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1.
There are only a few luminescence dating studies of loess sediments in Japan, but interleaved with these deposits are many well-described tephras of known age based on 14C and fission track analysis; these independent age controls provide an opportunity to test the reliability of loess luminescence ages. This study provides such a comparison at two sites in central Honshu, the largest island in the Japanese archipelago. Samples were collected from sequences of interleaved volcanic tephra and loess deposited on a Middle Pleistocene river terrace in the Niigata Prefecture and on an Early to Middle Pleistocene dissected fluvial surface at in the Tochigi Prefecture, Honshu. Equivalent doses (De) were estimated from fine grains (4–11 μm) using both polymineral IR-OSL and (post-IR) blue-OSL, and quartz blue-OSL. The blue-stimulated luminescence signals could be represented by up to three exponentially decaying components; only the most light sensitive of these components was used in the final De estimation. Almost all the estimates of De from polymineral IR-OSL are smaller than those from polymineral (post-IR) blue-OSL and quartz blue-OSL, whereas the latter two are in good agreement. The blue-light stimulated luminescence ages using the most light sensitive component are shown to be in good agreement with the independent control, up to 500 ka. Although the IR-OSL signals underestimate the known age, a simple laboratory fading test is found empirically to correct for this underestimation. We conclude that the most rapidly blue-stimulated luminescence signals from quartz extracted from our loess samples give reliable ages, and that future loess dating studies should concentrate on these signals.  相似文献   

2.
Optically stimulated luminescence of fine silt quartz was investigated to establish chronologies for lake sediments from the British Isles. Feldspar contamination and its potential effects on equivalent dose (De) determination were examined. A new feldspar contamination test based on the thermal quenching of quartz OSL and thermal assistance of feldspar OSL identified feldspar contamination in samples being treated for 20 min in 20% hydrofluoric acid. Feldspar component monitoring based on the post-IR OSL/OSL ratio was not sufficiently sensitive to monitor a feldspar component, but is a good indicator whether a standard SAR procedure can be applied successfully, despite the presence of feldspar. Based on these results we used a modified SAR protocol including a 100 s IRSL stimulation at 50 °C before OSL readout. This protocol could overcome any malign effects of feldspar even for a feldspar bearing polymineral sub-sample.  相似文献   

3.
Previous luminescence dating studies on loess from China and Tajikistan have focused on the establishment of the regional chronology of the loess sequences. In order to improve the precision and accuracy of optical ages derived from the loess of the last glacial period in these regions, we have examined the components of luminescence signals in three loess samples from western China and southern Tajikistan. Our results show that the polymineral IRSL and post-IR OSL, and quartz OSL signals from loess of the two regions are represented by three components, which display different bleaching and growth characteristics. While the composition of the polymineral IRSL signals is similar between samples with the same age from the two regions, in the case of quartz there is significant discrepancy in the proportion of the fast and medium components of the OSL signals. Greater difference is observed in the composition of the polymineral post-IR OSL signals for the loess from the two regions. The three components of polymineral IRSL signals yield almost identical equivalent dose values as that derived from the total IRSL signal. An apparent agreement in equivalent dose is observed between the fast component of the polymineral post-IR OSL and the quartz OSL for the loess of western China but not in the loess of the same age from southern Tajikistan. The fast component of the quartz OSL yields an equivalent dose 25% higher than that based on the total signal for the sample from the base of the Late Pleistocene loess in southern Tajikistan. This demonstrates the importance of signal selection for an accurate luminescence dating of Central Asian loess.  相似文献   

4.
Luminescence dating has long been used for chronological constraints on marine sediments due to the ubiquitous dating materials (quartz and feldspar grains) and its applicability over a relatively long time range. However, one of the main difficulties in luminescence dating on marine sediments is partial bleaching, which causes age overestimations. Especially, partial bleaching is typically difficult to be detected in the fine grain fraction (FG) of marine sediments. The recently developed feldspar post-IR IRSL (pIRIR) protocol can detect non-fading signals and thus avoid feldspar signal instability. In the current study, fine grains were extracted from a gravity core in the northern Sea of Japan, and the aim is to test the feasibility of using different luminescence signals with various bleaching rates to explore the bleaching conditions of fine grain fraction in marine sediments. The results suggest that the quartz OSL signal and polymineral pIRIR signals at stimulation temperatures of 150 °C and 225 °C (pIRIR150 and pIRIR225) of FG were well bleached prior to deposition. The OSL ages were used to establish a chronology for this sedimentary core and the resulting age-depth relationship is self-consistent and comparable with radiocarbon dates. We conclude that different luminescence signals with various bleaching rates can be used to test the bleaching conditions of fine grain fraction in marine sediments; and the luminescence dating can be applied to marine sediments with great potential.  相似文献   

5.
Sediments of river deltas provide valuable records of past coastal environments. Optically-stimulated luminescence (OSL) dating has become an alternative to radiocarbon dating for constraining the sediment chronology in large deltas that allow for sufficient sunlight bleaching of sediments during the fluvial transport. However, its applicability to smaller deltas with mountainous riverine systems has not been confirmed yet. To check this, we examine multiple signals from two Holocene sediment cores in the wave-dominated Thu Bon River delta in central Vietnam. Two cores were collected, respectively, 3.9 km and 1.2 km inland from the present shoreline and both show a >-25-m thick succession of coarsening-upward mud to sand deposits. Coarse grains (180–250 μm in diameter) of quartz and K-feldspar, and fine grains (4–11 μm in diameter) of quartz and polymineral were extracted from the upper and lower parts of the cores for multi-grain measurements of quartz OSL, and of feldspar infrared-stimulated luminescence (IRSL) at 50 °C (IR50) and post-IR IRSL at 175 °C (pIRIR175) to determine burial ages. In addition, facies analysis and radiocarbon dating were conducted. The landward core consists of transgressive to early regressive estuarine and prodelta facies, which is overlain by a sandy beach-shoreface facies. The seaward core consists of a relatively simple shallowing-upward succession from muddy prodelta facies to sandy beach-shoreface facies. All luminescence ages except for pIRIR175 of fine grains are mostly consistent with the radiocarbon ages. Instead, pIRIR175 ages of fine grains are significantly overestimated with variable offsets. OSL and IR50 of fine grains provide reasonable age estimates, as these grains were likely well bleached during the transport even along a short and steep mountainous river. Consistent age estimates of all signals from sand indicate that sand was well-bleached in the beach and shoreface owing to the frequent sediment reworking by waves and currents. These results support the hypothesis that luminescence dating is applicable to Holocene wave-dominated deltas and reiterate that comparing different luminescence signals is an effective way to check reliability of the age estimates in environments where the sunlight bleaching is not ensured.  相似文献   

6.
The Late Pleistocene sea-level history of Antarctica is key to understanding and predicting the responses of icesheets, which significantly contribute to the global sea level, to changing climates. Coastal sediments at Lützow-Holm Bay, East Antarctica, have yielded radiocarbon ages of Holocene and Marine Oxygen Isotope Stage (MIS) 3 from deposits above the present sea level, suggesting that there have been two episodes of sea-level highstand. However, radiocarbon dating is likely to be less accurate for dating sediments close to or older than 40–50 ka, the upper limit of its application. We thus explored the applicability of luminescence dating to coastal sediments newly sampled from Langhovde on the eastern coast of Lützow-Holm Bay. Samples were collected from a trench <1 m deep and at several meters above the present sea level. Quartz coarse and fine grains, K-feldspar coarse grains, and polymineral fine grains were extracted from the samples. Quartz coarse and fine grains both showed very low optically stimulated luminescence sensitivity and no fast component and thus were not considered further. Dose-recovery tests on post-infrared infrared-stimulated luminescence (post-IR IRSL) signals of K-feldspar and polymineral grains yielded variable results and suggested acceptable measurement conditions for each grain size fraction and expected equivalent dose. Preliminary measurements revealed that the trench section can be divided into the upper and lower layers, corresponding to the Holocene and MIS 7, respectively. Further application of post-IR IRSL dating to coastal sediments, including to previously radiocarbon-dated sections, could refine our understanding of the late Quaternary relative sea-level history in East Antarctica.  相似文献   

7.
In this study we test the potential of the elevated temperature infrared stimulated luminescence (IRSL) signals for dating Romanian loess. The recently developed post-IR IRSL protocol is applied to Romanian loess using polymineral fine grains extracted from the loess-palaeosol sequence at Mircea Vodă (SE Romania). This approach is aimed at obtaining an additional age control to examine the age discrepancy obtained from previous optically stimulated luminescence (OSL) studies using different grain-sizes of quartz (4–11 μm and 63–90 μm).Two preheat post-IR IR stimulation temperature combinations were used, 250–225 °C and 325–300 °C, respectively. The signals obtained are documented in terms of dose response curve, laboratory tests and fading. Although both post-IR IRSL signals exhibit small fading rates, dose response characteristics indicate that these rates may be laboratory artefacts. The post-IR IRSL signal stimulated at 300 °C is observed to suffer from dose dependent initial sensitivity changes as both natural and regenerated signals are observed to lie above the saturation level of the dose response curve. Uncorrected age results obtained using both post-IR IRSL signals are in general agreement with previously reported silt-sized quartz OSL ages for samples collected from the uppermost loess unit L1. For older material, the post-IR IRSL signal stimulated at 225 °C is considered to provide reliable age results, in agreement with independent age control available for this sequence.  相似文献   

8.
The Altyn Tagh Fault(ATF)is one of the most prominent active strike-slip faults in the India-Eurasia collision. Fresh features of surface ruptures, which are attributed to seismic events taking place in the last millennium, are identified at several sites along the Che'erchen River to Qingshui River section on the central part of ATF. Accurate chronology of these earthquake events would help understand the spatial-temporal relationship of the recent earthquakes. However, great difficulties are encountered. The central ATF is located in the arid area, and the vegetation cover is so limited that rare organic materials appropriate for radiocarbon dating can be found in the sediments. Luminescence dating technique may serve as an alternative to directly determine the burial ages of the earthquake related sediments. The optically stimulated luminescence(OSL)signal of quartz, which has been widely employed for luminescence dating, displays unwanted charateristics for accurate dating. Firstly, the quartz OSL signal is not sensitive to irradiation, which leads to low signal-to-noise ratio or even no measurable quartz OSL signal. Secondly, the targeted samples of the last millennium are very young, and the radiation dose received during the burial is expected to be less than 3~4Gy, which futher deteriorates the signal-to-noise ratio of the quartz OSL signal. Therefore, quartz OSL signal is not appropriate for dating the sediments relevant to the recent earthquakes on ATF.
The infrared stimulated luminescence(IRSL)signal of potassium feldspar is an alternative, and it is in usual an order of maginitude more sensitive to raidation than the quartz OSL signal. The enhanced signal-to-noise ratio makes it applicable to young samples. The post-IR IRSL signal has been successfully applied to date the sediments beyond the Holocene, however, the relatively slow bleaching of the post-IR IRSL signal poses challenges on applying it to young sediments, especially for the sediments deposited during the last millennium. In this study, we investigated the feasibility of using post-IR IRSL signal from potassium feldspar to date the earthquake events of the last millennium by employing modern sag pond deposits with different sorting and expected equivalent dose(De)of 0Gy. Choosing an appropriate measurement procedure and identifying the well bleached pottassium feldspar grains are essential for post-IR IRSL dating of young sediments. The non-fading characteristic of the post-IR IRSL170 signal measured at 170℃ following a prior IR stimulation at 110℃ was verified by employing the De plateau test with respect to the signal integration interval and IR stimulation temperature together. Reducing the amount of potassium feldspar grains mounted on an aliquot would help reveal the among grains variation of bleaching level of post-IR IRSL170 signal before depostion and identify the most sufficiently bleached grains. Therefore, the post-IR IRSL170 De values of 2mm aliquots were measured for three samples with different sedimentary textures. The median of De distribution of well sorted and stratified sag pond deposits is consistent with the minimum De value inferred from the minimum age model(MAM-3) and finite mixture model(FMM), while for the poorly sorted deposits, the median is significantly overestimated compared with the minimum De values from the MAM-3 and the FMM. The minimum De values of 0.6~0.8Gy of all three samples are consistent with the unbleachable residual dose previously reported for post-IR IRSL signals measured at similar temperature for well bleached samples. It implies that by combined use of small aliquot and statistical age models, the well-bleached potassium feldspar grains could be identified. Such an intrinsic unbleachable component needs to be properly corrected when earthquake events of last millennium are to be dated in this area. Otherwise, the post-IR IRSL170 age would be overestimated by 200~300a.
The post-IR IRSL170 procedure investigated in this study is not only applicable for dating the paleoearthquake events along the Altyn Tagh Fault, but also with great potential to be applied to other tectonically active area. With consideration of the potential variability in post-IR IRSL signal characteristics of potassium feldspar grains from different origins, the signal stability needs to be routinely inspected. The modern analog sample would also be informative for justifying the measurement procedure and analytical method employed.  相似文献   

9.
Anomalous fading of the infrared stimulated luminescence (IRSL) signal from the polymineral fine-grain and K-feldspar fractions of aeolian sediments from Hungary has been studied. The samples in this study have previously been dated using the multiple aliquot additive dose (MAAD) protocol to measure the IRSL signal. The IRSL measurements using MAAD were conducted ～4 weeks after the irradiation, making it difficult to assess to what extent these age estimates were affected by anomalous fading. In this study, equivalent doses were obtained using the single aliquot regenerative dose (SAR) protocol. The fading rate for each sample was calculated using the different IRSL components and different parts of the decay curve. For each sample, the middle part of the decay curve always showed a lower fading rate than the initial part of the decay curve. The difference between the fading rates for different parts of the decay curve was greater for the K-feldspars than for the polymineral fine grains. Fading corrected ages were calculated by integrating both the initial and the middle part of the decay curve. These ages were compared with optically stimulated luminescence (OSL) ages from quartz, infrared radiofluorescence (IR-RF) ages obtained from K-feldspars and also with independent ages, provided by radiocarbon dating of shells and charcoal, and uranium-series dating of travertine.  相似文献   

10.
Modern and known-age Pleistocene fluvial sediments were investigated by optical dating of quartz to test the suitability of the approach for dating deposits from the deeply incised Middle Rhine Valley. Samples from modern flood sediments revealed skewed distributions indicating different residual levels of equivalent dose (De) within the different aliquots. Nevertheless, a substantial number of aliquots from the modern deposits reflect De values close to zero. For the Pleistocene samples, optical ages are in general consistent with age control given by the presence of the Laacher See Tephra and radiocarbon dating. However, some samples overestimate the known age by a few thousand years when using the arithmetic mean. This is apparently explained by including aliquots in the determination of mean De where the optical signal was incompletely bleached at deposition. The most difficult issue in this context is identifying a suitable approach that can distinguish between the variability of De due to partial bleaching and microdosimetry. However, even when considering these limitations it appears that optical dating will by a quite suitable method to date Pleistocene sediments from such a complex fluvial environment, especially when focusing on a precision scale beyond a few thousand years.  相似文献   

11.
A thick Middle and Late Pleistocene loess-palaeosol sequence is exposed at the Stari Slankamen section in the Vojvodina region situated in the south-eastern part of the Pannonian basin, Serbia. The profile exposes an about 45 m thick series of loess intercalated by at least eight pedocomplexes. Ten samples were dated by luminescence methods using a modified single aliquot regenerative dose (SAR) protocol for polymineral fine grains and for quartz extracts from the upper part of the Stari Slankamen loess sequence. The infrared stimulated luminescence (IRSL) and post-IR optically stimulated luminescence (OSL) signals from all polymineral samples showed anomalous fading, suggesting that the post-IR OSL signal is still dominated by feldspar OSL. The ages ranging from 4.6 to 193 ka were obtained after fading correction. These ages indicate that the loess unit V-L1L1, the weakly developed soil complex V-L1S1 and the loess unit V-L1L2 were deposited during marine isotope stage (MIS) 2, 3, and 4, respectively, and also indicate that the loess unit V-L2 is of the penultimate glacial age.  相似文献   

12.
A comparative study using quartz optically stimulated luminescence (OSL) and feldspar post-infrared infrared stimulated luminescence (post-IR IRSL) was undertaken on Quaternary fluvial sediments from an unnamed tributary of the Moopetsi River in South Africa. The aim is to assess whether the post-IR IRSL signal can be used to date incompletely bleached sediments. Several post-IR IRSL signals using varying stimulation and preheat temperatures were investigated; of these the post-IR IRSL225 signal was deemed most appropriate for dating because it bleached most rapidly. The feldspar post-IR IRSL225 equivalent dose (De) values from this site are consistently larger than those from quartz OSL, probably due to differences in the bleaching characteristics of the two signals. Additionally, the post-IR IRSL225 De values within a sample showed less variation in precision than the quartz De data, possibly due to greater averaging between grains in the feldspar small aliquots. The agreement between ages based on the OSL and post-IR IRSL225 signals was better for younger samples (<20 ka) than for older ones (>50 ka); the cause of this variation is unclear.  相似文献   

13.
Linking the timing of glacial episodes and behaviour to climatic shifts that are documented in ice and marine sedimentary archives is key to understanding ocean-land interactions. In the NW Scottish Highlands a large number of closely spaced (‘hummocky’) moraines formed at retreating glacier margins. Independent age control on one palaeo-glacier limit is consistent with the timing of Younger Dryas (YD) glaciation in the area, but adjacent glacier lobes have remained undated due to the lack of sites and material for 14C dating. Direct dating of ice-marginal moraines using optically stimulated luminescence (OSL) techniques has never been attempted before in Scotland, but if successful, they may be the most appropriate methods for constraining the age of sediment deposition in the absence of organic material. Coarse-grained quartz and K-feldspar minerals from supraglacial sheet flow deposits and glacilacustrine sediments within ice-marginal moraines were analysed using the single-aliquot regenerative-dose (SAR) protocol. Independent age control and clear geomorphological relationships indicate that all samples should yield YD or post-Last Glacial Maximum (LGM) ages. Quartz OSL shine down curves showed low luminescence sensitivity, significant medium-to-slow components, a weak fast component, and scattered SAR data; Linearly Modulated-OSL (LM-OSL) measurements confirmed that the fast component was weak or absent. In contrast, feldspar infrared stimulated luminescence (IRSL) was highly sensitive with excellent SAR data. However, SAR data from 3 mm diameter aliquots of feldspar (200 grains) give higher than expected equivalent doses (De) by an order of magnitude. SAR measurements of small clusters of feldspar grains (ranging from 1–8) considerably broaden the apparent De distribution, but even the lowest value is about 2–3 times the expected De. Two possibilities arise to explain the quartz and feldspar data: (1) that glacial sequences in the NW Highlands re-work inherited (older) glacial deposits and that some of the pre-Devensian existing glacial landforms have only been modified during Devensian glaciation; or (2) that the sedimentary processes operating in these ice-marginal environments are not conducive to adequate bleaching of quartz and feldspar grains. Our study implies that ice-proximal supraglacial sediments from this region in NW Scotland reflect older ages of deposition, but dating YD sediments has not been possible.  相似文献   

14.
Constraining the ages of fluvial terraces is essential to understanding fluvial responses to climate and sea-level changes and estimating uplift/incision. Luminescence dating of sand or silt grains from fluvial terrace deposits in Japan is difficult because sand layers are often absent from gravelly deposits, quartz grains are typically dominated by medium/slow components and/or contaminated by feldspars, and short transport distances and short residence times in riverbeds result in poor bleaching of luminescence signals. Luminescence dating of cobbles may overcome these difficulties, but few studies have applied this technique to fluvial terrace deposits. Here, we examine the utility of luminescence dating applied to three granodiorite cobbles from a late Pleistocene fluvial terrace deposit of the Ara River, Japan. We investigated variations of the infrared stimulated luminescence (IRSL) and post-IR IRSL signals with depth in each cobble. The IRSL and post-IR IRSL signals generally increase with depth, indicating that the cobbles were not completely bleached before deposition. Nonetheless, the IRSL ages of the cobble surfaces (19–17 ka) are consistent with the age of a tephra layer (16–15 ka) at the base of loess deposits overlying the terrace. In contrast, IRSL ages of sand-sized feldspar grains overestimate the depositional age because of incomplete bleaching, whereas silt-sized quartz grains greatly underestimate the depositional age, likely because of the thermal instability of the medium component. Our results demonstrate that luminescence dating of cobbles could provide a better understanding of fluvial systems in which luminescence dating of sand grains is difficult.  相似文献   

15.
OSL dating of sediments from deserts in northern China   总被引：2，自引：0，他引：2  
Aeolian samples from deserts in northern China were studied using the optically stimulated luminescence (OSL) of quartz and potassium (K) feldspar separates. K-feldspar has shown advantages over quartz for dating samples younger than 100 years, due to its more homogeneous equivalent dose (De) values, higher internal dose rate and higher luminescence sensitivity to dose. Without additional measurements, the luminescence characteristics of quartz obtained in De determination procedures can be used to reveal the source material and/or quartz thermal history for the deserts in northern China. The results indicated that the duration of paleosol formation in desert areas reflects regional paleoenvironments.  相似文献   

16.
Post-depositional mixing or exhumation is common in surficial sediments, yet may be unobservable from field evidence. However, any disturbance may have significant consquences in terms of establishing a reliable luminescence age determination. Optically stimulated luminescence (OSL) measurements, particularly measurements at the single grain level, can be used to gain an insight into both contemporary and past post-depositional processes.

This paper examines sites from Texas and Florida (USA) with independent chronological control to demonstrate the potential effects of varying degrees of bioturbation on OSL. Results show that contemporary soil forming processes clearly impact on the palaeodose (De) replicate distributions which are measured in order to derive an OSL age. Significant levels of scatter and apparently zero dose grains are observed in the upper-most sediments; declining with depth from the surface. De replicates from undisturbed and fully bleached sediments are unskewed, show low overdispersion (OD) and comparable single grain and single aliquot OSL ages. Bioturbated sediments, however, may show highly skewed multi-model De distributions with higher OD values, zero dose grains at depth, and significant diffences between single grain and single aliquot results. True burial ages may be derived from minimally bioturbated sediments through the application of statistical analysis such as finite mixture modelling to isolate De components. However, for significantly bioturbated sediments, the latter approach, even at the single grain level, produces inaccurate ages. In such cases we argue that additional evidence (both dating and contexual) may be required to identify with confidence the burial De population.  相似文献   


17.
This study applies single-grain optically stimulated luminescence (SG OSL) dating of quartz sand temper to Intermountain Ware ceramics recovered from four archaeological sites in northwestern Wyoming, USA. We show that SG OSL dating can strengthen and further refines existing archaeological site chronologies in certain settings. The SG OSL results are compared to multi-grain infrared stimulated luminescence (IRSL) dating of the polymineral (feldspar and quartz) silt fraction in the ceramic paste of the same sherds. Results from the two methods are statistically indistinguishable, although coarse-grained quartz SG OSL ages have consistently lower standard error terms due to higher relative sensitivity and avoidance of anomalous fading calculations. Moreover, the SG OSL results produced precision at two-sigma standard error greater than or equal to associated calibrated radiocarbon ages. SG OSL dating of quartz temper from Intermountain Ware ceramics provides more reliable site occupation timing than radiocarbon dating, which can be conditioned by incorporation of old wood and contamination from young soil carbon. This study highlights the importance of SG OSL dating on sherds from buried contexts when exposure to wildfires may have occurred, as ceramics recovered from the ground surface of one site after a high-intensity fire produced near-modern apparent ages, suggesting they were thermally reset during the fire. We suggest SG OSL should be applied to date similar ceramics with quartz temper to determine site age and bolster regional chronologies.  相似文献   

18.
In this article we test for the first time the potential of single-grains of K-rich feldspar to date well-bleached and poorly bleached sediments using a post-IR IRSL (pIRIR) protocol. We measure natural dose distributions using K-rich feldspars from four coastal samples applying the pIRIR protocol with a preheat of 200 °C and a pIRIR stimulation temperature of 180 °C; each sample had an independent age control obtained from quartz OSL and radiocarbon dating. We also analyse single-grain dose distributions of “zero-dose” and γ-irradiated samples to determine thermal transfer/residual doses and the intrinsic sources of variability of pIRIR single-grain measurements, respectively. Based on these experiments, we conclude that thermal transfer/residual dose give rise to an offset of ∼0.6 Gy in these samples and that the uncertainty assigned to individual pIRIR single-grain dose estimates cannot be smaller than 16.5%.The analysis of the well-bleached samples shows that only the brightest 30% of the grains give pIRIR single-grain ages in agreement with the age control; this effect may arise from the suggested correlation between blue emission and potassium content of individual grains. Comparison of single-grain quartz and feldspar dose distributions from the poorly bleached samples shows that quartz is relatively better bleached; nevertheless, selection of a reliable ‘minimum’ feldspar dose was achieved using two different statistical models.  相似文献   

19.
The effect of weathering on optically stimulated luminescence dating   总被引：2，自引：0，他引：2  
Optically stimulated luminescence (OSL) dating was applied to quartz samples recovered from the gravel sediments of deformed marine terrace at the Suryum site, southeastern Korea, but has yielded stratigraphically inconsistent ages. Micromorphological, chemical, and mineralogical analyses of the gravels indicate the possible influence of chemical weathering on the apparent OSL ages. In the course of weathering after emerging from beach environments, originally permeable gravels underwent infilling by halloysite-rich clays in their voids, export and import of radioactive elements, and loss of mechanical strength with the creation of a porosity within pebbles. Calculation based on the evolution of the weathering profile showed a severe fluctuation of dose rate caused by the change of water content and radioactive element concentrations. Samples recovered from the weathering profile inevitably include quartz grains derived from mechanically weakened pebbles or illuviated from the upper layer, making it difficult to determine the equivalent dose (De) values of exclusively depositional quartz sands. Quantitative evaluation of the change of fabric and chemistry of the sediments on the basis of pedologic insight significantly aids in the derivation of OSL ages consistent with geomorphology and other independent age controls.  相似文献   

20.
Resetting of sediments mobilised by the LGM ice-sheet in southern Norway   总被引：3，自引：0，他引：3  
Former geological field investigations in the Rondane area, east-central southern Norway, have proposed that the maximum Fennoscandian ice-sheet coverage occurred during the Late Weichselian Glacial Maximum (LGM, ca. 20 ka) and that subsequent glaciofluvial sediments were first deposited in the early Holocene (after 10 ka). However, recent field investigations with ages from three internally consistent quartz optically stimulated luminescence (OSL) age series show an apparent deglaciation of northern Rondane in the period 20.0–13.8 ka. We examine here the possibility that these ages are too old because the sediment was not completely zeroed prior to deposition. Our investigations of incomplete bleaching use modern analogues, small aliquots, and single grains of quartz. First, the symmetric shape of small aliquot equivalent dose distributions suggests that the sediment was probably well bleached at deposition. This is supported by 5 modern analogue equivalent doses (De) of 0.6 Gy, 1.5% of the typical De from the deglaciation sediments. Finally, from single grain studies on three samples, we conclude that there is no evidence for poor bleaching in these samples; thus the weighted mean gives the best estimates of De, and these are completely consistent with both large and small aliquot estimates for these samples. These comparisons between large aliquots, modern analogues, small aliquots and single-grain analyses help to validate the OSL ages and confirm the complete resetting of these sediments prior to deposition.  相似文献   

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