poles located at: A (70.3°S, 5.5°E), B (71.3°S, 31.2°E), C (48.7°S, 351.0°E, virtual geomagnetic pole), and D (11.6°S, 312.3°E). Antipodal polarities found in the fracture fills, together with dissimilarities in magnetization found in calcite and hosting carbonates, indicate the lack of simultaneous remagnetization, and different times of remanence acquisition for the rocks under comparison. Taking both palaeomagnetically inferred palaeolatitudes and regional tectonics into consideration, a Mesozoic (Cretaceous?) age is estimated for palaeopoles A and B, a Permian age for pole C, and a Carboniferous age for pole D. These age determinations are in line with the calcite ages estimated from isotopic studies. A comparative palaeomagnetic study performed on a well-dated Upper Devonian neptunian dyke of limestone and a Lower Triassic clastic vein yielded virtual geomagnetic poles (VGPs) close to the APWP for Baltica. Generally, the remanence from fracture fills may be useful for dating related tectonics, karst phenomena and mineralization processes.  相似文献   

18.
Summary. The directions of remanent magnetism of samples of the Dunnet Head sandstone from Scotland are very scattered on a scale down to a few millimetres, although an overall mean direction is reasonably well defined. The scattered directions show considerable stability against thermal demagnetization and there is evidence that haematite pigment is an important carrier of the remanence. It is concluded that the origin of the inhomogeneous magnetization is a disturbed ambient field during acquisition of chemical remanence by the pigment.  相似文献   

19.
Laboratory studies of depositional DRM   总被引：3，自引：0，他引：3  
Summary. Acquisition of magnetic remanence in slurries of fme grained organic muds settling in long tubes is investigated using a cryogenic magnetometer. The average settling behaviour of remanence carrying grains relative to the whole sediment gives information about the relative magnetic grain size spectrum, whereas the response of settled deposits to vibration gives an indication of the degree of alignment of particles and their average shape.
Two classes of behaviour are apparent in both the time and field dependence of detrital remanent magnetization (DRM) acquisition. Dilute slurries settling in the Earth's field (analogous to detrital sedimentation) acquire a remanence which reaches a maximum after about 2 day, whereas for concentrated slurries (analogous to slumped or bioturbated sediments) this takes only a matter of minutes. The field dependence of DRM in dilute slurries is in plausible quantitative agreement with Stacey's extension of the classical Langevin expression for the susceptibility of a paramagnetic gas, whereas concentrated slurries show a quasi-linear dependence of DRM on the applied field. Inclination errors are generally absent, but do appear in fields less than about 0.5 Oe, and when the magnetic fraction settles out preferentially. A weak negative dependence of DRM on temperature is found, but the results are too crude to provide a further test of Stacey's theory.
Remanence acquisition in slurries settled in zero field indicates that short term post-depositional magnetization processes are relatively unimportant in slurries that have ceased to compact rapidly. A large increase in remanence from naturally occurring sediments to slowly redeposited long cores, to rapidly settled slurries is best explained as a feature of compaction.  相似文献   

20.
Palaeomagnetic and geochronological measurements have been carried out on the late Pleistocene basaltic–andesitic unit of Monte Chirica–Costa Rasa, on the island of Lipari (Aeolian Archipelago). The lava flow sequence is about 10  m thick and has been sampled in detail. Magnetic properties are rather uniform; Curie temperatures of 540° to 580 °C, and the saturation IRM reached at applied values of 0.1  T point to titanomagnetite as the main magnetization carrier. Thermal and AF demagnetization have shown the presence of secondary magnetization components. These were removed mostly at 450°–500 °C or 20–30  mT, indicating a highly stable ChRM with directions from transitional to reverse. Where a ChRM could not be isolated by application of the demagnetization techniques, the converging remagnetization circles method gave a mean ChRM value fully comparable with that obtained from other methods. 40Ar/39Ar determinations were performed on two lava flows, in the lower and upper parts of the sequence. The former shows a transitional ChRM direction and a whole-rock age of 157±12  ka, the latter a reverse direction, a whole-rock age of 143±17  ka and a ground-mass age of 128±23  ka. The radiometric data and the reconstructed stratigraphy, which indicate ages of 150±10  ka and 104±3.5  ka, respectively, for the volcanic units at the bottom and top of the Monte Chirica–Costa Rasa unit, suggest that the reverse directions recorded in Lipari are related to the Blake event.  相似文献   

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