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1.
We present the results of a combined Electron Spin Resonance (ESR) and Luminescence dating study for the lowermost stratigraphic unit (TD1) of the palaeoanthropological site of Atapuerca Gran Dolina, Spain. Ten samples collected through the Main Section were dated using either the Multiple Centre (MC) ESR approach or the single-grain thermally transferred optically stimulated luminescence (SG TT-OSL) technique, both of which were applied to quartz grains. The two methods yield consistent ages, providing a robust chronostratigraphic framework for the TD1 deposits and enabling improved correlation of the magnetostratigraphic succession (comprising three intervals of normal polarity; N1 to N3, from bottom to top) with the Geomagnetic Polarity Time Scale. Specifically, the results provide a late Early Pleistocene chronology for TD1, and clearly position the deposits in the post-Olduvai time range (<1.77 Ma). The final age estimates range from 1.30 ± 0.14 Ma (TT-OSL) close to the bottom of the section to a mean ESR age of 1.05 ± 0.12 Ma (1 s.d.) for three samples from the N3 interval towards the top. Consequently, the N3 interval may confidently be correlated to the Jaramillo Subchron, while we propose a correlation of N1 and N2 with the Cobb Mountain subchron and Punaruu excursion, respectively; although we cannot exclude that these two normal intervals may correspond to other, unknown, geomagnetic events given the existing uncertainties associated with the ESR and luminescence ages.From a methodological point of view, the ESR MC approach shows that the Titanium signal provides the most reliable burial ages for TD1. In contrast, the Aluminium centre yields systematically overestimated age estimates, as a result of incomplete resetting of the signal before sediment deposition. The SG TT-OSL ages presented here are amongst the oldest published so far, and highlight the potential of the high temperature SG TT-OSL290 approach for obtaining finite ages exceeding 1 Ma at Atapuerca.Finally, these new dating results provide key insights into the rates and nature of sedimentary processes at Gran Dolina, modifying long-standing interpretations of the cave formation and infilling dynamics. An age of at least 1.4 Ma may be inferred for the base of the sedimentary infill at the Main Section, providing minimum age constraint for the formation of the cavity and, by extension, for the intermediate level of the Atapuerca karst. The opening of the cave, which pre-dates human occupation, most likely occurred close to or slightly after 0.9 Ma. This suggests that both TD4 and TD6 archaeological levels were deposited within a relatively short time range of <100 kyr. The so-called autochthonous fluvial deposits from TD1 unit, or at least those dated in the present study, were also clearly primarily derived from outside the karst system, and were not reworked from older deposits within the karst. They experienced sufficient daylight exposure and minimum transport times within the karst system to enable consistency between the ESR and TT-OSL burial ages and the independent magnetostratigraphic evidence. Our results highlight the need to reconsider the terminology traditionally employed to differentiate the two main phases of Gran Dolina's sedimentary infill.  相似文献   

2.
The Sima del Elefante site is located within the Sierra de Atapuerca karst system (Burgos, northern Spain), and forms part of a series of important Early, Middle and Late Pleistocene archaeological complexes that have been dated previously with luminescence techniques (Gran Dolina, Galería Complex, Sima de los Huesos, Galería de las Estatuas). This study focuses on the upper Middle Pleistocene units (TE18 and TE19) at Sima del Elefante, which contain Acheulean and transitional lithic assemblages (Mode 2/3), as well as large and small mammal fossils. Importantly, these uppermost units are associated with a sediment plug located in the cave's interior at Galería Baja, which marks the closure of a significant palaeoentrance to the Atapuerca karst system. Establishing the accumulation history of these related deposits is important for understanding both Lower Palaeolithic technological dynamics via comparisons with similar levels at other Atapuerca sites (i.e., Gran Dolina and Galería Complex), as well as past human occupation patterns and carnivore use of (and accessibility to) the caves. We present single-grain TT-OSL and multi-grain pIR-IR chronologies for the Sima del Elefante upper sequence and the Galería Baja sediment cone, as well as U-series dating results for a stalagmitic crust capping the combined clastic infill sequence. The paired luminescence ages for the upper occupation levels are in agreement with each other and reveal that the host deposits accumulated 576–481 ka for the TE18 stratified scree layers, 266–237 ka for TE19 and 206–250 ka for the Galería Baja upper cone section (weighted mean 2σ age ranges). A concordant U-series age of 202 ± 65 ka is obtained for the overlying stalagmitic crust at Galería Baja. The Sima del Elefante ages are consistent with those previously obtained using U-series and biochronology, confirming that there is an erosional unconformity and complex carbonate deposition phase associated with the upper layers of unit TE18 and that the original cave entrance likely closed by ∼200 ka. Chronological correlation with other Atapuerca sites reveals potential equivalence between TE18 and unit TD8 (at Gran Dolina), and between TE19 and units GIIb–GIIIb (at Galería Complex) and, possibly, TD10.1 and TD10.2 (at Gran Dolina), though more refined dating is required to confirm the latter.  相似文献   

3.
The Sierra de Atapuerca (Northern Spain) is characterized by a well-developed karst system where several major archaeological sites have been discovered, attesting an almost continuous hominin occupation of the area during the whole Pleistocene period. Previous geomorphological studies showed a connection between genesis of the karst system and the evolution of the nearby Arlanzón river Valley. However, numerical dating results were missing to refine the chronostratigraphical framework of the Arlanzón valley's fluvial incision. To address this, we applied the Electron Spin Resonance (ESR) dating method to sedimentary optically bleached quartz grains from several fluvial terraces. Nine samples were collected from five of the 14 identified terraces. The ESR age results are stratigraphically coherent and in general agreement with both previous geomorphological observations and available palaeomagnetic data. Consequently, an ESR chronology of the geological evolution of the Arlanzón valley is proposed, which can be then correlated to the sedimentary sequence of the palaeoanthropological site of Atapuerca Gran Dolina. Our results provide important information about the chronology of hominid occupation in this area during Early and Middle Pleistocene.  相似文献   

4.
During the last two decades, extensive road-construction works in Northern France have allowed the discovery of numerous Middle Palaeolithic sites. Geological and multidisciplinary studies performed on these localities allowed the establishment of a precise chronostratigraphical and biostratigraphical framework of regional significance, which could be correlated to the global marine palaeoclimatic scale. Each human occupation layer has been linked to this regional framework, thus providing a stratigraphical age-control for the Middle Palaeolithic human settlements of this area.At the same time, a program of geochronological studies was developed using TL, OSL, U-series, ESR and, as often as possible, ESR/U-series methods. Hence, bones and teeth recovered from archaeological sites of Savy, Ault, Caours, Gentelles and La Celle-sur-Seine, were analyzed and the results compared to the chronostratigraphical ages. The age results are generally in good agreement with the geological data while bones and dental tissues display in some cases U-series ages higher that the EU-ESR ones, suggesting U-loss phenomena.  相似文献   

5.
Sedimentary records from the inner-shelf of the East China Sea (ECS) are unique for the reconstruction of post-glacial palaeoclimate and sea-level changes. So far, the chronology of sediment succession from this region has mainly been based on radiocarbon dating, which might be problematic due to reworked deposition or old carbon contamination. In this study we tested the applicability of optically stimulated luminescence (OSL) dating to a drilling core (ECS-DZ1) taken from the northern ESC. A total of 20 OSL samples and two radiocarbon samples were collected from the upper 58 m of this core. The results indicate the likely sufficient reset of OSL signal of fine-grained (4–11 μm) quartz before burial, and thus reliable chronology for the studied core sediments. For one sample, however, the extracted coarse-grained (100–200 μm) quartz overestimated the deposition age significantly, presumably resulting from partial bleaching prior to deposition. The fine-grained quartz ages are generally consistent with the stratigraphical order, and the reliability of these OSL ages are further validated by two selective robust 14C dates. The chronological framework of core ECS-DZ1 reveals striking sedimentation-rate changes. By comparison with other chronostratigraphical records, we infer that post-glacial deposition history (since ∼15 ka) of the study site is likely related to regional sea-level rise and delta-estuary environment evolution, as well as strengthened human activities and/or coastal currents.  相似文献   

6.
Single-grain thermally transferred optically stimulated luminescence (TT-OSL) dating has recently been applied to a number of the Atapuerca palaeoanthropological sites. As yet, however, there have not been any direct assessments of TT-OSL signal stabilities for specific grains used for dating. In this study, we undertake a series of TT-OSL suitability assessments on known-age samples from Gran Dolina and Sima del Elefante. Our results suggest that the Atapuerca samples contain populations or sub-populations of grains with suitably stable TT-OSL signals for dating over late-Early and Middle Pleistocene timescales. Equivalent dose (De) distribution analysis in combination with pulse-annealing assessments provides a useful means of identifying inter-grain and inter-sample differences in TT-OSL signal stabilities. We also show that obtaining De values using different preheat conditions may help to identify potentially problematic TT-OSL behaviours. Analyses of multi-grain aliquot TL curves for these samples reveal that 'bulk' TL signal loss experiments may provide limited insights into TT-OSL source trap lifetimes due to averaging effects, the dominance of grain populations that do not produce TT-OSL, and interference from slowly bleaching OSL components. Our results improve the robustness and precision of existing TT-OSL chronologies for units TD6-3 and TE16-TE17 at Gran Dolina and Sima del Elefante, and support the broader suitability of the single-grain TT-OSL approach at the Atapuerca sites.  相似文献   

7.
The Caune de l'Arago, located at Tautavel in the southern part of France, is one of the best documented Middle Pleistocene sites allowing a good understanding of human evolution in Europe. Since its discovery in 1829, the cave yielded more than 140 human remains associated with abundant lithic industries and thousands of faunal remains in a 10 m thick stratigraphical sequence divided in three complexes (Lumley et al., 2014). The Lower stratigraphic complex is only known from cores while the Middle and Upper ones can be divided into about 17 main archaeological levels indexed from the bottom to the top: from level Q to level A. Since 1981, a number of dates were done using practically all the methods available for dating Quaternary period up to 700 ka. U-series dates performed on the upper stalagmitic floor yielded a minimum age of 400 ka for human remains found in the underneath level G (Falguères et al., 2004). This age range confirmed the direct non-destructive gamma-ray age published more than 30 years before (Yokoyama and Nguyen, 1981). Recently, a methodological work was published on herbivorous teeth coming from different parts of the G level highlighting the difficulties to get reliable radiometric dates on a level so rich in bones and partly weathered by guano deposits or issues associated with carbonate accumulation (Han et al., 2010).This study presents new ESR/U-Series dates obtained on herbivorous teeth coming from the lowest excavated layers (Q–P levels) which yield an age range for the entire thick archaeological infilling. The new results suggest that the sedimentological levels containing lithic and faunal artefacts began to be deposited at 550 ka in the P–Q levels and a younger age of 350–400 ka for the F level. The P–Q levels which have yielded bifaces are one of the oldest evidence of the Acheulian culture in the southern part of Western Europe while the dates obtained on G level suggest a contemporaneity with la Sima de los Huesos and TD10 Dolina level at Atapuerca.  相似文献   

8.
The area of Pléneuf-Val-André, Brittany, France, has delivered several Palaeolithic sites containing palaeontological remains, very rare into this granitic area. In order to precise the stratigraphical framework of the prehistoric human occupations of this zone, an ESR dating program was initiated in the late 1980s and different kinds of materials (mammal bones and teeth, naturally bleached quartz extracted from marine or aeolian sediments and marine mollusc shells) were then sampled for geochronological analyses. The present paper displays the main obtained results on three stratigraphically connected middle Palaeolithic sites: Piégu, Les Vallées and Nantois. The results are consistent with the regional chronostratigraphic framework and permit to suggest palaeoenvironmental reconstruction of the area and the dating of the various archaeological evidences.  相似文献   

9.
Based on detailed field observation and multidisciplinary studies of integrated stratigraphy, the marine Lower and Middle Triassic of Lower Yangtze region is divided into five third-order sequences, the general approach of the outcrop sequence stratigraphical study of carbonate ramp is proposed, the pattern in the development of the Early and Middle Triassic sequence under the major regression is summarized, and the sequence stratigraphical and chronostratigraphical frameworks across various paleogeographical facies zones on the marginal platform are established. Project supported by the Stake Key Project “SSLC” and the National Natural Science Foundation of China (Grant Nos. 49502022, 49632070).  相似文献   

10.
The site of Bonneval (France) exhibits a 6 m thick stratigraphical sequence in which Middle and Lower Palaeolithic artefacts were discovered. The stratigraphy of the site consists of an alternation of loess-like silt layers deposited along glacial stages, and paleosoil horizons corresponding to the vegetal stabilization of the area during interglacials. These layers hence provide past environmental informations and can be used as stratigraphical markers and compared with well dated sequences of Northern France. Eight sediment samples from this Middle and Upper Pleistocene sequence were dated using the recuperated optically stimulated luminescence (Re-OSL) signal of quartz grains. The middle-size fraction (40–63 μm) shows a good reproducibility of the OSL signals which allows the application of a multiple-aliquot additive-dose approach for De determination. For all samples, the growth curves are linear up to an accumulated dose of 3000 Gy. The Re-OSL ages range from ~100 to ~450 ka and are in good agreement with the independent chronological information; they establish when handaxe industries have been made during the Middle and Upper Pleistocene in the Paris Basin.  相似文献   

11.
Dose saturation represents a fundamental limitation for obtaining finite optically stimulated luminescence (OSL) quartz ages over Middle Pleistocene timescales. Single-grain OSL studies typically reveal significant intra- and inter-sample variability in quartz dose saturation properties at the individual grain level. This enhanced variability may offer the potential to obtain extended-range chronologies exceeding the traditional upper age limits of multiple-grain OSL dating. However, there have been relatively few detailed assessments of single-grain OSL properties over high dose ranges. In this study we investigate extended-range single-grain OSL dating potential at Cuesta de la Bajada, one of the most important Ancient Middle Palaeolithic sites in the Iberian Peninsula. The quartz samples from this site exhibit exceptional dose saturation properties and contain significant populations of individual ‘supergrains’ with bright OSL signals, very high characteristic saturation dose (D0) limits of 200 to >600 Gy, and dose-response curves that closely conform to single saturating exponential functions. Assessments of OSL signal composition and the ability to successfully recover a known laboratory dose of 470 Gy support the potential for obtaining high equivalent dose (De) values with reasonable fitting uncertainties. A series of novel sensitivity tests are used to assess potential biases in supergrain De estimation over high dose ranges related to (i) thermally transferred signal contributions, (ii) choice of dose-response curve fitting function, and (iii) insufficient dose saturation properties of individual grains. The single-grain De values obtained using the standard quality assurance criteria and novel sensitivity tests are consistent at 2σ, and are in agreement with quartz Ti-centre ages obtained on two of three paired electron spin resonance (ESR) samples collected from Cuesta de la Bajada. These comparisons support the suitability of our single-grain OSL results and suggest there may be good potential for using quartz supergrains to establish extended-range chronologies at some Middle Pleistocene sites. Comparisons with other single-grain OSL studies across the Iberian central plains suggest that favourable dose saturation properties may be influenced by regional-scale geological controls. The importance of undertaking single-grain OSL dating at Cuesta de la Bajada is also demonstrated by the results of synthetic aliquot experiments, which reveal multiple-grain age offsets of 60–170 ka when unsuitable grain types are inadvertently included in the final age calculations. The single-grain OSL results indicate that the main archaeological horizon at Cuesta de la Bajada (unit CB3) accumulated between 264 ± 22 and 293 ± 24 ka. These ages are consistent with the chronologies of other key early Middle Palaeolithic sites in the region (Ambrona AS6 and Gran Dolina TD10) and indicate that the Ancient Middle Palaeolithic techno-complex likely spread across Iberia from at least Marine Isotope Stage 9 onwards.  相似文献   

12.
Since 1970, many prehistoric sites have been discovered in the alluvial terraces of several rivers of the Middle Loire River basin (France). During the last decade, the stepped-terraces systems of three of the Loire tributaries, the Creuse, the Cher and the Loir Rivers, were the focus of multidisciplinary studies, involving Quaternary geology, prehistory and geochronology. The geochronological data now available for these systems were mainly obtained by electron spin resonance (ESR) method applied to optically bleached fluvial quartz. These results provide a chronological framework for the evolution of fluvial systems and the human settlements of this area during Lower and Middle Pleistocene. Two phases of human settlement could be distinguished, around 1.1 Ma (Early Palaeolithic – Mode 1) and around 0.7 Ma ago (Acheulean – Mode II).  相似文献   

13.
Dating of quartz by optically stimulated luminescence (OSL) has been revolutionized with introduction of the test dose (TD) in development of a measurement sequence known as the single-aliquot regenerative-dose (SAR), whereby a valid sensitivity correction for the luminescence signal is provided in the measurement cycle. However, the size of the TD used in the SAR protocol remains controversial. Previous studies show that the TD has little effect on the equivalent dose (De) for young samples in luminescence dating in which the applicability of different deposits varies greatly in different regions. However, detailed studies are lacking on how TD size affects SAR–OSL results of samples with a relatively high De range. In this study, typical loess samples with high De values (∼60 Gy–∼250 Gy) from the eastern Tibetan Plateau were selected to investigate the effects of variation in TD size on the quartz SAR–OSL protocol. Dose recovery tests show that a known dose could be recovered successfully by applying different TDs. Test dose size has an effect on shapes of regenerated dose–response curves (DRCs) and has different influences on Des and characteristic saturation doses for quartz samples with a high dose range. A TD size of 20%–30% De is a good compromise for Tibetan loess with De of ∼60–120 Gy in the quartz SAR protocol, and a TD size larger than 30% should be considered for samples with a larger De. The results of this study highlight the importance of TD size in the SAR–OSL protocol for quartz samples with a high dose range.  相似文献   

14.
OSL and IRSL dating are applied to samples from a 152 m-long drill core to constrain the timing of three glaciolacustrine depositional periods within the infill of an overdeepened bedrock trough in the Lower Glatt valley, N Switzerland. The characterisation of the dose-response suggests that the polymineral IRSL50 and pIRIR180/225 signals are close to saturation, while quartz OSL ages are within the range of reliable dating. The demarcation of the upper quartz OSL dating limit, however, remains challenging. Dose-recovery tests performed with long storage periods were used to investigate the reliability of the high region of the dose-response curve. They suggest an upper limit for reliable dating of ∼400 Gy for these samples, which was considerably lower than the commonly used 2D0 criterion. Lifetimes were calculated for the quartz OSL and the thermal stability of the signal is not considered as problematic for the determined ages. Allowing for a contribution from inherited dose due to partial bleaching, places the infill of the overdeepened valley within the penultimate glacial cycle (MIS6).  相似文献   

15.
The archaeological site of Payre (France) yielded Middle Palaeolithic layers with Neanderthal remains, which are partly bracketed by two stalagmitic flowstones. To obtain a precise chronological framework for the human occupation and the faunal remains of this site, several dating methods were used: uranium-series (U-series by alpha spectrometry and TIMS) and electron spin resonance (ESR) on stalagmitic flowstones, combined ESR/U-series on teeth and bones, and thermoluminescence (TL) on burnt flints. Most of the ages obtained for levels H to C range from 300 to 140 ka. The age-spread obtained for the anthropic (burnt flints) and faunal remains (bones and teeth) suggests that the dated levels represent several human occupation periods, near the transition from MIS8 to MIS7 (levels G–F) and from MIS6 to MIS5 (levels D–E).  相似文献   

16.
17.
Loess deposits distributed in southeastern China play an important role for paleoclimate reconstruction of the subtropical regions. These loess-paleosol deposits are mainly spread within the middle and lower reaches of the Yangtze River as well as in the drainage area of the Huai River. The ages of loess paleosol sequences that are distributed along the Huai River are not well constrained. In this study, the standard single-aliquot regenerative dose (SAR) optically stimulated luminescence (OSL) protocol and two elevated temperature post infrared-infrared stimulated luminescence SAR protocols (pIRIR225 and pIRIR290) were applied on 4–11 μm quartz and polymineral fine grains, respectively, in order to obtain the first numerical luminescence chronology for a loess-paleosol sequence in northern Jiangsu Province. Our results show a good agreement between quartz SAR-OSL and polymineral pIRIR ages up to ~70 ka. These findings confirm that Xiashu loess accumulated during the Last Glaciation. For samples older than this, the ages increasingly deviate with depth. Fine quartz ages beyond 70 ka are interpreted as underestimates, as previous studies reported that quartz ages >70 ka from various sedimentary origins worldwide may underestimate even if they pass rejection criteria and dose recovery tests. On the other hand, the pIRIR ages are most likely overestimating the true depositional ages as indicated by the results of dose recovery tests, where a 30–60% overestimation of the recovered dose is reported for values larger than ~400 Gy. The overestimation of pIRIR protocols was also confirmed by the results obtained when large beta doses were added on top of the natural accrued dose. Moreover, our dating results suggest that L1/S1 transition (corresponding to MIS 5/4 boundary) occurred much higher in the stratigraphic sequence than may have been interpreted from the magnetic susceptibility enhancement. This inconsistency can be assigned to invalidity of magnetic susceptibility as a chronostratigraphical proxy due to ferrimagnetic minerals dissolution or transformation during paedogenesis processes in this humid subtropical region in the southeastern China.  相似文献   

18.
In this site response study we examined local earthquakes recorded at surface stations of a local seismic network and at a temporary underground seismic array installed in a tunnel underneath the Gran Sasso Massif in Abruzzo (central Italy). This allowed us to compare the seismic site response beneath the mountain and on the surface in similar geological environment (soft rock sites). We applied spectral ratios method on different segments of the seismograms and used different reference spectra in the 1–20 Hz frequency band. We found little or no amplification effects at most of the surface stations whereas site transfer functions evaluated with respect to underground sites show an amplification factor up to 6 in the 1–8 Hz frequency range. Coda spectral ratios estimated at soft rock sites are confirmed as good estimates of shear wave transfer function.  相似文献   

19.
Multiple-centres electron spin resonance (MC-ESR) dating of quartz grains has been commonly applied to fluvial and lacustrine deposits and can provide a precise chronological framework for depositional histories. However, the reliability of this method for quartz grains obtained from sediments of boreholes, which are usually deposited continuously and record information regarding basin evolution and climate change, has not yet been assessed. In this study, we have initially applied the MC-ESR dating method to borehole sediments from the Zhoulao core (ZLC), located in the depocenter of the Jianghan Basin, middle Yangtze River, China. Dating of quartz grains from the ZLC using MC-ESR yields estimated ages that are generally consistent with the established paleomagnetic chronological framework. For Middle Pleistocene samples (i.e., 0.7–0.3 Ma), the Ti–Li centre provides more accurate ages than those of Al centre, which are overestimated. For Early Pleistocene samples (i.e., 2.3–0.8 Ma), both the Al centre and Ti–Li centre give highly consistent estimate ages, indicating that this is a favorable dating range for MC-ESR. Overall, the Al centre shows promise for dating Pliocene samples, whereas the Ti–Li centre is more suitable for Middle-Early Pleistocene (2.3–0.3 Ma) sediments. In addition, the deposition rate of depth <170 m in the ZLC is greater than those of depth >170 m sediments; however, the specific tectonic, climatic, or geomorphic mechanism for this change in sedimentation rate is still unclear.  相似文献   

20.
—The Gran Sasso chain (Central Apennines, Italy) contains one of the largest aquifers of Central Italy. From 1970–1986 the massif was tunnelled through in order to build up a highway and an international underground laboratory for nuclear physics research. These works have strongly modified the hydrogeological situation of the chain, as shown by the decrease in flow rate that occurred in many springs located at the border of the carbonatic structure, along the boundary between the permeable limestone of the massif and the surrounding aquicludes. The analysis of the seismicity (M≥ 3.0) that occurred in the Gran Sasso area from 1956 to 1995 suggests that after the tunnelling works both the number of earthquakes has increased and epicenters have migrated, gathering at the northwestern border zone. The foremost events which occurred in this zone in recent years took place on May 5, 1992 (M = 3.1), August 25, 1992 (M = 3.9) and March 13, 1994 (M = 3.5). The flow rate data of four springs and water level data of an underground karst pool located at the border of the carbonatic structure of the massif show clear anomalies before the occurrence of the quoted earthquakes. Regardless, these anomalies can be explained by the rapid melting of the thick mantle of snow on the Gran Sasso chain, due to sudden increases of mean temperatures. In this paper we present and discuss the possibility that the quoted earthquakes are induced by the irregular variations of the Gran Sasso aquifer, evidenced by the quoted anomalies in the flow rate and water level.  相似文献   

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