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1.
Photogrammetry is a low-cost, nondestructive approach for producing 3-D models of meteorites for the purpose of determining sample bulk density. Coupled with the use of a nondestructive magnetic susceptibility/electrical conductivity field probe, we present measurements for the interrogation of several physical properties, on a set of Antarctic meteorites. Photogrammetry is an effective technique over a range of sample sizes, with meteorite bulk density results that are closely comparable with literature values, determined using Archimedean glass bead or laser scanning techniques. The technique is completely noncontaminating and suitable for the analysis of rare or fragile samples, although there are limitations for analyzing reflective samples. It is also flexible, and, with variations in equipment setup, may be appropriate for samples of a wide range of sizes. X-ray computed tomography analyses of the same meteorite samples yielded slightly different bulk density results, predominantly for samples below 10 g, although the reason for this is unclear. Such analyses are expensive and potentially damaging to certain features of the sample (e.g., organic compounds), but may be useful in expanding the measurements to accommodate an understanding of internal voids within the sample, lending itself to measurement of grain density. Measurements of bulk density are valuable for comparisons with estimates of the bulk densities of asteroids that are suggested as meteorite parent bodies.  相似文献   

2.
We are entering in a new era of space exploration signed by sample return missions. Since the Apollo and Luna Program, the study of extraterrestrial samples in laboratory is gathering an increased interest of the scientific community so that nowadays exploration program of the Solar System is characterized by swelling sample return missions. Beside lunar samples, the NASA Stardust mission was the first successful space mission that on 15 January 2006 brought to Earth solid extraterrestrial samples collected from comet 81P/Wild 2 coma. Grains were collected during cometary fly-by into aerogel and once on Earth have been extracted for laboratory analyses. In the coming two decades many space missions on going or under study will harvest samples from minor bodies. Measurements required for detailed analysis that cannot be performed from a robotic spacecraft, will be carried out on Earth laboratories with the highest analytical accuracy attainable so far. An intriguing objective for the next sample return missions is to understand the nature of organic compounds. Organic compounds found in Stardust grains even if processed to large extend during aerogel capturing are here reported. Major objectives of Marco Polo mission are reported. Various ground-based observational programs within the framework of general characterizations of families and classes, cometary–asteroid transition objects and NEOs with cometary albedo are discussed and linked to sample return mission.  相似文献   

3.
Primitive substances in asteroid and meteorite materials represent a record of early solar system evolution. To allow the study of these materials, they must be collected and transferred to the laboratory. Collection during sample return missions requires an assessment of the size of samples needed. Meteorite falls or finds must be subdivided into appropriate subsamples for analysis by successive generations of scientists. It is essential, therefore, to determine a representative mass or volume at which the collected or allocated sample is representative of the whole. For the first time, we have used a Bayesian statistical approach and a selected meteorite sample, Murchison, to identify a recommended smallest sample mass that can be used without interferences from sampling bias. Enhancing background knowledge to inform sample selection and analysis is an effective means of increasing the probability of obtaining a positive scientific outcome. The influence of the subdivision mechanism when preparing samples for distribution has also been examined. Assuming a similar size distribution of fragments to that of the Murchison meteorite, cubes can be similarly representative as fragments, but at orders of magnitude smaller sizes. We find that: (1) at all defined probabilities (90%, 95%, and 99%), nanometer‐sized particles (where the axes of a three‐dimensional sample are less that a nanometer in length) are never representative of the whole; (2) at the intermediate and highest defined probabilities (95% and 99%), micrometer‐sized particles are never representative of the whole; and (3) for micrometer‐sized samples, the only sample that is representative of the whole is a cube and then only at a 90% probability. The difference between cubes and fragments becomes less important as sample size increases and any >0.5 mm‐sized sample will be representative of the whole with a probability of 99.9%. The results provide guidance for sample return mission planners and curators or advisory boards that must distribute valuable samples for analysis.  相似文献   

4.
A considerable investment has been made by NASA and other space agencies to develop instrumentation suitable for in situ analytical investigation of extra terrestrial bodies including various mass spectrometers (time-of-flight, quadrupole ion trap, quadrupole mass filters, etc.). However, the front-end sample handling that is needed to collect and prepare samples for interrogation by such instrumentation remains underdeveloped. Here we describe a novel approach tailored to the exploration of Mars where ions are created in the ambient atmosphere via laser ablation and then efficiently transported into a mass spectrometer for in situ analysis using an electrodynamic ion funnel. This concept would enable elemental and isotopic analysis of geological samples with the analysis of desorbed organic material a possibility as well. Such an instrument would be suitable for inclusion on all potential missions currently being considered such as the Mid-Range Rover, the Astrobiology Field Laboratory, and Mars Sample Return (i.e., as a sample pre-selection triage instrument), among others.  相似文献   

5.
In this study, we present a method for high precision Δ′17O (Δ′17ORL = ln(δ17O + 1) – λRL ln(δ18O + 1)) analysis of small mass silicate and oxide materials. The analyses were conducted by laser fluorination in combination with gas chromatography and continuous flow isotope ratio monitoring gas spectrometry. We could analyze the oxygen isotope composition of samples down to 1 μg, which corresponded to about 13 nmol O2. The analytical error (we report the 1σ external reproducibility of a single analysis) in δ18O increases with decreasing sample sizes from ~0.2‰ for ~20 μg samples to ~0.9‰ for 1 μg samples. For Δ′17O, we achieved an external reproducibility of 0.04‰ for a sample mass range between 1 and 27 μg. The uncertainty in Δ′17O is smaller than the uncertainty in δ18O due to the correlated errors in δ17O and δ18O. We applied the method to urban micrometeorites, that is, small meteorites (<2 mm) that were sampled from a rooftop in Berlin, Germany. A total of 10 melted micrometeorites (S-type cosmic spherules, masses between 11 and 22 μg) were analyzed. The oxygen isotope compositions are comparable to that of modern Antarctic collections, indicating that the urban micrometeorites sample the same population. No indication for terrestrial weathering had been identified in the studied set of urban micrometeorites making them suitable materials for the study of micrometeorite origins.  相似文献   

6.
Experimental studies related to the sublimation of ice, in bulk or as small particles, alone or mixed with dust similar to that expected on the surface of Mars, are reported. The experiments, a cloud physics particle sublimation model, and a convection model presented by Ingersoll, all indicate a strong dependence of sublimation rate on temperature, and this appears to be the dominant factor, assuming that the relative humidity of the air is fairly low. In addition the rate of loss of water vapour appears to depend primarily on exposed surface area and less on particle size and the total mass of the sample, or the mass of ice in the sample. The 2007/8 Phoenix Scout mission plans to obtain and analyse samples of sub-surface ice from about 70° N on Mars. A concern is that these samples, in the form of ice chips of size about 1 mm diameter, could be prone to sublimation when exposed for prolonged periods (many hours) to a relatively warm and dry atmosphere. Our laboratory simulations confirm that this could be a problem if particles are simply left lying on the surface, but also indicate that samples kept suitably cold and collected together in confined piles will survive long enough for the collection and delivery (to the analysis instruments) procedure to be completed.  相似文献   

7.
We present quantitative analyses of 7 galactic O stars of spectral types from O3 to O6. By means of classical hydrostatic and planeparallel models we find the so-called He and Mass Discrepancies for a number of stars of our sample. We also prove the need of line-blocking for the correct reproduction of these spectra. For stars with effective temperature around 50 000 K and above, there is no possibility of reproducing their spectra with these kind of models. Further analyses with unified models, including sphericity and mass loss, allow us to reproduce even the earliest spectra. They also show that the Mass Discrepancy is not only due to the neglect of sphericity and mass loss in the planeparallel analysis, and give us the mass loss rate of these stars. We find that HD15 570, with a present mass of 100 M⊙, can be the most massive star known in the solar neighbourhood. This revised version was published online in July 2006 with corrections to the Cover Date.  相似文献   

8.
We present a statistical analysis of the largest X-ray survey of nearby spiral galaxies in which diffuse emission has been separated from discrete source contributions. Regression and rank-order correlation analyses are used to compare X-ray properties, such as total, source and diffuse luminosities and diffuse emission temperature, with a variety of physical and multiwavelength properties, such as galaxy mass, type and activity, and optical and infrared luminosity.
The results are discussed in terms of the way in which hot gas and discrete X-ray sources scale with the mass and activity of galaxies, and with the star formation rate. We find that the X-ray properties of starburst galaxies are dependent primarily on their star-forming activity, whilst for more quiescent galaxies, galaxy mass is the more important parameter. One of the most intriguing results is the tight linear scaling between far-infrared and diffuse X-ray luminosity across the sample, even though the hot gas changes from a hydrostatic corona to a free wind across the activity range sampled here.  相似文献   

9.
We report the investigation of cutting methods for Hayabusa samples. The purpose of our study is to explore the possibility of applying multiple analyses to a single particle effectively. We investigated the cutting performance of a blade dicing saw, laser, focused ion beam (FIB), and physical breaking by microindenter. Cutting performance was examined by estimating the aspect ratio of the cut slit, i.e., depth over width of the slit. We also investigated the possible contamination and sample damage by cutting. The result of the investigation shows that we can cut the samples from <50 μm to 500 μm using those methods with aspect ratios from 10 to 20, although they would introduce some contamination or damage to the samples. Our investigations also provide an important basis for the analysis of samples obtained by future sample return missions.  相似文献   

10.
Abstract— The relative abundance of different compositional types and mass frequency distributions are presented for four meteorite samples (the modern falls, Antarctic finds, Yamato finds and Allan Hills Main Icefield finds). The modern falls sample represents continuous collection of a known number of falls over a short timespan, while the Antarctic samples represent a longer timespan and an unknown number of falls. The Allan Hills Main Icefield sample has many desirable collection characteristics indicating it best represents Antarctic meteorites. By retabulating the modern falls to create a sample with characteristics similar to those of the Allan Hills Main Icefield finds, we can directly compare the two. The mass frequency distributions of Antarctic samples exhibit a tail toward the larger sizes and thus differ from that of the modern falls (which approximates a normal curve). In general, normal and power law models prove to be inadequate to explain the observed mass frequency distributions, possibly because they fail to correctly account for atmospheric and collection effects. Non-parametric statistics show that it is unlikely that the two are good samples of a single steady-state meteoritic complex. In addition, there is an excess in numbers of small H chondrites in Allan Hills Main Icefield finds relative to modern falls which is not easy to explain given modern showerfall rates of occurrence. This supports the view that the delivery of meteoritic material to Earth might be variable over the short timescale represented by these samples.  相似文献   

11.
The gas fraction is important for understanding the formation and evolution of galaxies. It is found that there are linear correlations between the atomic-gas-to-stellar mass ratio (G/S) and stellar population properties (age, metallicity and stellar mass) of galaxies. However, only a nearby galaxy sample was used. This work investigates how the correlations change with the redshift limit of galaxies, using three volume limited galaxy samples selected from Sloan Digital Sky Survey (SDSS). It shows that there are linear correlations between the G/S and logarithmic values of stellar age, metallicity and mass, for all galaxy samples. It also shows that the linear correlation between G/S and stellar age is much better than others and possibly can be used in future studies. In addition, the scatters of the fitted correlations are found to increase with upper redshift limit of sample galaxies.  相似文献   

12.
Abstract— The capability of modern methods to characterize ultra‐small samples is well established from analysis of interplanetary dust particles (IDPs), interstellar grains recovered from meteorites, and other materials requiring ultra‐sensitive analytical capabilities. Powerful analytical techniques are available that require, under favorable circumstances, single particles of only a few nanograms for entire suites of fairly comprehensive characterizations. A returned sample of > 1000 particles with total mass of just 1 μg permits comprehensive quantitative geochemical measurements that are impractical to carry out in situ by flight instruments. The main goal of this paper is to describe the state‐of‐the‐art in microanalysis of astromaterials. Given that we can analyze fantastically small quantities of asteroids and comets, etc., we have to ask ourselves, how representative are microscopic samples of bodies that measure a few to many kilometers across? With the Galileo flybys of Gaspra and Ida, it is now recognized that even very small airless bodies have indeed developed a particulate regolith. Acquiring a sample of the bulk regolith, a simple sampling strategy, provides two critical pieces of information about the body. Regolith samples are excellent bulk samples because they normally contain all the key components of the local environment, albeit in particulate form. Furthermore, because this fine fraction dominates remote measurements, regolith samples also provide information about surface alteration processes and are a key link to remote sensing of other bodies. Studies indicate that a statistically significant number of nanogram‐sized particles should be able to characterize the regolith of a primitive asteroid, although the presence of larger components (e.g., chondrules, calcium‐aluminum‐rich inclusions, large crystal fragments, etc.) within even primitive meteorites (e.g., Murchison) points out the limitations of using data obtained from nanogram‐sized samples to characterize entire primitive asteroids. However, the most important asteroidal geological processes have left their mark on the matrix, because this is the finest‐grained portion and therefore most sensitive to chemical and physical changes. Thus, the following information can be learned from this fine grain size fraction alone: (1) mineral paragenesis; (2) regolith processes; (3) bulk composition; (4) conditions of thermal and aqueous alteration (if any); (5) relationships to planets, comets, meteorites (via isotopic analyses, including O); (6) abundance of water and hydrated material; (7) abundance of organics; (8) history of volatile mobility; (9) presence and origin of presolar and/or interstellar material. Most of this information can be obtained even from dust samples from bodies for which nanogram‐sized samples are not truly representative. Future advances in sensitivity and accuracy of laboratory analytical techniques can be expected to enhance the science value of nano‐ to microgram‐sized samples even further. This highlights a key advantage of sample returns—that the most advanced analysis techniques can always be applied in the laboratory and that well‐preserved samples are available for future investigations.  相似文献   

13.
Recent observations indicate that >99% of the small bodies in the solar system reside in its outer reaches—in the Kuiper Belt and Oort Cloud. Kuiper Belt bodies are probably the best‐preserved representatives of the icy planetesimals that dominated the bulk of the solid mass in the early solar system. They likely contain preserved materials inherited from the protosolar cloud, held in cryogenic storage since the formation of the solar system. Despite their importance, they are relatively underrepresented in our extraterrestrial sample collections by many orders of magnitude (~1013 by mass) as compared with the asteroids, represented by meteorites, which are composed of materials that have generally been strongly altered by thermal and aqueous processes. We have only begun to scratch the surface in understanding Kuiper Belt objects, but it is already clear that the very limited samples of them that we have in our laboratories hold the promise of dramatically expanding our understanding of the formation of the solar system. Stardust returned the first samples from a known small solar system body, the Jupiter‐family comet 81P/Wild 2, and, in a separate collector, the first solid samples from the local interstellar medium. The first decade of Stardust research resulted in more than 142 peer‐reviewed publications, including 15 papers in Science. Analyses of these amazing samples continue to yield unexpected discoveries and to raise new questions about the history of the early solar system. We identify nine high‐priority scientific objectives for future Stardust analyses that address important unsolved problems in planetary science.  相似文献   

14.
Organic matter in astromaterials can provide important information for understanding the chemistry of our solar system and the prebiotic conditions of the early Earth. However, once astromaterials reach the Earth's surface, they can be readily contaminated through contact with the Earth's surface as well as during processing and curation. Here, we investigate how typical handling and curation materials interact with meteorite specimens by documenting hydrophobic organic compound contamination in the laboratory environment and on materials that might be used for their collection and storage. We use gas chromatography–mass spectrometry analysis of soluble organic compounds in dichloromethane extracts of these materials to gain insights into what materials and methods are best for the collection and curation of astromaterials. Our results have implications for how extraterrestrial samples—especially those containing significant intrinsic organic matter—are handled and curated to preserve them in their most pristine states. Following recommendations of other researchers in the area of returned sample curation, we advocate for a thorough investigation into the materials used in handling and curation of meteorites to create a contamination baseline to inform soluble organic analyses on astromaterials and enable the discrimination of terrestrial and extraterrestrial compounds.  相似文献   

15.
We study the effect of contamination by interlopers in kinematic samples of galaxy clusters. We demonstrate that without the proper removal of interlopers the inferred parameters of the mass distribution in the cluster are strongly biased towards higher mass and lower concentration. The interlopers are removed using two procedures previously shown to work most efficiently on simulated data. One is based on using the virial mass estimator and calculating the maximum velocity available to cluster members and the other relies on the ratio of the virial and projected mass estimators. We illustrate the performance of the methods in detail using the example of A576, a cluster with a strong uniform background contamination, and compare the case of A576 to 15 other clusters with different degree of contamination. We model the velocity dispersion and kurtosis profiles obtained for the cleaned data samples of these clusters solving the Jeans equations to estimate the mass, concentration and anisotropy parameter. We present the mass–concentration relation for the total sample of 22 clusters.  相似文献   

16.
Abstract– The Planetary Material Sample Curation Facility of JAXA (PMSCF/JAXA) was established in Sagamihara, Kanagawa, Japan, to curate planetary material samples returned from space in conditions of minimum terrestrial contaminants. The performances for the curation of Hayabusa‐returned samples had been checked with a series of comprehensive tests and rehearsals. After the Hayabusa spacecraft had accomplished a round‐trip flight to asteroid 25143 Itokawa and returned its reentry capsule to the Earth in June 2010, the reentry capsule was brought back to the PMSCF/JAXA and was put to a series of processes to extract recovered samples from Itokawa. The particles recovered from the sample catcher were analyzed by electron microscope, given their ID, grouped into four categories, and preserved in dimples on quartz slide glasses. Some fraction of them has been distributed for initial analyses at NASA, and will be distributed for international announcement of opportunity (AO), but a certain fraction of them will be preserved in vacuum for future analyses.  相似文献   

17.
The matrix of the C2-ungrouped Tarda meteorite contains abundant smectite minerals that swell and crumble when exposed to polar liquids, causing the sample to rapidly slake. This phenomenon presents a serious challenge when polishing the meteorite, as common polishing liquids used on carbonaceous chondrites, such as water, ethanol, ethylene glycol, and isopropyl alcohol, are polar and will cause the sample to swell, making it unsuitable for some analyses. Hexane and mineral oil are nonpolar liquids that were found to not induce swelling on highly expansive montmorillonite-clay analog material and were effectively integrated into a polishing procedure for Tarda. Here, we detail a procedure for mounting, cutting, and polishing the Tarda meteorite to prepare a surface that is suitable for a variety of sensitive techniques, such as electron microprobe analysis. This work offers a practical methodology for the preparation of other clay-rich samples, which may include the recently returned Ryugu and Bennu materials.  相似文献   

18.
Using two volume-limited Main galaxy samples of the Sloan Digital Sky Survey Data Release 10 (SDSS DR10), we investigate the dependence of the clustering properties of galaxies on stellar velocity dispersion by cluster analysis. It is found that in the luminous volume-limited Main galaxy sample, except at r=1.2, richer and larger systems can be more easily formed in the large stellar velocity dispersion subsample, while in the faint volume-limited Main galaxy sample, at r≥0.9, an opposite trend is observed. According to statistical analyses of the multiplicity functions, we conclude in two volume-limited Main galaxy samples: small stellar velocity dispersion galaxies preferentially form isolated galaxies, close pairs and small group, while large stellar velocity dispersion galaxies preferentially inhabit the dense groups and clusters. However, we note the difference between two volume-limited Main galaxy samples: in the faint volume-limited Main galaxy sample, at r≥0.9, the small stellar velocity dispersion subsample has a higher proportion of galaxies in superclusters (n≥200) than the large stellar velocity dispersion subsample.  相似文献   

19.
Major and trace element analyses and triple oxygen isotope measurements were performed on 11 individual specimens of Australasian tektites (AAT) with exactly known field positions from Laos. The sample set was dominated by Muong Nong‐type tektites (MNAAT), including separated layers of glass of different appearance and chemistry from four samples. This first larger set of oxygen isotope data of MNAAT revealed the δ18O range 8.7 ≤ δ18O ≤ 11.6‰ on VSMOW2 scale (12 analyses), only slightly wider than the previously reported range for splash‐form AAT. The Δ’17O values of MNAAT (?0.098 ≤ Δ’17O ≤ ?0.069‰; 12 analyses) and splash‐form AAT (?0.080 ≤ Δ’17O ≤ ?0.068‰; three analyses) are all in the range of data typical for terrestrial crustal rocks, with no mass‐independent oxygen isotope fractionation (from impactor or from exchange with atmospheric O2) being observed.  相似文献   

20.
We examine the H I kinematics of the “Bluedisk” ensemble of 48 galaxies selected from the Sloan Digital Sky Survey and observed in H I with the Westerbork Synthesis Radio Telescope. The sample consists of 25 galaxies with a high H I mass fraction and a comparatively large control sample comprising 23 galaxies of comparable stellar mass, stellar mass surface density, redshift, and inclination. By studying the H I velocity fields of these galaxies, we investigate whether there are signatures of ongoing gas accretion: i.e. global asymmetries and indications for warping and kinematical lopsidedness. We find no enhanced kinematical asymmetries between the H I‐rich sample and the control sample galaxies, indicating no significant difference in kinematical signatures such as warping and lopsidedness. Furthermore, we find no difference in position angle and systemic velocity offset with respect to the optical between both sub‐samples. We therefore do not find compelling evidence for enhanced global asymmetry of the H I‐excess galaxies ensemble properties in comparison to the control sample galaxies. (© 2015 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim)  相似文献   

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