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1.
通过分析不同稀土La添加量对铁基胎体烧结性能的影响,指出在本试验使用预合金粉末和烧结条件下,当La添加量为0.1%时,胎体材料的综合力学性能最好。此外,适量的稀土La加入铁基胎体粉末后可以改善粉末分布的均匀性,提高金属胎体对金刚石的包镶能力。  相似文献   

2.
刘冀 《探矿工程》2021,48(5):47-53
为提高金刚石钻头钻进钢筋混凝土、强磨性岩层的钻进效率,选择了一种耐磨性高、冷压成型好的铁预合金粉。本文设计了铁基胎体配方,研究了铁基预合金粉、Cu、Ni、Co各成分对铁基金刚石钻头胎体及钻进性能的影响。测试了不同配方下烧结试样的抗拉强度、三点抗弯强度和硬度,使用扫描电镜对断口进行微观分析,通过现场钻进实验测试钻头的钻进效率与寿命。同时分析了保温时间对铁基胎体力学性能的影响。结果表明:Cu、Ni、Co对铁基胎体的抗弯强度和硬度影响较大,且保温时间为5 min时,铁基胎体可以获得较好的力学性能。  相似文献   

3.
金刚石工具用金属粉末一种能够提高胎体性能及改善胎体对金刚石粘结状态的金属粉末最近由北京科技大学粉末冶金教研室郭志猛副教授研制成功。该粉末系铬基合金(含铬量67%),液相温度低,可充分发挥Cr的作用,且价格低廉,适用于铁基、钴基和铜基胎体的刀头和磨块,...  相似文献   

4.
设计了粉末冶金法制备短碳纤维增强金刚石钻头铁基胎体材料,通过分析不同碳纤维添加量对胎体烧结性能的影响,得出在本实验制备条件下,短碳纤维对铁基胎体材料性能的影响规律,并对该结果进行了讨论分析,在此基础上,提出了制造更加优良短碳纤维增强铁基胎体材料的可能性。  相似文献   

5.
胎体配方预合金化近年来已成为有关孕镶金刚石钻头研究的一个新热点。根据相同的热压富铁基含金刚石钻头胎体配方,通过改变CSB-2预合金的加量和烧结温度,制作试样进行摩擦磨损测试,并对抗弯强度测试后的试样进行SEM分析和EDS能谱测试。摩擦磨损试验结果表明,4种烧结温度条件下,胎体磨损量均随着CSB-2加量的增大而减小,且相同CSB-2加量条件下,胎体磨损量随烧结温度的升高先增大后减小。SEM分析表明,添加CSB-2预合金可使胎体组织细化,孔隙数减少;高温烧结(980℃以上)时,铁基胎体对金刚石具有热腐蚀作用,随着胎体配方中CSB-2预合金含量的增加,金刚石的热腐蚀程度逐渐减缓。EDS能谱测试表明,胎体配方的预合金化可增大胎体金属对金刚石的润湿性,提高胎体对金刚石的包镶强度。  相似文献   

6.
胎体耐磨性(胎体硬度)是金刚石钻头的一个重要技术指标,它直接影响钻头、钻进规程参数的选择和钻探工程技术指标的提高。目前,现场所用钻头实际胎体硬度低于出厂钻头的标称硬度,而钻探施工一般按胎体标称硬度进行安排生产,所以会对钻探效率和进尺的提高带来误导和负面影响。为了提高钻头胎体硬度,进行了如下研究工作:改进钻头烧结工艺,提高胎体材料中碳化钨的比例和增加混料时间。在改进钻头烧结工艺中,建议讨论研究俄罗斯冷压烧结技术,其烧结压力可以达到70~100 MPa,远远高于我国热压烧结的压力,这将有利于胎体耐磨性的提高和钻探技术经济指标的改善。  相似文献   

7.
针对孕镶金刚石钻头在强研磨性地层中磨损快、寿命短的问题,利用WC硬度高、润湿性好、耐磨性好的特点,向铁基预合金粉末中添加WC颗粒作为胎体骨架金属。通过测试不同WC含量的胎体试样的硬度、抗冲击韧性以及抗弯强度,寻找骨架金属WC对胎体性能的影响规律。试验结果发现,随着WC含量的逐渐增加,胎体的硬度、抗冲击韧性、抗弯强度均呈现先增大后减小的变化趋势。从微观和能量的角度出发,分析了出现这种规律的原因。最后得出烧结温度为830 ℃、WC含量为5%时,胎体的性能达到最优,此时胎体的强度和研磨性最大。  相似文献   

8.
齐艳华  刘宝昌 《世界地质》2005,24(1):97-101
为降低孕镶金刚石复合材料的烧结温度,采用脉冲电流烧结法,对纳米Cu粉末、纳米WC-12%Co粉末及常规的63^#配方胎体进行了烧结实验。结果表明,纳米Cu粉在700℃可实现致密化,纳米WC-12%Co粉末、63^#配方胎体可分别在1100℃、850℃实现致密化,均大大低于常规烧结方法的烧结温度,还起到保护金刚石、降低能耗、增加石墨模具寿命的作用。  相似文献   

9.
从研究粘结金属在液态时与骨架材料和石墨(代替金刚石)的相互作用规律人手,对加入有强碳化物形成元素的几种铜基系列粘结材料做一系列实验,从中选择对金刚石润湿性好,附着功大的一种制成预合金化粉末粘结剂,同时采用金刚石表面离子化和改进烧结工艺,提高和改善胎体性能.本文以大量的实验资料对提高胎体金属与金刚石的粘结性能作一些讨论.  相似文献   

10.
热压碳化钨基复合胎体材料性能试验   总被引:3,自引:0,他引:3  
为了提高碳化钨(WC)基复合胎体材料的性能,在烧结压力为13 MPa、升温时间为6 min、保温时间为5 min的情况下,采用真空热压烧结的方法制备了金刚石钻头所用的10种不同比例WC基胎体材料试样30块,并对试样进行了洛氏硬度(HRC)、抗弯强度(σ)等性能测试。通过试验数据分析研究了WC、663青铜(ZQSn663)、锰(Mn)、钴(Co)、镍(Ni)与胎体材料HRCσ的关系。结果表明:WC质量分数对胎体的HRCσ的影响是主要因素,胎体的HRCσ具有内在联系,HRC高的胎体σ往往也高;在胎体配方中各个成分的含量都应得到控制才能保证胎体的性能优良,各成分的质量分数控制为:w(WC)<59.1%, w(ZQSn663)>25%, 3%<w(Ni)<6.5%, 0.9%<w(Co)<3.5%, w(WC-ZQSn663)<20%。  相似文献   

11.
磁铁矿是岩石、土壤和沉积物中少量而又普遍存在的副矿物,是环境磁记录的主要载体.磁铁矿在表生地质过程中受到机械、生物和化学风化作用使其结构、粒径、氧化程度、磁学性质发生一系列变化,这些变化对环境磁学以及表生地质过程的研究具有重要意义.从矿物学角度研究了磁铁矿粒径、相转变、氧化程度和磁化率随着研磨时间的变化规律.结果表明,平均粒径为4 μm的磁铁矿在研磨1 h后粒径变化趋于稳定,但随着研磨时间的增加,磁化率逐步降低而氧化率逐渐增加.通过对研磨后样品进行XRD分析表明,随着研磨时间的增加,磁铁矿衍射峰强度明显减弱,衍射峰宽化,赤铁矿的衍射峰强度逐渐增强.由此可见,原生磁铁矿(对沉积物而言属于碎屑磁铁矿)低温氧化产物是赤铁矿而不是磁赤铁矿.在表生地质演化过程中颗粒的机械碰撞不仅使磁铁矿颗粒变细,而且可能影响到磁铁矿常温氧化、磁学性质和晶体结构.  相似文献   

12.
煤矸石制作轻质莫来石砖研究   总被引:2,自引:0,他引:2       下载免费PDF全文
本文研究了利用煤矸石生产高档轻质莫来石砖的可行性,实验研究表明,在煅烧后的煤矸石中加入部分工业氧化铝粉,一起混磨至800目筛余小于5%,再经加有机质成型和1550℃×5小时煅烧,可制成物相及各种性能指标达到从德国进口轻质莫来石砖的制品。  相似文献   

13.
为减小孕镶金刚石切削工具的烧结温度对单晶金刚石性能的影响和改善切削工具胎体性能,降低烧结温度和优选胎体配方材料是很好的解决方法。在切削工具的胎体中加入适量纳米镍粉,通过对制备试样的硬度、强度和耐磨性测试及微观特征分析,综合评价该方法的可行性。结果表明:对于WC基胎体,含有纳米镍粉的胎体较不含纳米镍粉的胎体HRC提高11.9%,抗弯强度提高18.4%,耐磨性提高44.5%;对于Fe基胎体,含有纳米镍粉的胎体较不含纳米镍粉的胎体HRC提高19.5%,抗弯强度提高0.2%,耐磨性提高33.3%。既减小了温度对金刚石的影响,又提高了切削工具整体性能。  相似文献   

14.
INTRODUCTION The properties of phosphor usedin a plasma dis-play panel (PDP) affect the performance of the PDP(Okazaki et al .,2000 ; Rao and Devine ,2000) . Theluminescent properties of the phosphor are decided bythe morphology ,particle size and size distribution ofthe powder ,sothe requirements for the powder mor-phology are high in a color PDP which belongs to ahigh resolution display apparatus (I m et al .,2005 ;Yang et al ., 2005) . Studies have shown that withsmall particle si…  相似文献   

15.
The physical processes that govern the grain size of rocks in the upper mantle are examined. The analysis is based on the experimental data on creep, recrystallization, and grain growth in dunites and on a theoretical model for the thermomechanical structure of the cooling moving lithosphere. The grain size of rocks is shown to be determined by the in situ stress only at the deeper part where the temperature is high enough to allow significant strain rate. Above this depth, the microstructures record the thermomechanical history of rocks rather than the in situ stress.In the case of the oceanic lithosphere where the thermomechanical history is best known, the following features of grain-size distribution are found. At the uppermost mantle, where the amount of grain growth is limited, the grain size is determined by the initial value and the growth rate, and, where the effect of grain growth dominates, it increases with depth. When the amount of grain growth becomes large and the grain size reaches the steady state size corresponding to the ambient stress while the rock is hot enough to deform, the grain size is then determined by the applied stress. This grain size is, however, frozen, when the rock gets cool and the strain rate becomes too small to induce any further dynamic recrystallization. Thus, at the intermediate depth region, the grain size records the fossil (frozen) stress at which the microstructures of rock have been frozen. Since the frozen stress increases with age, the grain size in this depth interval decreases with depth. Finally, the grain size below this level reflects the in situ stress, and increases with depth, its extent being dependent on the nature of return flow in the deep mantle.Thus the grain size versus depth relation may show a sigmoid curve. The qualitative features of this curve may be similar also in the case of the continental lithosphere, if a similar thermal event (i.e., the intrusion of hot material and subsequent cooling) occurs. The results are quite consistent with the observed depth variation of olivine grain size in peridotite nodules (Avé Lallemant et al., 1980). The present model suggests that the depth of minimum grain size (65 and 150 km at the continental rift zone and the shield region respectively) corresponds to that where the mechanical properties of the upper mantle change from elastic to ductile at tectonic stress levels (~ 1 MPa) and in the geological time scale. This result leads to a new definition of the thickness of lithosphere in terms of its rheological properties. This thickness is about twice as large as that inferred from the flexure of lithosphere but approximately equal to seismic thickness. The model suggests the importance of grain growth as well as dynamic recrystallization and plastic flow in determining the texture of upper mantle rocks and therefore seismic anisotropy.  相似文献   

16.
钻井液在页岩钻探中对维护孔壁稳定十分重要,其滤失形成的泥饼对保护储层同样有着举足轻重的作用。为了研究页岩岩粉侵入低固相钻井液中对泥饼基本性能的影响,选取湘西北硅质页岩岩粉为研究对象,通过正交试验设计并对结果进行了极差分析和方差分析。研究结果表明:岩粉的含量是影响泥饼厚度的主要因素;影响泥饼韧度的主要因素为滚动时间以及岩粉的粒径;质量分数为6%的200目岩粉在滚动6 h后形成的泥饼最薄;150目的岩粉在质量分数为6%时滚动12 h后形成泥饼的韧度最大;级配为(200+100)目时,质量分数为2%的岩粉滚动24 h后形成泥饼最薄;级配为(200+150)目时,质量分数为4%的岩粉在滚动12 h后形成泥饼韧度最大。研究结论对钻井液现场的固相控制有积极意义。   相似文献   

17.
针对不同用户对煤炭粒径有不同的要求,煤颗粒粒径在4mm以下,其中0.125mm粒径以下的颗粒不能超过10%的无烟煤精粉有大量的出口需求,而目前所用设备产品质量不能满足要求,而且效率低的状况,对煤颗粒粒级分选设备的工作原理进行了分析并提出改进方案。基于流体力学理论对改进的设备的工作原理进行了数学建模和算例分析,得出随粒径不同,沉降时间不同,因而在风流中沉降距离不同,从而可以利用风流达到对煤粒进行分选的目的。  相似文献   

18.
The sintering behavior of olivine and olivine-basalt aggregates has been examined at temperatures near 1,300° C. Experimental factors contributing to rapid sintering kinetics and high-density, fine-grained specimens include: (i) the uniform dispersion of basalt throughout the specimen, (ii) a very fine, uniform particle size for the olivine powder, (iii) oxygen fugacities near the high P O2 end of the olivine stability field, and (iv) rapid heating to the sintering temperature. Olivine-basalt specimens prepared from olivine particles coated with a synthetic basalt achieve chemical and microstructural equilibrium more rapidly, as well as produce higher density and finer grain-sized aggregates, than do specimens prepared by mechanical mixing of olivine and natural basalt powders. The grain boundary mobility for olivine, measured for olivine-basalt aggregates which have undergone secondary recrystallization, is on the order of 2×10?15 (m/s)/(N/m2) in the temperature range 1,300–1,400° C. Solution-precipitation (pressure-solution) processes make an important contribution to the development of the microstructure in olivine-basalt aggregates.  相似文献   

19.
按硅粉的1%,5%,6%,10%将铌粉加入硅粉中,用“液硅渗透法”制备出四种掺铌硅化石墨样品。力学性能测试结果表明:6%铌掺杂增强效果最好,可使硅化石墨抗折、抗拉强度达178.5MPa,94.2%MPa,XRD、SEM、EPMA测试分析表明铌掺杂增强硅化石墨的机理是:碳化铌相的生成使原材料平直表面界面锯齿化,并平衡晶界附近不饱和价键,降低了晶界能;同时掺杂行为使晶粒细化,晶粒尺寸减小、气孔均匀分布,从而减弱应力集中,抑制裂纹扩展,提高材料强度。铌掺杂硅化石墨是改善材料性能的有效方式。  相似文献   

20.
Quartz powders (mean grain size: 22 μm) were pressed into sample discs of different green densities (ρ0=1.65; 1.85 and 2.05 g/cm3) and subjected to shock pressure between 1.5 and 17.0 GPa. Peak shock pressures were determined by the impedance method using the Hugoniot curves of steel and quartz powders. Fourier techniques were used to analyse the line broadening of 5 X-ray reflections in each case. The Fourier coefficients were subjected to a Rothman-Cohen correction before further processing. The coherent domain size decreases abruptly from several thousand Ångström in the unshocked state to about 800 Å at 1.5 GPa, and reaches a constant mean value of about 200 to 300 Å at dynamic pressures of about 4 GPa. At very high dynamic pressures (?15 GPa) there is further fragmentation to very small domain size. There is no systematic correlation between sample density and coherent domain size produced by the shock event. A more or less linear dependency exists between microstrain and pressure for each starting density of the quartz powder. The observation that microstrain decreases with increasing starting density could be explained by the fact that increasingly larger portions of the input energy are consumed to create fresh surfaces by comminution. Consequently, less energy will be available for strain strengthening. The stored energies in the shocked quartz powders are of the same order as the surface energy. Shock-treated quartz should therefore be suitable for accelerating any activated process such as sintering.  相似文献   

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