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1.
The effect of alumina and water solubility on the development of fabric in orthopyroxene in response to simple shear deformation has been investigated at a pressure of 1.5 GPa and a temperature of 1,100 °C using the D-DIA apparatus. The microstructure observations at these conditions indicate that dislocation glide is the dominant deformation mechanism. In MgSiO3 enstatite and hydrous aluminous enstatite, partial dislocations bounding the stacking faults in [001] glide parallel to the (100) (or) the (100) [001] slip system. Electron backscattered diffraction analysis of anhydrous aluminous enstatite, however, indicates operation of the (010) [001] slip system, and microstructure analysis indicates dislocation movement involving [001] on both (100) and {210} planes. The strong covalent bonding induced by the occupation of M1 and T2 sites by Al could have restricted the glide on (100), activating slip on {210}. The resulting seismic anisotropies (~2 %) in orthopyroxene are weaker compared to olivine (~9.5 %), and reduced anisotropy can be expected if orthopyroxene coexists with olivine. Weak anisotropy observed in stable cratonic regions can be explained by the relatively high abundance of orthopyroxene in these rocks.  相似文献   

2.
Cleaved and mechanically polished surfaces of olivine from peridotite xenoliths from San Carlos, Arizona, were chemically etched using the techniques of Wegner and Christie (1974). Dislocation etch pits are produced on all surface orientations and they tend to be preferentially aligned along the traces of subgrain boundaries, which are approximately parallel to (100), (010), and (001). Shallow channels were also produced on (010) surfaces and represent dislocations near the surface that are etched out along their lengths. The dislocation etch channel loops are often concentric, and emanate from (100) subgrain boundaries, which suggests that dislocation sources are in the boundaries. Data on subgrain misorientation and dislocation line orientation and arguments based on subgrain boundary energy minimization are used to characterize the dislocation structures of the subgrain boundaries. (010) subgrain boundaries are of the twist type, composed of networks of [100] and [001] screw dislocations. Both (100) and (001) subgrain boundaries are tilt walls composed of arrays of edge dislocation with Burgers vectors b=[100] and [001], respectively. The inferred slip systems are {001} 〈100〉, {100} 〈001〉, and {010} 〈100〉 in order of diminishing importance. Exploratory transmission electron microscopy is in accord with these identifications. The flow stresses associated with the development of the subgrain structure are estimated from the densities of free dislocations and from the subgrain dimensions. Inferred stresses range from 35 to 75 bars using the free dislocation densities and 20 to 100 bars using the subgrain sizes.  相似文献   

3.
The microstructure and texture in cordierites of a moldanubian gneiss from the Bohemian Massif has been analysed by transmission electron microscopy (TEM) and universal stage in order to get information on the deformation mechanisms and textural development of this rock-forming mineral. Deformation may have taken place at temperatures between about 500° C and 630° C and pressures smaller than about 3 kb. The elongated cordierite xenoblasts show a typical dislocation creep microstructure consisting of subgrain boundaries and free dislocations. The dislocations have [001], [010] and 1/2<110> Burgers vectors. [001] dislocations often have pure screw and edge character the latter type being climb-dissociated on (001). Among the dislocations reactions are common. The main subgrain boundaries observed are (010)[001], {110}[001] and (001)[010] tilt boundaries. Burgers vectors and dislocation line directions reveal (100)[001], (010)[001], (100)[010], {110} 1/2<110> and (001)1/2<110> as activated slip systems. The crystallographic preferred orientation (here referred to as texture) consists of a [001] maximum in the foliation parallel to the mineral lineation. [100] and [010] maxima are perpendicular to it within and normal to the foliation, respectively, with a girdle tendency normal to the lineation. The texture may be explained by simple shear deformation on the {hkO}[001] slip systems with preference of (010)[001].  相似文献   

4.
We have used a first-principle approach based on the calculation of generalised stacking faults (GSF) to study the influence of pressure on the mechanical properties of forsterite. Six cases corresponding to [100] glide over (010), (021) and (001), and [001] glide over (100), (010) and (110) have been considered. The relaxed energy barriers associated with plastic shear have been calculated by constraining the Si atoms to move perpendicular to the fault plane and allowing Mg and O atoms to move in every direction. These conditions, which preserve dilations as a relaxation process, introduce Si–O tetrahedral tilting as an additional relaxation mechanism. Relaxed GSF show little plastic anisotropy of [100] glide over different planes and confirms that [001] glide is intrinsically easier than [100] glide. The GSF are affected by the application of a 10 GPa confining pressure with a different response for each slip system that cannot be explained by sole elastic effect. In particular, [100](010) is found to harden significantly under pressure compared to [001](010). Our results give the first theoretical framework to understand the pressure-induced change of dominant slip systems observed by Couvy et al. (in Eur J Mineral 16(6):877–889, 2004) and P. Raterron et al. (in GRL, submitted). It appears necessary to account for the influence of pressure on the mechanical properties of silicates in the context of the deep Earth.  相似文献   

5.
The microstructures and fabrics of naturally deformed orthopyroxenites from the Giles Complex, central Australia are described in some detail. Coarse grained enstatite is deformed and recrystallised where it is incorporated in planar gneissic (mylonite) zones which show a gradation in strain from their margins inwards. Deformation takes place by slip on (100) [001] to produce regular lattice bending and kinking, and recrystallisation takes place preferentially along grain boundaries and kink band boundaries (KBB's). The microstructures and preferred orientation of recrystallised grains along KBB's are interpreted in terms of possible nucleation mechanisms, and both bulge nucleation (Bailey and Hirsch, 1962) and subgrain coalescence (Hu, 1963) are likely contributors. Electron microprobe analyses have indicated a small compositional difference between new (recrystallised) and host (deformed) grains, which is related to the nucleation mechanism. The total preferred orientation patterns for host and new grains are discussed with special reference to previous measurements and interpretations.  相似文献   

6.
As uniaxial compression tests of α spodumene LiAlSi2O6 at various temperatures and strain rates systematically led to brittle fracture, room-temperature microindentations have been performed with a view to characterizing the glide systems. Transmission electron microscopy (TEM) investigations show that only the [010] (100) glide system is activated. The resulting dislocations are widely dissociated (up to 3,000 Å) following the reaction [010]→[0 1/2 1/6]+[0 1/2 \(\bar 1\) /6]. In contrast, in naturally deformed spodumene the activated glide systems found in TEM studies are [001] {110} and 1/2〈110〉{1 \(\bar 1\) 0} and the corresponding dislocations are not dissociated. Such a difference in mechanical behaviour is interpreted in considering the necessary impingement of the oxygen atoms during dislocation glide. It is shown that only the dissociated b dislocations can glide with a moderate lattice friction at room temperature. The proposed model is supported by the first exploratory deformation runs performed under confining pressure.  相似文献   

7.
Dislocations decorated by hematite and magnetite have been observed optically in the olivine grains of undeformed or highly annealed peridotite xenoliths from Hawaii and Baja California ( 5 × 105 cm–2). The observed structures include loops, low-angle boundaries, and structures produced by multiple cross-glide of [100] screws. Loops are almost invariably parallel to (001). Simple arrays of parallel dislocations lie predominantly in (100), (010) and (001) with dislocation lines subparallel to low-index directions. [100] screws pinned to (100) boundaries are frequently seen to bow out on (001). Preliminary electron petrography has confirmed that all dislocations are decorated.  相似文献   

8.
藏南变质橄榄岩的橄榄石组构可划分为三个主要类型:[100]、[010]和[001]组构。橄榄石[100]组构反映洋壳下部—上地幔上部的高温粘性流变和高温塑性流变,橄榄石[010]和[001]组构基本上是构造侵位阶段陆壳中低温塑性流变结果。变质橄榄岩中橄榄石组构转化具有明显的规律性,在岩体变形过程中,总的显示由高温的[100]组构逐渐转化为低温的[001]、[010]组构。高温塑性流变组构影响和制约低温塑性流变组构的发育,叠加变形有利于橄榄石[100]极密的加强和[100]组构向[010]、[001]组构的转化。  相似文献   

9.
A San Carlos olivine polycrystal has been deformed under uppermost mantle conditions, by compression at 900 °C, at a strain rate of 1.1 × 10?5 s?1, under a confining pressure of 300 MPa, using the Paterson press. Transmission electron tomography of dislocations has been performed by scanning transmission electron microscopy, by conventional transmission electron microscopy using the weak-beam dark-field technique, associated with precession or not, in order to determine the glide planes of [001] screw dislocations. This recent technique is the most suitable one since most [001] dislocations exhibit straight screw segments due to the high lattice friction on this character at low temperature. We find that [001] dislocations glide in (100), (010) and {110} as already reported, but also more unexpectedly in {120} and {130}. We show that at 900 °C, [001] {110} glide is dominant in polycrystals. We have, however, noted and characterized numerous cross-slip events in the specimen.  相似文献   

10.
This paper reports the results of optical and electron microscopic investigations of mantle olivine samples with H2O contents of tens-hundreds ppm weight. Samples were obtained from the xenoliths and xenocrysts of the Udachnaya pipe. At the scale of optical microscope magnification, a peculiar banded microstructure was observed in thin sections prepared parallel to the olivine (010) plane. It is formed by cross-hatched bands parallel to four crystallographic directions of the olivine structure: [100], [001], [101], and [−101]. At the scale of electron optical magnifications, the banded microstructure is observed as nanometer-sized heterogeneities of various types which are related to olivine deformation: (a) planar defects parallel to (100) and (001) corresponding to the (100)[010] and (001)[100] dislocation glide systems, respectively; they are occasionally transformed into lamellae or decorated by nanoinclusions; and (b) nanometer-sized heterogeneities formed by nanoinclusion arrays not related to planar defects and oriented along the same directions of the olivine structure as the optically visible bands. The deformation structures are decorated by coupled point OH-bearing defects, which were initially present in the olivine. The crystallographically oriented arrays of nanoinclusions of high-pressure hydrous silicates are considered as a result of olivine deprotonization (elimination of OH-bearing defects from the olivine structure) in the zones of previous deformation compression in the crystal. Light refraction effects on the nanoinclusions make these zones optically visible and produce the banded microstructure, which is a consequence of previous deformation.  相似文献   

11.
Naturally deformed clinoamphiboles from the Selbu-Tydal and Forsbäck-Tärnaby areas of the Scandinavian Caledonides exhibit a well defined subgrain microstructure. From a transmission electron microscopy study (TEM), the subgrain boundaries are shown to consist of arrays of positive and negative screw dislocations with Burgers vector . Locally expanded loops are present having long screw segments. The subgrain boundaries are parallel to rational crystallographic planes of the type (hk0). The density of isolated dislocations within the subgrains is low. In addition planar defect structures parallel to (010) and bounded by screw dislocations with are observed. Based on metamorphic criteria the PT values at the time of the amphibole growth have been estimated at 450°–600°C and 4–6 kbar, and these represent maximum conditions for the deformation. The present results indicate that slip on (hk0) [001] is an operative deformation mechanism in naturally deformed clinoamphiboles.  相似文献   

12.
We present here a numerical modelling study of dislocations in perovskite CaTiO3. The dislocation core structures and properties are calculated through the Peierls–Nabarro model using the generalized stacking fault (GSF) results as a starting model. The GSF are determined from first-principles calculations using the VASP code. The dislocation properties such as collinear, planar core spreading and Peierls stresses are determined for the following slip systems: [100](010), [100](001), [010](100), [010](001), [001](100), [001](010), and All dislocations exhibit lattice friction, but glide appears to be easier for [100](010) and [010](100). [001](010) and [001](100) exhibit collinear dissociation. Comparing Peierls stresses among tausonite (SrTiO3), perovskite (CaTiO3) and MgSiO3 perovskite demonstrates the strong influence of orthorhombic distortions on lattice friction. However, and despite some quantitative differences, CaTiO3 appears to be a satisfactory analogue material for MgSiO3 perovskite as far as dislocation glide is concerned.  相似文献   

13.
A set of sanidine single crystals were previously deformed at 700° C in a Griggs triaxial press with different crystallographic orientations of the core so as to induce dislocation glide of different slip systems respectively. Deformed crystals have been studied by transmission electron microscopy (TEM) and the activated slip systems have been characterized for two orientations. (010)[001] and (001)1/2[ \(\overline 1 \) 10] systems expected for one orientation (main stress nearly parallel to [012]) are observed, whereas the (001)[100] system expected for the other orientation (main stress nearly parallel to [101]) is never observed. In the latter specimen the deformation is rather difficult and occurs through unexpected systems characterized as (110)1/2[1 \(\overline 1 \) 2] and (1 \(\overline 1 \) 1)1/2[110]. In all the samples studied the deformation is heterogeneous, exhibiting dislocation configurations related to temperature variations.  相似文献   

14.
The core structures of dislocations in diopside have been calculated within the Peierls model, which assumes a planar core. 1/2<110> dislocations can dissociate into two collinear partial dislocations. We show that [001] glide is very difficult in (010) and that a non-collinear dissociation of [001](100) (modelled within a Peierls–Nabarro–Galerkin approach) makes glide equally easy in (100) and {110}. A widely spread core structure corresponding to a low lattice friction has been found for [100](010) and [010](100) dislocations which is not supported by mechanical data and, together with TEM observations, suggests that another, probably non-planar core structure is possible for these dislocations.  相似文献   

15.
Diopside twins mechanically on two planes, (100) and (001), and the associated macroscopic twinning strains are identical (Raleigh and Talbot, 1967). An analysis based on crystal structural arguments predicts that both twin mechanisms involve shearing of the (100) octahedral layers (containing Ca2+, Mg2+ and Fe2+ ions) by a magnitude of c/2. Small adjustments or shuffles occur in the adjacent layers containing the [SiO4]4? tetrahedral chains. While the (100) twins are conventional with shear parallel to the composition plane, this analysis predicts that (001) twins form by a mechanism closely related to kinking. A polycrystalline diopside specimen was compressed 8% at a temperature of 400° C, a pressure of 16 kilobars, and a compressive strain rate of about 10?4/s. Transmission electron microscopy on this specimen has revealed four basic lamellar features:
  1. (100) mechanical twin lamellae;
  2. (100) glide bands containing unit dislocations;
  3. (001) twin lamellae;
  4. (101) lamellar features, not as yet identified.
The (001) twins often contain remnant (100) lamellae of untwinned host. Twinning dislocations occur in these (100) lamellae and in the (001) twin boundaries with very high densities. Diffraction contrast experiments indicate that the twinning dislocations associated with both twin laws glide on (100) with Burgers vector b=X [001] where X is probably equal to 1/2 on the basis of the structural analysis. Parallels are drawn between mechanical twinning in clinopyroxenes and clinoamphiboles. The exclusive natural occurrence of basal twins in shock-loaded clinopyroxenes and of analogous ( \(\bar 1\) 01) twins in clinoamphiboles is given a simple explanation in terms of the relative difficulty of the “kinking” mechanism as compared to direct glide parallel to the composition plane.  相似文献   

16.
Dunite samples have been deformed non-coaxially at high temperatures and pressures. In samples which were deformed by translation glide on {Okl}[100], olivine [100] = Z-axes rotated toward the maximum extensile-strain axis. In samples which were partly or completely recrystallized syntectonically the new olivine grains attained preferred orientations with [010] = X and [100] = Z parallel to the maximum and least principal compressive stress axes, respectively. These results may be used for kinematic and dynamic analysis of naturally deformed dunites and peridotites.  相似文献   

17.
We have performed detailed transmission electron microscope on most of the deformed synthetic dunite specimens prepared in the study by Zeuch and Green (1984). We have identified three basic types of sub-boundaries, simple tilt walls in (100) and (001). composed by b = [100] and b = [001] edge dislocations, respectively, and twist boundaries in (010) composed of b = [100] and b = [001] screws. We have also observed more complex, asymmetric lilt boundaries in (100) and (001). Like the (010) twist boundaries, these asymmetric tilt walls are common only at the highest temperatures and lowest strain rates. Subgrain development is extensive at the higher temperatures and lower strain rates, and subgrains are composed of the above-mentioned three types of sub-boundaries; edge components in (100) and (001) ire “knitted” to screw components in (010) as described by Kirby and Wegner (1978) for naturally deformed olivine. In many areas of the samples which we studied, subgrain development is not observed, but parallel arrays of tilt boundaries of one type or the other are present. At higher temperatures and lower strain rates. “(100) organization” (Durham et al., 1977) is common; this structure consists of parallel arrays of (100) tilt boundaries with b = [100] screws connecting the sub-boundaries. At lower temperatures we have observed an analogous arrangement of (001) sub-boundaries and b = [001] screws, which we refer to as “(001) organization”. Under all experimental conditions, dislocations with b = [100] and b = [001] are present in approximately equal numbers. However, the two types of dislocations also have distinctly different geometries under all test conditions. We suggest that the transition from slip parallel to [001] to slip parallel to [100] with increasing temperature, which has been reported in earlier studies may also depend upon water content. The substructures which we observe are virtually identical to those seen in many naturally deformed peridolites. and we conclude that the mechanisms involved in both natural and laboratory deformation of olivine polycrystals are similar. On the other hand, the substructures reported here are very different from those observed in experimentally deformed olivine single crystals. It seems likely that these substructural differences reflect fundamental differences in the behavior oh single crystals and polycrystals. which are in turn reflected in different measured creep strengths.  相似文献   

18.
Automated electron backscattered diffraction (EBSD) was applied using a scanning electron microscope to obtain lattice preferred orientation (LPO) data for olivine in garnet peridotites of the Central Alps. As a reference frame, the LPOs of enstatite were also investigated. In the garnet peridotite at Cima di Gagnone (CDG), a weak foliation carrying a distinct lineation is present. The lineation is characterized by elongated enstatite, olivine and poikiloblastic garnet. Olivine shows a very unusual LPO with [100] normal to foliation and [001] parallel to lineation. Achsenverteilungsanalyse (AVA) maps demonstrate that [001] of olivine grains corresponds quite well to their maximum length axes which are preferentially parallel to the lineation. Numerous planar hydrous defects within (001) planes of olivine are marked by palisades of ilmenite rods and show a preferred orientation normal to lineation. Calculated P-wave velocities for CDG are fastest (8.32 km sу) normal to foliation with a relatively low anisotropy (2.9%). Compared to mantle peridotites with the usual (010)[100] LPO where the fastest Vp direction is towards the lineation, the relationship between flow geometry and seismic anisotropy is significantly different at CDG. Several mechanisms for the formation of the LPO type at CDG are considered, with glide possible on (100)[001] of olivine. On the basis of field data as well as petrographic and petrologic evidence, it has been demonstrated that the CDG garnet peridotite formed by prograde metamorphism from a hydrous protolith at pressures and temperatures of about 3.0 GPa and 750 °C, respectively. The CDG LPO is interpreted to have formed during hydrous subduction zone metamorphism. The same interpretation may hold for the previously investigated olivine LPO at Alpe Arami, which is similar to that at the nearby CDG. The observed anomalous LPO is no proof for ultradeep (>3.0 GPa) conditions.  相似文献   

19.
Detailed electron microscope and microstructural analysis of two ultrahigh temperature felsic granulites from Tonagh Island, Napier Complex, Antarctica show deformation microstructures produced at  1000 °C at 8–10 kbar. High temperature orthopyroxene (Al 7 wt.% and  11 wt.%), exhibits crystallographic preferred orientation (CPO) and frequent subgrain boundaries which point to dislocation creep as the dominating deformation mechanism within opx. Two different main slip systems are observed: in opx bands with exclusively opx grains containing subgrain boundaries with traces parallel to [010] and a strong coupling of low angle misorientations (2.5°–5°) with rotation axes parallel to [010] the dominating slip system is (100)[001]. Isolated opx grains and grain clusters of 2–5 grains embedded in a qtz–fsp matrix show an additional slip system of (010)[001]. The latter slip system is harder to activate. We suggest that differences in the activation of these slip systems is a result of higher differential stresses imposed onto the isolated opx grains and grain clusters. In contrast to opx, large qtz grains (up to 200 μm) show random crystallographic orientation. This together with their elongate and cuspate shape and the lack of systematic in the rotation axes associated with the subgrain boundaries is consistent with diffusion creep as the primary deformation mechanism in quartz.Our first time detailed microstructural observations of ultrahigh temperature and medium to high pressure granulites and their interpretation in terms of active deformation mechanisms give some insight into the type of rheology that can be expect at lower crustal conditions. If qtz is the mineral phase governing the rock rheology, Newtonian flow behaviour is expected and only low differential stress can be supported. However, if the stress supporting mineral phase is opx, the flow law resulting from dislocation creep will govern the rheology of the rock unit; hence, an exponential relationship between stress and strain rate is to be expected.  相似文献   

20.
Two crystals of natural chalcopyrite, CuFeS2, experimentally deformed at 200° C have been studied by means of transmission electron microscopy (TEM). The activated glide planes are (001) and {112}. The dislocations in (001) have the Burgers vector [110] and a predominating edge character. They are split into two colinear partials b=1/2[110] and can cross split into {112}. The dislocations in {112} consist of straight segments along low index lattice lines. They are often arranged in dipoles generating trails of loops. Few dislocations with b=1/2[ \(\overline {11} \) 1] and [1 \(\bar 1\) 0] are present and dislocations with b=[0 \(\bar 2\) 1] occur in low angle subgrain boundaries. From weak beam contrasts it is presumed that most of the dislocations gliding in {112} have b=1/2〈3 \(\overline {11} \) 〉. They are dissociated into up to four partials. Microtwins and different types of stacking faults in {112} also occur. Models of the dissociation of dislocations are discussed.  相似文献   

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