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晚第四纪细颗粒河流阶地沉积物的准确定年是当前光释光测年研究中的一个难点。利用简单多片再生法(SMAR)、单片再生法(SAR)等对新疆西南天山喀什前陆盆地明尧勒背斜喀浪勾律克河阶地沉积物样品的细颗粒石英光释光(BLSL)信号、混合矿物红外释光信号(IRSL)和红外后蓝光释光信号([Post-IR]OSL)进行测量。通过对比同一样品的细颗粒石英BLSL、混合矿物IRSL和[Post-IR]OSL的等效剂量值,认为细颗粒石英简单多片再生法是河流阶地沉积物释光测年最为适用的方法之一。对于细颗粒混合矿物而言,由于长石矿物的异常衰退,对于等效剂量De>70Gy的样品,其IRSL等效剂量值均偏小;其[Post-IR]OSL等效剂量值仍需慎重使用。通过对同一样品细颗粒石英多个测片的单片再生法等效剂量值分布以及简单多片再生法多个测片校正后天然释光信号强度的一致性判断,认为样品LEDL03-87q,LEDL03-86q和LEDL04-54q在沉积时的光晒退是不均匀的,采用最小等效剂量组分来计算沉积年龄 相似文献
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海原断裂带刺儿沟剖面烘烤次生黄土的光释光测年及其地质意义 总被引：1，自引：2，他引：1
选择海原活动断裂带刺儿沟剖面2个烘烤次生黄土样品LEDL0588H和LEDL0365的细颗粒石英,采用改进后的单测片再生法(SAR)和简单多测片再生剂量法(SMAR)进行了一系列实验研究。2个样品细颗粒石英的光释光信号均以快速组分为主,其等效剂量(DE)的预热坪实验表明,在180～260℃的预热温度范围内均能获得基本一致的DE值。SAR法测量不同预热温度下的释光感量变化、剂量恢复实验和LN/TN比值的关系以及SMAR法测量中LN/TN比值与预热温度的关系的研究表明,文中所采用的流程能有效地校正测量过程中释光信号感量变化。2种方法均适用于采自不同层位的2个烘烤样品细颗粒石英的OSL测年,并获得了非常接近的OSL年龄。2个样品最后一次被烘烤的时间可能代表的是同一时期的人类活动 相似文献
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水成相沉积物细颗粒石英光释光综合生长曲线的建立与应用 总被引：1，自引：0，他引：1
选择中国不同地区的冲洪积相等水成相沉积物样品,根据其简单多片再生法(SMAR)测量数据建立了细颗粒石英光释光信号的综合生长曲线(Standardised growth curves,SGC)。对未知年龄的水成相沉积物细颗粒石英样品,通过测量其天然光释光信号和试验剂量响应信号,并利用上述SGC方程可计算出其等效剂量值。将此值与简单多片再生法(SMAR)测量结果相比较,统计得出对于天然等效剂量为12~65Gy的样品,其误差可达19%;对于天然剂量>65Gy的样品,其误差更大;对于等效剂量<12Gy的样品,最大误差也达25%。实验表明,应用这个SGC估计未知年龄样品的等效剂量值范围,再对样品采用简单多片再生法(或单片再生法)进一步测量,可大大节省测量时间 相似文献
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2008年5月12日四川汶川发生MS8.0大地震,形成了200多km长的地震地表破裂带。破裂带的古地震研究对于认识龙门山断裂带的活动习性和大地震的发生规律具有重要的理论和现实意义。文中用光释光(OSL)测年中的校正感量简单多片再生法(SMAR),对映秀-北川地震地表破裂带擂鼓探槽样品进行了光释光测年,并对探槽中含有的炭屑进行了AMS14C测年。样品的光释光年龄和校正的AMS14C年龄吻合,该地区与汶川地震类似规模的上一次古地震事件发生在距今约(2.1±0.2)ka至(1.1±0.2)ka间 相似文献
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等效剂量预热温度坪实验是光释光(OSL)测年中确定预热温度的常用手段,一般选择坪区温度作为OSL测年的预热温度。对于黄土细颗粒石英,无论采用单片再生法(SAR)还是简单多片再生法(SMAR),以10s为预热时间,其天然和再生剂量预热温度坪区间均为250～280℃,试验剂量的预热温度分布较广,如180～260℃。常规等效剂量预热温度坪实验需要耗费较长的实验室时间。通过对SMAR法测试数据的再分析发现,天然与再生剂量OSL信号校正强度的比值(N/R)随预热温度的变化与常规等效剂量坪实验中等效剂量随预热温度的变化有着相似的趋势,这样,N/R预热温度坪就可作为黄土样品细颗粒石英等效剂量预热温度坪的替代,为实验室OSL测年确定预热温度提供一个简捷途径 相似文献
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通过对滹沱河冲洪积物、阳原盆地湖相地层细颗粒石英天然热转移光释光(TT-OSL)信号测量、回授剂量恢复测试以及简单多片光释光(OSL)与回授光释光(Re-OSL)测量结果对比等,探讨了细颗粒石英回授光释光在水成沉积物测年中应用的可能性。结果表明,冲积样品回授光释光信号没有随深度逐步增加的规律,而湖相样品热转移光释光信号随深度逐渐增大;冲洪积物细颗粒石英样品回授光释光不能得出剂量值,剂量不能恢复;而湖相样品回授实验室附加剂量与测得的剂量在2%的误差范围内一致,说明回授光释光测年在一定时间范围内对于湖相样品测年是可行的;细颗粒石英回授释光在测量>10万a的湖相样品年龄方面具有很大的潜力 相似文献
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In the quest for extending the upper age limit of optically stimulated luminescence (OSL) dating of quartz, it was shown that violet stimulated luminescence (VSL) may be a promising candidate. However, difficulties in the application of the single aliquot regenerative dose (SAR) protocol for VSL has been reported in previous studies. In this study, a set of experiments was carried out to investigate the behaviour of the VSL signal under different measurement conditions with the aim to improve the SAR VSL protocol in terms of passing the procedural tests of the SAR protocol, i.e., recycling ratio, recuperation and dose recovery. The validity of an optimised SAR protocol was then evaluated on four coarse-grained quartz samples from Sardinia, for which previously reported OSL and post-IR IRSL ages are available. Our result showed that all measured aliquots meet the recuperation, recycling ratio and dose recovery criteria, indicating that the proposed protocol is suitable for the studied samples. The obtained VSL and reference ages agree within uncertainty (2σ) for most of the samples except one sample with a largest expected equivalent dose of ∼320 Gy, for which the VSL significantly (∼50%) underestimates despite satisfactory dose recovery result. This underestimation is most likely due to trapping sensitivity change between the natural and all subsequent regenerated VSL signals induced by the first preheating in the SAR procedure, which is likely dose dependent. To minimise sensitivity change, the sensitivity-corrected multiple aliquot regenerative dose (SC-MAR) protocol was applied. The SC-MAR protocol yields VSL ages in agreement with reference ages for two samples (1σ); the other two samples show overestimation. We show that the observed age overestimation can be explained by incomplete resetting of the natural signal after 7 days SOL2 exposure used for the SC-MAR procedure. Bleaching experiments confirm variable bleaching behaviour among different samples. However, it is unclear whether this different bleaching behaviour arises from measuring samples with different bleaching histories, mineralogical compositions, or VSL source trap properties. 相似文献
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Similar to the loess in the Chinese Loess Plateau (CLP), the loess deposits in the Ili basin of Central Asia arid area play an important role in understanding the climate and environmental changes. However, in contrast to the intensively investigated loess deposits in the CLP, the Ili loess is still insufficiently known and poorly understood. The geochronology study of the Ili loess remains controversial. In order to examine the potential of optically stimulated luminescence (OSL) dating for the Ili loess, we carry out a combined luminescence and radiocarbon dating study on a 6.9 m loess section in the south margin of the Ili basin. Polymineral fine grains were investigated by post infrared (IR) OSL using a Multiple-Aliquot Regenerative-dose (MAR) protocol. Radiocarbon dating of organic carbon were carried in a 3 Megavolt (MV) multi-element Accelerator Mass Spectrometry (AMS). The results indicate that the OSL ages are in agreement with the observed stratigraphy in the field, which is well correlated with that of the CLP, but the AMS 14C ages are much younger than the OSL and assumed stratigraphical ages. Thus, the OSL dating technique may provide an absolute chronology in this loess section. Further methodological approaches and more samples analysis will lead to the improvement of this chronology for high-resolution paleoclimatic interpretation. 相似文献
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Dating of quartz by optically stimulated luminescence (OSL) has been revolutionized with introduction of the test dose (TD) in development of a measurement sequence known as the single-aliquot regenerative-dose (SAR), whereby a valid sensitivity correction for the luminescence signal is provided in the measurement cycle. However, the size of the TD used in the SAR protocol remains controversial. Previous studies show that the TD has little effect on the equivalent dose (De) for young samples in luminescence dating in which the applicability of different deposits varies greatly in different regions. However, detailed studies are lacking on how TD size affects SAR–OSL results of samples with a relatively high De range. In this study, typical loess samples with high De values (∼60 Gy–∼250 Gy) from the eastern Tibetan Plateau were selected to investigate the effects of variation in TD size on the quartz SAR–OSL protocol. Dose recovery tests show that a known dose could be recovered successfully by applying different TDs. Test dose size has an effect on shapes of regenerated dose–response curves (DRCs) and has different influences on Des and characteristic saturation doses for quartz samples with a high dose range. A TD size of 20%–30% De is a good compromise for Tibetan loess with De of ∼60–120 Gy in the quartz SAR protocol, and a TD size larger than 30% should be considered for samples with a larger De. The results of this study highlight the importance of TD size in the SAR–OSL protocol for quartz samples with a high dose range. 相似文献
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XianJiao Ou LiuBing Xu ZhongPing Lai Hao Long Zhong He QiShun Fan ShangZhe Zhou 《Quaternary Geochronology》2010,5(2-3):257-262
Optically stimulated luminescence (OSL) dating methods have been widely applied in Quaternary glaciology. However, glacigenic deposits are considered in general as problematic for OSL dating, mainly because they are transported shorter distances prior to burial and are usually partially bleached. Thus, most researchers choose glaciofluvial and glaciolacustrine sediments (with relatively longer transportation times) for OSL dating when constraining the age of glaciation. In this study, four samples were collected from a lateral moraine series at Zhuqing Village, northern margin of Queer Shan Mountain, eastern Tibetan Plateau, in order to investigate the applicability of OSL dating for morainic deposits. Quartz grains (38–63 μm) were extracted and measured using single aliquot regenerative-dose (SAR) protocol. Internal checks and dose recovery test show that the SAR protocol is appropriate for equivalent dose (De) determination. The effect of thermal transfer is small for all samples and the recycling ratio for each individual sample is close to unity. The symmetry in the De distributions indicates that quartz grains were well-bleached prior to burial. OSL ages show good agreement with geomorphological and field investigations, and are also concordant with an independent ESR age. It is concluded that: (a) the morainic deposits in Zhuqing were well-bleached and suitable for OSL dating; (b) SAR protocol can be applied to morainic deposits for samples under study. 相似文献
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Sally E. Lowick Frank Preusser Roberta Pini Cesare Ravazzi 《Quaternary Geochronology》2010,5(5):583-590
Palynostratigraphical records have been used to understand the response of vegetation to climate change, and benefit from independent dating to ensure a robust correlation with global climate and sea-level change. In order to constrain the pollen chronology of a long sedimentary core taken at Azzano Decimo in the Friulian foreland of northeastern Italy, optically stimulated luminescence (OSL) has been applied to fine grain quartz. The samples meet all the standard performance criteria set to test the reliability of the single-aliquot regenerative-dose (SAR) protocol, and still show increasing dose response at 500 Gy. OSL ages are in good agreement with radiocarbon dating and the pollen interpretation down to 70 ka, and with De values of ～140 Gy, but below this point, they display an increasing age underestimation towards the Eemian and beyond. The comparison of De values measured using both a SAR and single-aliquot regeneration and added-dose (SARA) protocol, confirmed that both were successfully correcting for sensitivity changes in the quartz during measurement of the burial dose, and this was not the reason for the age underestimation. The quartz OSL dose response curve for all samples is best described by a saturating exponential plus linear (SEPL) function. Although all underestimated ages are derived from De values that fall on the high dose linear region of this curve, it is unclear if this is the cause of the underestimation. 相似文献
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The reliability of single-grain optically stimulated luminescence (OSL) dating of young (<500 years old) samples is assessed by examining the results of 166 single-grain OSL analyses of Australian alluvial, lacustrine, estuarine, coastal and marine sediment samples. All samples have been analysed using the modified SAR protocol of Olley et al. [2004b. Optical dating of Holocene sediments from a variety of geomorphic settings using single grains of quartz. Geomorphology 60, 337–358], with burial doses (Db) calculated by fitting a single Gaussian curve to the peak of a multi-Gaussian summed probability distribution (PDFGaussian). The near-equivalence of this approach to currently accepted methods of palaeodose estimation – namely the minimum age and central age models of Galbraith et al. [1999. Optical dating of single and multiple grains of quartz from Jinmium rock shelter, northern Australia: part I, experimental design and statistical models. Archaeometry 41, 339–364] – is demonstrated. Considered as a whole, OSL ages calculated using the PDFGaussian Db determination method are consistent with other chronometric, geomorphological, botanical and historical indicators of depositional age, while four alternative (previously published) methods are generally less reliable when applied to the samples analysed here. The single-grain data from 12 samples of known age (reported by Olley et al. [2004b. Optical dating of Holocene sediments from a variety of geomorphic settings using single grains of quartz. Geomorphology 60, 337–358]) are re-analysed using the PDFGaussian approach, with all but one yielding a Db consistent with the independently known age. Examples of luminescence data (dose recovery tests, preheat plateaux, continuous-wave and linear-modulated OSL, growth curves, single-grain dose distributions) are provided that together indicate the suitability of Australian quartz for dating young sediments. 相似文献
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Raised beach sand deposits along the southeastern coast of Norway were dated by optical (OSL) and infrared stimulated luminescence (IRSL) and the quartz and K-feldspar luminescence characteristics were described. Due to the poor quartz luminescence characteristics, only a limited number of samples were suitable for OSL dating. More promising are the K-feldspar extracts, with typical K-feldspar luminescence characteristics and no sign of fading. For equivalent dose (De) determination, sand-size quartz and feldspar extracts were used, applying a single aliquot regenerative (SAR) protocol. Both, OSL and IRSL De estimates show a wide distribution, unexpected for beach deposits. The calculated OSL and IRSL age estimates were generally in good agreement and the correctness of the ages was confirmed by independent age control. Because only a limited number of the quartz samples were suitable for OSL dating, IRSL dating of the K-feldspar represents an alternative to OSL quartz dating. 相似文献
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The loess deposits surrounding the high mountainous regions of Central Asia play an important role in understanding environmental changes in Eurasia on orbital and sub-orbital timescales. However, problems with dating Central Asian loess have limited the interpretation of climatic and environmental data, especially on sub-orbital timescales. We selected a controversial loess section, Zeketai (ZKT, with a thickness of 23 m), in the Yili basin in Xinjiang Province in western China, to establish a detailed and systematic Optically Stimulated Luminescence (OSL) chronology. Quartz grains of 38–63 μm were isolated from 15 samples and the single-aliquot regenerative-dose (SAR) protocol was employed for De determination. OSL ages are in stratigraphic order and range from 13.8 ± 1 to 72 ± 6 ka, suggesting continuous loess accumulation during the last glaciation. We compared these dating results with that of the previously published fine-grain sized quartz (4–11 μm) using simplified multiple aliquot regenerative-dose (SMAR) protocol, and with the previous published radiocarbon dating (14C) ages on snail shells. With the exception of three young samples from the upper 6 m of the section, the SMAR dating results are basically consistent with the results using the SAR protocol. Both the SMAR and SAR OSL ages are consistently older than the 14C ages, and the radiocarbon date results should be used with caution since they appear to have been underestimated. 相似文献