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1.
Daniel Buscombe 《Sedimentology》2013,60(7):1709-1732
In images of sedimentary or granular material, or simulations of binary (two‐phase) granular media, in which the individual grains are resolved, the complete size distribution of apparent grain axes is well‐approximated by the global power spectral density function derived using a Morlet wavelet. This approach overcomes many limitations of previous automated methods for estimating the grain‐size distribution from images, all of which rely on either: identification and segmentation of individual grains; calibration and/or relatively large sample sizes. The new method presented here is tested using: (i) various types of simulations of two‐phase media with a size distribution, with and without preferred orientation; (ii) 300 sample images drawn from 46 populations of sands and gravels from around the world, displaying a wide variability in origin (biogenic and mineralogical), size, surface texture and shape; (iii) petrographic thin section samples from nine populations of sedimentary rock; (iv) high‐resolution scans of marine sediment cores; and (v) non‐sedimentary natural granular patterns including sea ice and patterned ground. The grain‐size distribution obtained is equivalent to the distribution of apparent intermediate grain diameters, grid by number style. For images containing sufficient well‐resolved grains, root mean square errors are within tens of percent for percentiles across the entire grain‐size distribution. As such, this method is the first of its type which is completely transferable, unmodified, without calibration, for both consolidated and unconsolidated sediment, isotropic and anisotropic two‐phase media, and even non‐sedimentary granular patterns. The success of the wavelet approach is due, in part, to it quantifying both spectral and spatial information from the sediment image simultaneously, something which no previously developed technique is able to do. 相似文献
2.
Haosheng Wu Roman Bttger Frdric Couffignal Jens Gutzmer Joachim Krause Frans Munnik Axel D. Renno Ren Hübner Michael Wiedenbeck Ren Ziegenrücker 《Geostandards and Geoanalytical Research》2019,43(4):531-541
Although electron probe microanalysis and secondary ion mass spectrometry are widely used analytical techniques for geochemical and mineralogical applications, metrologically rigorous quantification remains a major challenge for these methods. Secondary ion mass spectrometry (SIMS) in particular is a matrix‐sensitive method, and the use of matrix‐matched reference materials (RMs) is essential to avoid significant analytical bias. A major problem is that the number of available RMs for SIMS is extremely small compared with the needs of analysts. One approach for the production of matrix‐specific RMs is the use of high‐energy ion implantation that introduces a known amount of a selected isotope into a material. We chose the more elaborate way of implanting a so‐called ‘box‐profile’ to generate a quasi‐homogeneous concentration of the implanted isotope in three dimensions, which allows RMs not only to be used for ion beam analysis but also makes them suitable for EPMA. For proof of concept, we used the thoroughly studied mineralogically and chemically ‘simple’ SiO2 system. We implanted either 47Ti or 48Ti into synthetic, ultra‐high‐purity silica glass. Several ‘box‐profiles’ with mass fractions between 10 and 1000 μg g?1 Ti and maximum depths of homogeneous Ti distribution between 200 nm and 3 μm were produced at the Institute of Ion Beam Physics and Materials Research of Helmholtz‐Zentrum Dresden‐Rossendorf. Multiple implantation steps using varying ion energies and ion doses were simulated with Stopping and Range of Ions in Matter (SRIM) software, optimising for the target concentrations, implantation depths and technical limits of the implanter. We characterised several implant test samples having different concentrations and maximum implantation depths by means of SIMS and other analytical techniques. The results show that the implant samples are suitable for use as reference materials for SIMS measurements. The multi‐energy ion implantation technique also appears to be a promising procedure for the production of EPMA‐suitable reference materials. 相似文献
3.
At first sight, experimental results and observations on rocks suggest that the Zr content in rutile, where equilibrated with quartz and zircon, should be a useful thermometer for metamorphic rocks. However, diffusion data for Zr in rutile imply that thermometry should not, for plausible rates of cooling, give the high temperatures commonly observed in high‐grade metamorphic rocks. It is suggested here that such observations can be accounted for by high‐T diffusive closure of Si in rutile, causing the interior of rutile grains to become insensitive to the thermometer equilibrium well above the temperature of Zr diffusive closure. Paired with comparatively slow grain boundary diffusion and problematic zircon nucleation, this allows for cases of Zr retention in rutile through temperatures where Zr is still diffusively mobile within rutile grains. Other observations that may be accounted for in this context are large inter‐grain ranges of rutile Zr contents uncorrelated with rutile grain size, and flat Zr profiles across individual rutile grains, counter to what would be expected from diffusive closure. A consequence is that it is unlikely that Zr‐in‐rutile thermometry will be useful for estimating rock cooling rates. 相似文献
4.
YanYan Yang LianYou Liu XiaoYan Li PeiJun Shi GuoMing Zhang YiYing Xiong YanLi Lyu LanLan Guo Bo Liang MengDi Zhao JiaDong Dai XiYang Zuo XuJiao Han 《Sedimentology》2019,66(2):590-603
Aeolian sand entrainment, saltation and deposition are important and closely related near surface processes. Determining how grains are sorted by wind requires a detailed understanding of how aerodynamic sand transport processes vary within the saltating layer with height above the bed. Grain‐size distribution of sand throughout the saltation layer and, in particular, how the associated flux of different grain size changes with variation in wind velocity, remain unclear. In the present study, a blowdown wind tunnel with a 50 cm thick boundary layer was used to investigate saltating sand grains by analyzing the weight percentage and transport flux of different grain‐size fractions and the mean grain size at different wind velocities. It was found that mean grain size decreases with height above the sand bed before undergoing a reversal. The height of the reversal point ranges from 4 to 40 cm, and increases with wind velocity following a non‐linear relationship. The content of the finer fractions (very fine and fine sand) initially increases above the sand bed and then decreases slightly with height, whereas that of the coarser fractions (medium and coarse sand) exhibits the opposite trend. The content of coarser grains and the mean grain size of sand in the saltation layer increase with wind velocity, indicating erosional selectivity with respect to grains in multi‐sized sand beds; but this size selectivity decreases with increasing wind velocity. The vertical mass flux structure of fine sand and very fine sand does not obey a general exponential decay pattern under strong wind conditions; and the coarser the sand grain, the greater the decrease rate of their transport mass with height. The results of these experiments suggest that the grain‐size distribution of a saltating sand cloud is governed by both wind velocity and height within the near‐surface boundary layer. 相似文献
5.
6.
Christopher J. Stevenson Peter J. Talling Douglas G. Masson Esther J. Sumner Michael Frenz Russell B. Wynn 《Sedimentology》2014,61(4):1120-1156
Grain‐size breaks are surfaces where abrupt changes in grain size occur vertically within deposits. Grain‐size breaks are common features in turbidites around the world, including ancient and modern systems. Despite their widespread occurrence, grain‐size breaks have been regarded as exceptional, and not included within idealized models of turbidity current deposition. This study uses ca 100 shallow sediment cores, from the Moroccan Turbidite System, to map out five turbidite beds for distances in excess of 2000 km. The vertical and spatial distributions of grain‐size breaks within these beds are examined. Five different types of grain‐size break are found: Type I – in proximal areas between coarse sand and finer grained structureless sand; Type II – in proximal areas between inversely graded sand overlain by finer sand; Type III – in proximal areas between sand overlain by ripple cross‐laminated finer sand; Type IV – throughout the system between clean sand and mud; and Type V – in distal areas between mud‐rich (debrite) sand and mud. This article interprets Types I and V as being generated by sharp vertical concentration boundaries, controlled by sediment and clay concentrations within the flows, whilst Types II and III are interpreted as products of spatial/temporal fluctuations in flow capacity. Type IV are interpreted as the product of fluid mud layers, which hinder the settling of non‐cohesive grains and bypasses them down slope. Decelerating suspensions with sufficient clay will always form cohesive layers near to bed, promoting the generation of Type IV grain‐size breaks. This may explain why Type IV grain‐size breaks are widespread in all five turbidites examined and are commonplace within turbidite sequences studied elsewhere. Therefore, Type IV grain‐size breaks should be understood as the norm, not the exception, and regarded as a typical feature within turbidite beds. 相似文献
7.
Michael Wiedenbeck 《Geostandards and Geoanalytical Research》2008,32(4):489-494
Secondary ion mass spectrometry (SIMS or ion microprobe) remains one of the most powerful tools available to the analytical geochemist. Despite the impressive progress witnessed by other competing laboratory methods over recent years, SIMS remains unsurpassed in its combination of small sampling volumes with low analytical uncertainties. Although the current SIMS analytical design has existed for over three decades, the period 2006–2007 saw significant advances in instrumentation, analytical methodology and, not least, the characterisation of new reference materials upon which all analyses depend. As of the end of 2007 the SIMS geoscience literature was reporting total sampling masses down to the 10 fg range, spatial resolution of better than 100 nm and uncertainties on major element isotope ratio determinations of better than ± 0.2‰ (1s). This article intends to synthesise the progress made by the geo‐SIMS community during this two year period and will also highlight some specific research results that were only possible due to the unique capabilities provided by SIMS. 相似文献
8.
文章回顾了粒度分析的历史,总结了常用的粒径类型,介绍了粒度标准和目前沉积学中常用的5种粒度分析方法,并对其中的沉降法、场干扰分析法、图像法作了详细的分类说明。此外,对每一种粒度分析方法的适用范围、测定原理以及其存在的优缺点也进行了详细的介绍。其中：直接测量法简单易行,但精度较差;筛析法较为普遍,但只限于松散或弱胶结沉积物,且不能反映颗粒形状;沉降法适用于松散样、弱胶结样和液体样的分析,可对细砂、粉砂或泥等细粒沉积物进行测量;场干扰法主要依据碎屑颗粒的衍射、散射及电压脉冲响应进行,固体样和液体样均可,精度高,适用性广;图像法手段多样,简单直观,操作性强。总体上,未来的几十年内,粒度分析方法仍将是新旧技术并存,多种方法共用的状况。 相似文献
9.
Both monsoons and westerlies have exerted influence on climate dynamics over the Tibetan Plateau (TP) since the last deglaciation, producing complex patterns of paleohydroclimatic conditions. Diverse proxy records are essential to forge a robust understanding of the climate system on the TP. Currently, there is a general lack of understanding of the response of inland lakes over the TP to climate change, especially glacier‐fed lakes. Paleohydrological reconstructions of such lakes could deepen our understanding of the history of lake systems and their relationship to regional climate variability. Here we use records of n‐alkanes and grain size from the sediments of Bangong Co in the western TP to reconstruct paleohydrological changes over the past 16,000 years. The Paq record (the ratio of non‐emergent aquatic macrophytes versus emergent aquatic macrophytes and terrestrial plants) is generally consistent with the variations in summer temperature and precipitation isotopes. The changes in grain‐size distributions show a similar trend to Paq but with less pronounced fluctuations in the early‐middle Holocene. The new data combined with previous results from the site demonstrate that: 1) Bangong Co experienced relatively large water‐level fluctuations during the last deglaciation, with a steadily high lake‐level during the early‐middle Holocene and a decreasing lake‐level in the late Holocene; 2) The lake level fluctuations were driven by both high summer temperatures via the melting water and monsoon precipitation. However, the dominant factor controlling lake level changed over time. The lake‐level history at Bangong Co deduced from the n‐alkanes and grain‐size records reveals the past hydrological changes in the catchment area, and stimulates more discussion about the future of glacier‐fed lakes under the conditions of unprecedented warming in the region. 相似文献
10.
沉积物粒径趋势分析:原理与应用条件 总被引：16，自引：1，他引：15
长期以来,沉积学家尝试用粒度数据来识别沉积环境的类型或判定物质运动的方式,但只取得了部分成功。粒度参数还有一项可能的用途,即用其平面差异来获取物质输运信息。沉积学家将粒度参数的平面差异定义为“粒径趋势”,并建立了以“粒径趋势分析”为基础的定性物质输运模型。粒径趋势分析的基本科学问题包括:如何提取粒径趋势信息;如何确定含有物质输运信息的粒径趋势类型;粒径趋势分析的应用条件是什么。粒径趋势信息可通过粒径趋势矢量的定义及其各向异性显著性的检验而获得,而经验证据也显示,含有物质输运信息的粒径趋势类型是存在的。初步研究表明,粒径趋势分析应满足以下条件:粒径趋势矢量具有显著性;底质采样深度应代表同一时间尺度;平面采样间距应符合地统计法的规则;避免使用位于采样网格边缘上的采样点的粒径趋势矢量;沉积物样品应属于同一个输运体系或研究区处于堆积状态。但是,由于不同来源的物质混合、源区沉积物特征及变化、不同水动力条件下的物质输运、悬沙沉降、溶解态—颗粒态物质转换、物质输运动力的侧向分布等因素与粒径趋势形成之间的关系还不够明确,因此这些条件还不是完备的,这个问题的解决依赖于粒径趋势形成的过程和机制的进一步研究。 相似文献
11.
Chemical zoning, recorded by grain growth during metamorphism, is a key source of information about P–T–t paths. Interpretation of these data must be carried out using appropriate models and recognizing their inherent assumptions. To assist with defining how zoned minerals form, a set of geometric criteria for three types of chemical zoning developed in minerals (diffusion, growth and grain recycling) is outlined. Re‐equilibration of minerals by lattice diffusion causes zoning if the re‐equilibration is incomplete. Growth of porphyroblasts is commonly considered in pelites, but in metagranitoids, large monophase domains undergo coarsening by recycling of material from one grain to another as grain boundaries migrate driven by surface energy. This type of grain size increase is termed here ‘grain recycling’. Zoning developed during grain recycling due to equilibration of the recycled material with grain‐boundary chemistry is termed ‘grain‐recycling zoning’. Furthermore, short lattice diffusion lengths relative to grain sizes cause metamorphic fractionation because material in the grain cores is not in communication thermodynamically with the rest of the rock. A new model is derived for this sort of grain size increase coupled with metamorphic reactions using Theriak–Domino. An example is given of plagioclase undergoing an increase in anorthite content as epidote breaks down during amphibolite facies metamorphism of a metagranitoid. Agreement between naturally occurring zoning profiles and those derived from modelled P–T–t paths shows that this model can be used to extract metamorphic conditions from rocks which are not accessible using conventional thermobarometry. 相似文献
12.
13.
Guo‐Qiang Tang Ben‐Xun Su Qiu‐Li Li Xiao‐Ping Xia Jie‐Jun Jing Lian‐Jun Feng Laure Martin Qing Yang Xian‐Hua Li 《Geostandards and Geoanalytical Research》2019,43(4):585-593
Secondary ion mass spectrometry (SIMS) requires matrix‐matched reference materials to calibrate mass fractionation during oxygen isotope measurement. Over one thousand SIMS oxygen isotope measurements were conducted on eleven natural mineral samples (five olivines, three clinopyroxenes and three orthopyroxenes) in nineteen sessions using CAMECA IMS 1280 SIMS instruments to evaluate their potential as SIMS reference materials. The obtained results reveal oxygen isotope homogeneity of these samples. No matrix effect was measured for the same variety of mineral samples with limited Mg‐number variations (89.6–94.2, 90–91.9 and 90.1–92.1 for olivine, clinopyroxene and orthopyroxene, respectively). The recommended oxygen isotope compositions of these samples were determined using laser fluorination. These samples are therefore suitable to be used as reference materials for in situ oxygen isotope microanalysis. 相似文献
14.
Rucao Li Xiaoping Xia Shenghong Yang Huayong Chen Qing Yang 《Geostandards and Geoanalytical Research》2019,43(1):177-187
Sulfur isotope measurements in three sulfide (two pyrite and one pyrrhotite) samples on two epoxy mounts showed that the mount‐to‐mount variation of raw δ34S values was negligible when secondary ion mass spectrometry (SIMS) analytical settings remained stable. In consequence, an off‐mount calibration procedure for SIMS sulfur isotope analysis was applied in this study. YP136 is a pyrrhotite sample collected from northern Finland. Examination of thin sections with a polarising microscope, backscattered electron image analyses and wavelength dispersive spectrometry mapping showed that the sample grains display no internal growth or other zoning. A total of 318 sulfur isotope (spot) measurements conducted on more than 100 randomly selected grains yielded highly consistent sulfur isotope ratios. The repeatability of all the analytical results of 34S/32S was 0.3‰ (2s, n = 318), which is the same as that of the well‐characterised pyrite reference materials PPP‐1 and UWPy‐1. Its δ34S value determined by gas mass spectrometry was 1.5 ± 0.1‰ (2s, n = 11), which agrees with the SIMS data (1.5 ± 0.3‰, 2s) calibrated by pyrrhotite reference material Po‐10. Therefore, YP136 pyrrhotite is considered a candidate reference material for in situ sulfur isotope determination. 相似文献
15.
Yu Liu Qiu‐Li Li Guo‐Qiang Tang Xian‐Hua Li 《Geostandards and Geoanalytical Research》2020,44(3):421-437
A combined geochronological and geochemical investigation for the same domain of zircon provides valuable information on timing and genesis, particularly in the case of multi‐growth metamorphic zircon. A high spatial resolution concurrent analytical method for zircon U‐Pb age and rare earth element content was successfully achieved in this study, using a multi‐collector secondary ion mass spectrometer (SIMS) at a ~ 8 μm diameter scale. Special instrument parameters were employed, including a high mass resolution of approximately 15000 applied to replace the previous energy filter method, and a dynamic multi‐collector mode used to reduce the measurement time to 18 min per analysis. Six zircon reference materials yielded precise and accurate 206Pb/238U ages, which are comparable to those obtained by the ordinary mono‐collector method, but with 2–3 times higher spatial resolution. All zircon grains measured in this study showed enriched heavy‐REE (HREE) contents consistent with previously reported values determined by LA and solution ICP‐MS methods. The light‐REE (LREE) mass fractions measured using both SIMS and LA‐ICP‐MS methods in this study, although with quite different volume, show consistent results within uncertainties. 相似文献
16.
LIANG Chenyue LIU Yongjiang ZHENG Changqing LI Weimin Franz NEUBAUER ZHANG Qian 《《地质学报》英文版》2019,93(5):1477-1499
The calcite mylonites in the Xar Moron-Changchun shear zone show a significance dextral shearing characteristics. The asymmetric(σ-structure) calcite/quartz grains or aggregates, asymmetry of calcite c-axes fabric diagrams and the oblique foliation of recrystallized calcite grains correspond to a top-to-E shearing. Mineral deformation behaviors, twin morphology, C-axis EBSD fabrics, and quartz grain size-frequency diagrams demonstrate that the ductile shear zone was developed under conditions of greenschist facies, with the range of deformation temperatures from 200 to 300°C. These subgrains of host grains and surrounding recrystallized grains, strong undulose extinction, and slightly curved grain boundaries are probably results of intracrystalline deformation and dynamic recrystallization implying that the deformation took place within the dislocation-creep regime at shallow crustal levels. The calculated paleo-strain rates are between 10~(–7.87)s~(–1) and 10~(–11.49)s~(–1) with differential stresses of 32.63–63.94 MPa lying at the higher bound of typical strain rates in shear zones at crustal levels, and may indicate a relatively rapid deformation. The S-L-calcite tectonites have undergone a component of uplift which led to subhorizontal lifting in an already non-coaxial compressional deformation regime with a bulk pure shear-dominated general shear. This E-W large-scale dextral strike-slip movement is a consequence of the eastward extrusion of the Xing'an-Mongolian Orogenic Belt, and results from far-field forces associated with Late Triassic convergence domains after the final closure of the Paleo-Asian Ocean. 相似文献
17.
对大型湖泊盆地沉积物粒度组成进行研究,有助于解读全球致密油气和页岩油气勘探开发与其记录的古气候信息。
文章对青海湖沉积物粒度时空分布进行了详细的研究,通过采集覆盖大部分湖区的27根近现代沉积岩芯,并对湖心的三根
典型沉积岩芯进行了137Cs测定获取沉积岩芯的年龄;基于磁化率地层年龄模式,建立了整个湖区沉积岩芯的年代框架。粒
度分析结果显示,青海湖岩芯沉积物的粒度分布呈多峰,以细颗粒沉积为主,其中粉砂含量60%~70%,粘粒组分为10%~
35%,砂粒组分低于20%。青海湖沉积物的粒度变化在空间上相对较复杂,中值粒径呈现明显的砂岛附近、西部和西南湖
区高,其他湖区低的特征。在时间上,大体上自1960年到2017年呈现变粗的趋势,砂粒组分增多,粘粒组分减少。这些粒
度的时空变化可能是受风砂活动、流域土壤侵蚀、河流径流变化、湖平面变化和人类活动共同作用而成。 相似文献
18.
对大型湖泊盆地沉积物粒度组成进行研究，有助于解读全球致密油气和页岩油气勘探开发与其记录的古气候信息。
文章对青海湖沉积物粒度时空分布进行了详细的研究，通过采集覆盖大部分湖区的27根近现代沉积岩芯，并对湖心的三根
典型沉积岩芯进行了137Cs测定获取沉积岩芯的年龄；基于磁化率地层年龄模式，建立了整个湖区沉积岩芯的年代框架。粒
度分析结果显示，青海湖岩芯沉积物的粒度分布呈多峰，以细颗粒沉积为主，其中粉砂含量60%~70%，粘粒组分为10%~
35%，砂粒组分低于20%。青海湖沉积物的粒度变化在空间上相对较复杂，中值粒径呈现明显的砂岛附近、西部和西南湖
区高，其他湖区低的特征。在时间上，大体上自1960年到2017年呈现变粗的趋势，砂粒组分增多，粘粒组分减少。这些粒
度的时空变化可能是受风砂活动、流域土壤侵蚀、河流径流变化、湖平面变化和人类活动共同作用而成。 相似文献
19.
联用筛析法与激光法进行粒度接序分析的界点选择 总被引：1，自引：0，他引：1
筛析法、激光法和图像法是三种常用的粒度分析方法,但由于测试原理的不同,三种测试方法有不同的适用性。筛析法和图像法能够精确测量砂质颗粒的粒径,但不适用于泥质细颗粒（<0.063 mm）的粒径测量;相反,激光法无法准确测量中粗砂粒级颗粒（2~0.21 mm）,但能高精度测量较细沉积物粒径。分选较差的天然沉积物粒径分布范围较广,需要综合运用筛析法-激光法进行接序粒度测试。通常选用2 mm为界点开展接序粒度分析,但因激光法在测量中粗砂颗粒时误差较大,易导致接序粒度分析结果准确性不高。建议以0.21 mm为分界点开展接序粒度分析,分别避开筛析法和激光法测量精度不高的粒级区间,可使测试结果的准确性得到有效的提高。 相似文献
20.
A log‐normal spectral analysis of inorganic grain‐size distributions from a Canadian boreal lake core: Towards refining depositional process proxy data from high latitude lakes 
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下载免费PDF全文 Paul R. Gammon Lisa A. Neville R. Timothy Patterson Martine M. Savard Graeme T. Swindles 《Sedimentology》2017,64(3):609-630
Better methods for interpreting grain‐size spectra will enhance current understanding of past transport–depositional processes. A high‐resolution inorganic grain‐size dataset has been measured from a freeze core extracted from ‘Alberta Lake E’ a boreal fresh water lake 40 km east of the Athabasca Oil Sands in north‐eastern Alberta, Canada. The grain‐size spectra are remarkably consistent throughout the core, exhibiting a structure comprising six persistent grain‐size distributions below ca 250 μm, plus a rare medium‐sand distribution. Automated deconvolution of the grain‐size spectra produced poor results. Constraining the modes of two of the distributions produced deconvolution solutions that were statistically excellent and consistent with the structure of each spectrum. Statistical analysis of the ‘constrained’ solutions indicates that deconvolution successfully extracted independent grain‐size populations. Conversely, the multimodal spectra generate traditional measures (for example, mean grain size) that are inconsistent combinations of different individual populations and thus are poor proxies of transport–depositional processes. Alberta Lake E is situated in a boreal wetland landscape where sediment delivery is dominated by overland flow transport during spring melt. This context means that the Alberta Lake E grain‐size spectra can be interpreted to reflect: (i) a bedload component transported during short‐duration high discharge events that reflect the intensity of the melt; and (ii) a finer suspended load component representing material whose magnitude is controlled by the volume of the spring melt. Stratigraphically, bedload and suspended load populations demonstrate different short‐wavelength and long‐wavelength cyclicity, suggesting that spring melt is likely to be driven by cyclic external forcing factors. The links between the grain‐size spectra and spring melt have potential for generating proxy records that better capture the external controls over spring melt in boreal systems and the risks associated with these energetic hydrodynamics. This is exemplified by the coarsest Alberta Lake E distributions, which indicate that more intense spring‐melt dynamics occurred in pre‐historical times. 相似文献