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1.
Seven samples were collected from sediments at the Palaeolithic site of Jeongokri, Korea, known for the first discovery of Acheulian-like handaxes in East Asia. Optically stimulated luminescence (OSL) ages obtained from chemically purified quartz from the upper five samples are in stratigraphic order, but the ages of the lower samples are not. The OSL signal of the oldest samples occurs well above the saturation level of the exponential part of the dose response curve; however, the OSL signal has an additional component that grows linearly at high doses, making it possible to calculate a De value and thus an age. However the reliability of calculating De using this linear component is not clear. In contrast, the thermally transferred OSL (TT-OSL) signal grows linearly with dose up to at least 1600 Gy, thus permitting its use for dating. The TT-OSL ages are in agreement with those from the OSL for the four uppermost samples, but give older ages for the lower three samples. Ages obtained using TT-OSL are in stratigraphic order and indicate that the oldest artefacts have an age of ～195 ka.  相似文献   

2.
Quartz optically stimulated luminescence (OSL) is increasingly being used to constrain the depositional age of fluvial and glaciofluvial sequences over orbital (Milankovitch) timescales within the British Isles. Few of these previous studies have had any age control; however there is some evidence that OSL ages based on the single aliquot regenerative dose (SAR) protocol may be subject to systematic age underestimation as samples approach saturation. In this study, the age of 12 luminescence samples from a chronologically well-constrained site dating to 450 ka from the Thames terrace sequence, southern Britain, was measured using SAR in order to test the performance of the method close to its upper age limit. The characteristics, dose response and thermal stability of the OSL signal in these samples were assessed by investigating equivalent dose (De) as a function of stimulation time and component-resolved pulse annealing. Despite the fact that the samples are dominated by the quartz fast component, these results showed that both the medium and slow components have lower stabilities than the fast component, but with the unstable medium component most affecting the initial part of the OSL signal used in dating. Based on isolating the fast component either through curve fitting or eliminating the medium component using the early background subtraction method, OSL ages up to 450 Gy were found to compare well with the expected age of the site of 450 ± 23 ka. In contrast, a systematic age underestimation of 10% was manifested at lower doses when using the initial part of the OSL signal, contaminated by the medium component. These results suggest that the early background subtraction method should be used when dating in the non-linear part of the growth curve as it provides a better separation of thermally unstable signals and represents a more convenient approach than curve fitting in well-behaved samples.  相似文献   

3.
High resolution OSL dating back to MIS 5e in the central Sea of Okhotsk   总被引：1，自引：0，他引：1  
Marine sediments contain important archives of past ocean and climate changes, but at high latitudes the absence of carbonate has prevented the construction of accurate chronological models. We have begun a study to (1) determine the accuracy of luminescence ages in deep-sea marine sediments, e.g. by comparison with marine oxygen isotope stratigraphy where possible, (2) describe changes in sedimentation rate through time, and (3) test whether it is possible to date back to marine isotope stage 5e (MIS 5e). We show here that optical dating of fine grains of quartz from the central Sea of Okhotsk is able to provide an accurate and precise chronology for the reconstruction of the palaeoceanic and palaeoclimatic environment at our site. The upper 6.5 m of the 18.42 m long core MR0604-PC07A is believed, based on its magnetic susceptibility and the oxygen isotope (δ18O) records to contain the last ～150 ka. Forty OSL samples were taken from this upper part of the core. The single-aliquot regenerative-dose (SAR) procedure is used for equivalent dose (De) determination. The luminescence characteristics of fine-grained quartz (4–11 μm) extracted from the core are described. The OSL signal is dominated by the fast component and a dose recovery test shows that we can accurately measure a known dose given in the laboratory prior to any heat treatment. Dose rates were determined using high-resolution gamma spectrometry, and vary between 0.4 and 1.6 Gy/ka. The OSL ages from this section lie between ～140 ka and ～15 ka and are in very good agreement with the δ18O stratigraphy up to MIS 5e. A clear change in sedimentation rate is identified: between ～139 and 110 ka, the sedimentation rate was ～0.09 m/ka, but then from ～110 to 15 ka, the sedimentation rate decreases to a constant value of ～0.04 m/ka. Our data confirm that OSL dating using widely distributed fine-grain quartz has great potential for dating deep-sea sediments. Because luminescence methods use clastic materials, they do not depend on the presence of biogenic carbonate. As a result it is now likely that we can establish a chronology in regions of the ocean that were previously undatable.  相似文献   

4.
In order to test the accuracy of quartz optically stimulated luminescence (OSL) dating for young dune sediments (<100 a), a series of aerial images of a migrating sand dune is used to cross validate OSL ages. The investigated dune is situated on the northern part of the island of Sylt (southern North Sea). Based on aerial images and a map from 1925 to 2009 and the internal architecture of the dune obtained by ground-penetrating radar (GPR), an independent age model has been developed to attribute sedimentary-architectural elements of the dune to time. The annual rate of dune migration is calculated to be around 4.1 m/a. Along a 245 m transect oriented parallel to the direction of dune movement, 13 samples for OSL dating were collected at equidistant locations. Sand-sized quartz (150–250 μm) was used for determining the equivalent dose (De) applying a single-aliquot regenerative-dose (SAR) protocol. Results show that the oldest OSL age from the investigated recent dune appeared to be 110 ± 10 a, whereas the modern analogue was dated to 34 ± 3 a. In comparison with the aerial images, the OSL ages show a systematic overestimation of 10–40 a for six out of seven younger samples, which are expected to be younger than ∼60 a. This offset is negligible for older samples, but a substantial error in these younger ages. The overestimation is originated from a combination of small thermal transfer of 4–12 mGy during preheat and incomplete bleaching in medium OSL component causing a residual dose of about 15 mGy. The contribution of the incompletely bleached medium component cannot be removed totally by an early background subtraction approach. Despite the observed offset for youngest samples, this study corroborates the suitability of the OSL technique to date young dune sediments (<100 a).  相似文献   

5.
The Starmoen dune field is part of a larger aeolian system in the Jømna and Glomma river valleys in southeastern Norway. It is believed to have formed just after the last deglaciation in the area, but no absolute ages have been available to support this. Here, we present a set of quartz optically stimulated luminescence (OSL) ages from the aeolian sediments and the underlying glacifluvial deposits. The results show that the main dune-building phase was a short-lived event ∼10 ka ago, likely with a duration less than a few hundred years. This suggests a rapid stabilisation of an initially unstable environment in newly deglaciated terrain. A much younger event with limited and surficial reworking of sand is dated to 770 ± 110 years ago, and the modern age of an active dune provide additional OSL quality control. Age overestimation is found for glacifluvial sediments, probably due to incomplete bleaching as indicated by e.g. scattered dose distributions from small aliquots. OSL measurements were conducted using coarse quartz grains (180–250 m), which show a dominance of a fast signal component.  相似文献   

6.
《Quaternary Geochronology》2008,3(1-2):114-136
We present chronological constraints on a suite of permanently frozen fluvial deposits which contain ancient DNA (aDNA) from the Taimyr Peninsula of north-central Siberia. The luminescence phenomenology of these samples is first discussed, focusing on the optically stimulated luminescence (OSL) decay curve characteristics, thermoluminescence (TL) properties, and signal compositions of quartz from these previously unstudied deposits. Secondly, we assess the suitability of these samples for OSL dating and present the OSL chronologies obtained using both single-grain and multi-grain equivalent dose (De) measurements. The results of our analyses reveal a large amount of inter-aliquot variability in OSL decay curve shape that is directly related to differences in the size of the 280 °C TL peak and the associated slowly bleached ‘S2’ OSL component. Longer OSL stimulation durations are adopted in the De measurement procedure to prevent the progressive build-up of slowly bleached signal components throughout successive single-aliquot regenerative-dose (SAR) measurement cycles. The use of low preheat temperatures in the SAR procedure also reduces the deleterious effects of these slowly bleached signal components. The resultant single-grain and multi-grain OSL chronologies obtained using this approach are stratigraphically consistent and are in close agreement with independently established 14C ages at our sites. The findings of this research reveal the potential of OSL dating as a means of providing a reliable chronometric framework for sedimentary aDNA records in permafrost environments.  相似文献   

7.
This study presents first results of a project which aims to develop an absolute chronology of the Weichselian ice marginal positions in north-eastern Germany using Optically Stimulated Luminescence (OSL) dating. Owing to the special geomorphological and stratigraphical setting, many of the sampling sites were situated close to the former ice margin. At some sections the sediments showed an incomplete resetting of the OSL signal. For this study the representative sandur sediment section from the Beelitz outwash cone was chosen to elaborate a strategy to reliably detect insufficient bleaching and to choose an appropriate age model for the calculation of the true burial dose of each sample. The age determined for the formation of the Beelitz outwash cone is 34.1 ± 3.0 ka. Although this age might still be a maximum age, this study shows that by applying the proposed methodological strategy, plausible ages can be derived from insufficiently bleached, ice proximal sandur sediments.  相似文献   

8.
We present the results of K-feldspar IRSL dating of the four lower terraces (T3–T6) of the Portuguese Tejo River, in the Arripiado-Chamusca area. Terrace correlation was based upon: a) analysis of aerial photographs, geomorphological mapping and field topographic survey; b) sedimentology of the deposits; and c) luminescence dating. Sediment sampled for luminescence dating gave unusually high dose rates, of between 3.4 and 6.2 Gy/ka and, as a result, quartz OSL was often found to be in saturation. We therefore used the IRSL signal from K-feldspar as the principal luminescence technique. The K-feldspar age results support sometimes complex geomorphic correlations, as fluvial terraces have been vertically displaced by faults (known from previous studies). Integration of these new ages with those obtained previously in the more upstream reaches of the Tejo River in Portugal indicates that the corrected K-feldspar IRSL ages are stratigraphically and geomorphologically consistent over a distance of 120 km along the Tejo valley. However, we are sceptical of the accuracy of the K-feldspar ages of samples from the T3 and T4 terraces (with uncorrected De values >500 Gy). In these cases the Dose Rate Correction (DRC) model puts the natural signals close to luminescence saturation, giving a minimum corrected De of about 1000 Gy, and thus minimum terrace ages; this may even be true for those doses >200 Gy. Luminescence dating results suggest that: T3 is older than 300 ka, probably ca. 420–360 ka (～Marine Isotope Stage [MIS]11); T4 is ca. 340–150 ka (～MIS9-6); T5 is 136–75 ka (～MIS5); T6 is 60–30 ka (MIS3); an aeolian sand unit that blankets T6 and some of the older terraces is 30–≥12 ka. Collectively, the luminescence ages seem to indicate that regional river downcutting events may be coincident with periods of low sea level (associated, respectively, with the MIS10, MIS6, MIS4 and MIS2).  相似文献   

9.
We test the applicability of quartz optically stimulated luminescence (OSL) dating on clastic lake sediments to investigate whether this dating method can be applied to study the timing and rate of deposition in Holocene fluvio-deltaic lakes. Our study concerns the filling of a lake by the Angstel-Vecht system, part of the Rhine delta in the western Netherlands. Age constraints are provided by radiocarbon dates on the development and abandonment of the fluvial channels debouching into the lake. Results indicate that light exposure prior to deposition and burial was sufficient to reset the OSL signal of the vast majority of the quartz grains. Special attention was given to accurate estimation of the dose rate in the laminated and bedded deposits. The OSL ages obtained are in good agreement with the age constraints, especially for the relatively coarse sediments. OSL results indicate that the filling of the lake took about 700 years, with a sedimentation rate of ～3 mm per year. This study is a demonstration of the use of OSL dating of sand-sized quartz to determine the timing and rate of sedimentation in a Holocene fluvio-deltaic environment.  相似文献   

10.
A sand layer, interpreted as a hyperconcentrated flow deposit, was found interbedded between loess on a Yellow River terrace in Hukou, Shaanxi, China. The site is known as the Longwangchan Palaeolithic site. The deposits from the terrace were dated using optically stimulated luminescence (OSL). Two samples from the sand layer were dated to 30 ± 2 and 33 ± 3 ka using coarse-grained (CG) quartz, and to 82 ± 7 and 94 ± 5 ka using fine-grained (FG) quartz, respectively. The CG quartz OSL ages are believed to be reliable on the basis of the OSL ages of the bracketing loess samples. The overestimation of the FG quartz OSL ages of the sand samples is explained in terms of hyperconcentrated flow processes during sediment transport and deposition. The large difference between the CG and FG quartz OSL ages of the sand samples helps to better understand the formation of the hyperconcentrated flow deposit. The hyperconcentrated flow deposit in this study indicates an extreme river flood occurring at ～30 ka in this area. In addition, the stone artifacts found in the lower loess layer overlying the bedrock of the terrace were dated to ～47 ka.  相似文献   

11.
In Central Iran there are several cities along the Dehshir fault, which have similar geological conditions to that of the city of Bam prior to the 2003 earthquake (Mw 6.5), during which more than 30,000 lives were lost. Optical stimulated luminescence (OSL) samples were collected from the Dehshir fault in order to place constraints on its seismic history. The single aliquot regenerative (SAR) dose measurement protocol on coarse grained quartz extracts was used for this study. This SAR protocol had to be optimized for the low OSL sensitivity by varying both the preheat temperatures and test doses used. Dose recovery tests showed that given laboratory dose could be successfully recovered. However, replicate palaeodose (De) data were scattered and consequently ages based on mean De's had large uncertainties. As this is thought to largely reflect poor bleaching conditions prior to sediment burial at the site, various statistical procedures were employed in conjunction with the stratigraphic knowledge of the site to try and extract more refined burial ages from the samples. From this the timing of the last earthquake was estimated around 2.0 ± 0.2 kyr. This refined age suggests that the earthquake catalogue of Iran is incomplete and more paleoseismological investigation is required to recognize and date the previous events of Dheshir fault.  相似文献   

12.
We investigate the use of quartz optically stimulated luminescence (OSL) dating for determining fluvial overbank sedimentation rates over decades to centuries. For the study we took 11 samples from three cores from an embanked floodplain along the River Waal (Rhine) near Neerijnen (The Netherlands). We propose a measurement protocol for young fluvial quartz based on the single-aliquot regenerative dose procedure. Parameters for the protocol are chosen to isolate the fast OSL component, eliminate an ultrafast OSL component and avoid thermal transfer. The protocol shows excellent dose recovery and recycling ratios. For each sample, a Gaussian is fitted to the lower part of the equivalent dose distribution to obtain an estimate of the burial dose. We discuss the validity of the OSL ages using internal and external controls, and conclude that there is no evidence for large systematic offsets in the OSL ages. OSL based sedimentation rates are between ～3 and 8 mm/a, in line with previous estimates.  相似文献   

13.
The usual practice in optical dating is to derive an equivalent dose (De) (and hence age) from integration of the initial part of the measured optically stimulated luminescence (OSL) signal. This ‘bulk’ OSL signal is known to comprise several semi-independent components, each of which decays at different rates during measurement, and thus contributes a different proportion to the bulk signal as measurement time progresses. Data are presented here which show a strong dependence of De on the bulk signal integration interval, with reduced De for later signal integration intervals resulting from lower medium component De values. This dependence leads to two problems: (i) deciding which signal integral to choose, and (ii) the possibility that all bulk signals will provide systematic age underestimation due to medium component signal contributions. Isolating the fast component of the bulk OSL signal provides a solution to both problems and several methods of achieving this are assessed; an efficient new method is described which is incorporated in to standard single-aliquot regenerative-dose measurement sequences. This method involves the direct measurement of the fast-component signal using infrared (830 nm) stimulation of quartz at 160 °C, prior to the standard bulk OSL measurement with 470 nm stimulation. It is shown that the measured quartz infrared stimulated luminescence signals resolve pure fast-component signals and provide De estimates consistent with those from signal deconvolution. This approach can only be applied to samples with relatively bright luminescence emissions, but in these cases is expected to provide a more robust estimate of palaeodose.  相似文献   

14.
Lynch's Crater on the Atherton Tablelands in NE-Australia formed about 230,000 years ago during an explosive eruption, creating a maar more than 80 m deep. Since the eruption, the maar has been filled with lake sediments that are topped by peat material. A 64 m long core was recovered and an OSL dating project was undertaken to extend the chronology beyond 16 m depth, which according to 14C age control represents ～60 ka. The predominantly organic lake sediments contained abundant fine quartz of aeolian origin, and the Single Aliquot Regenerative Method (SAR) provided satisfactory equivalent dose (DE) estimates. However, the determination of the dose rate proved both critical and difficult. Extremely low radionuclide contents led to cosmic radiation being the dominant dose rate contribution for most samples. The OSL chronology presented in this paper thus relies on modelling the changing cover by sediments and lake water over the burial time.  相似文献   

15.
Palaeolimnological studies together with geomorphological investigations of exposed lacustrine sections on the Tibetan Plateau provided valuable palaeoclimate records. Radiocarbon dating is the most commonly used method for establishing chronologies of lake sediments. However, 14C dating of such sediments could be problematic due to the lack of organic matter or a reservoir effect, which commonly appears in radiocarbon ages of lacustrine sediments from the Tibetan Plateau. OSL dating is an alternative for dating the lake sediments and also provides the opportunity to independently test radiocarbon chronologies. The current study tries to compare OSL and 14C dating results in order to evaluate the reservoir effect of 14C dating, and then based on quartz OSL dating and stratigraphic analysis, to construct the chronostratigraphy of a lacustrine sedimentary sequence (TYC section), an offshore profile from Tangra Yumco lake on the southern Tibetan Plateau. Results suggest that: (1) it is possible to obtain robust OSL age estimates for these lake sediments and the OSL ages of the three samples range from ca. 7.6 ka to ca. 2.3 ka; (2) The discrepancy between the OSL and 14C ages is ca. 4–5 ka, which possibly results from the age overestimate of 14C dating due to a reservoir effect in the studied lake; (3) the chronostratigraphy of TYC section and sedimentological environmental analysis show a large lake with a lake level distinctively above the present during ca. 7.6–2.7 ka indicating a wet mid-Holocene in the study area.  相似文献   

16.
Daihai Lake is one of the largest lakes in the mid-latitude of northern China. Previous environmental change investigations using the sediments from the lake have been mainly focused on the last 13 ka. In 2006, we drilled an 80-m borehole on the southwest coast of the lake. Here we report the results of initial optical dating of the upper 22-m sediments from the core. Most of the samples allow separation of the 4–11 μm fine-grained and 45–63 μm medium-grained quartz, both of which were used for equivalent dose (De) determination. Dose recovery test experiments with the single-aliquot regeneration-dose (SAR) protocol indicate that a preheat at 240 °C for 10 s combined with a cut-heat of 240 °C is suitable for these samples. The De values show marked discrepancy between the two grain size fractions with the fine-grained quartz yielding up to over 50% higher De values than the medium ones for some samples. We consider the OSL ages for the samples from upper ～10 m to be overestimated. The main cause of the overestimation is attributed to the incomplete bleaching of the sediment grains at deposition. The OSL ages for the lower part of the sequence are considered to be reasonable age estimates which provide useful temporal constrains on the deposition of the sediments for the period of 20–40 ka.  相似文献   

17.
The site of Bonneval (France) exhibits a 6 m thick stratigraphical sequence in which Middle and Lower Palaeolithic artefacts were discovered. The stratigraphy of the site consists of an alternation of loess-like silt layers deposited along glacial stages, and paleosoil horizons corresponding to the vegetal stabilization of the area during interglacials. These layers hence provide past environmental informations and can be used as stratigraphical markers and compared with well dated sequences of Northern France. Eight sediment samples from this Middle and Upper Pleistocene sequence were dated using the recuperated optically stimulated luminescence (Re-OSL) signal of quartz grains. The middle-size fraction (40–63 μm) shows a good reproducibility of the OSL signals which allows the application of a multiple-aliquot additive-dose approach for De determination. For all samples, the growth curves are linear up to an accumulated dose of 3000 Gy. The Re-OSL ages range from ～100 to ～450 ka and are in good agreement with the independent chronological information; they establish when handaxe industries have been made during the Middle and Upper Pleistocene in the Paris Basin.  相似文献   

18.
Identification of past tsunamis is important for risk assessment and management of coastal areas. Obtaining accurate and precise ages of sediments originating from such extreme marine coastal floods is crucial for a reliable estimation of the recurrence interval of these often devastating events. We present here the results of quartz optical dating and 14C dating of two sites (Boca do Rio and Martinhal) on the Algarve coast (southern Portugal). These sites contain deposits of the great tsunami of November 1, 1755. The sections were described using sedimentological techniques; at both sites tsunami-laid sands and gravels were identified, intercalated between estuarine muds. Quartz luminescence ages from these sedimentary successions were derived using standard SAR-OSL dating using multi-grain sub-samples. A multiple sampling strategy was employed with several samples taken from the AD 1755 tsunami deposit and from the sediments bracketing the tsunami layer. Our SAR-OSL protocol was shown to be appropriate using dose recovery measurements (measured/given dose ratio of 1.004 ± 0.007, n = 165). The several OSL ages from the 1755 tsunamigenic deposits are internally reproducible but yield age overestimates of between 20 and 125% (60–310 years respectively); this is in agreement with values reported in the literature for similar deposits. The age overestimation of the tsunami-laid sands is presumably due to the rapid erosion and deposition of older sediments, with insufficient light exposure for complete bleaching during the tsunami event itself. The absence of significant bleaching during the tsunami is also suggested by the shape of the dose distributions based on sub-samples made up of only about 100 grains. Analysis of the distributions with the minimum-age model seems to yield the expected age for two of the three distributions. It is important to note that age offsets of a few tens of years to a few hundred years rapidly become insignificant when dating older (>1 to few ka) tsunami layers.  相似文献   

19.
Optically stimulated luminescence (OSL) dating methods have been widely applied in Quaternary glaciology. However, glacigenic deposits are considered in general as problematic for OSL dating, mainly because they are transported shorter distances prior to burial and are usually partially bleached. Thus, most researchers choose glaciofluvial and glaciolacustrine sediments (with relatively longer transportation times) for OSL dating when constraining the age of glaciation. In this study, four samples were collected from a lateral moraine series at Zhuqing Village, northern margin of Queer Shan Mountain, eastern Tibetan Plateau, in order to investigate the applicability of OSL dating for morainic deposits. Quartz grains (38–63 μm) were extracted and measured using single aliquot regenerative-dose (SAR) protocol. Internal checks and dose recovery test show that the SAR protocol is appropriate for equivalent dose (De) determination. The effect of thermal transfer is small for all samples and the recycling ratio for each individual sample is close to unity. The symmetry in the De distributions indicates that quartz grains were well-bleached prior to burial. OSL ages show good agreement with geomorphological and field investigations, and are also concordant with an independent ESR age. It is concluded that: (a) the morainic deposits in Zhuqing were well-bleached and suitable for OSL dating; (b) SAR protocol can be applied to morainic deposits for samples under study.  相似文献   

20.
The present study focuses on the chronological relationship between alternating dune sand and silty water-lain sediments in the central part of the Khongoryn Els dune field in the Gobi Desert, Southern Mongolia. The 23 m high section evolved from the construction of a natural dam by west–east moving sand dunes and fluvial inundation by a river system from the mountain ranges in the south. To resolve the chronology of events, optically stimulated luminescence (OSL) dating was applied and from sedimentological and geochemical analysis the depositional processes could be characterised. Quartz OSL dating of these sediments is hindered by feldspar contamination. Thus, dating of coarse-grain K-feldspars is applied to provide a more reliable chronostratigraphy. As this fraction might be influenced by signal loss over geological time scales, the extent of fading is measured and corrected for. The resulting ages fit well in a supraregional reconstruction of Central Asian palaeoclimate. The data imply that the basal aeolian sediments were deposited 27 ka ago, while the major part of the profile was accumulated in a rather short period of time around ～15 ka. The temporal differentiation implies that the stratification of aeolian and fluvial sediments is not caused by long term climatic variations. It rather represents arid conditions with episodical fluvial activity. Samples between 20 and 15 m depth could not be taken, but it is assumed that this part of the section represents an extremely arid time period with an intensive remobilisation of sand around LGM. A dune overlying the section was deposited during the Late Holocene and represents the ongoing aridity in this region.  相似文献   

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