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1.
通过高温高压实验研究了铁橄榄石集合体的流变性.首先,利用高精度的Paterson气体介质变形装置对铁橄榄石集合体Fe2SiO4进行了高温三轴压缩蠕变试验.变形试验条件为:温度1273～1423K,围压300MPa,差应力10～250MPa,应变率10-7～10-4s-1,试件的最大变形量不超过20%.利用三维非线性拟合方法对蠕变试验数据进行分析,得到铁橄榄石集合体的微观变形机制为扩散域和位错域,扩散域的应力指数为1左右.位错蠕变域中,干燥铁橄榄石集合体的应力指数为5.4.活化能为781kJ/mol;含水铁橄榄石集合体的应力指数为3.4,活化能为516kJ/mol.实验结果表明,含水时铁橄榄石的流变强度比干燥时小一个数量级.将实验结果与铁橄榄石单晶的强度进行对比,发现铁橄榄石集合体的流变强度比铁橄榄石单晶的强度高.从而得到了铁橄榄石集合体高温高压流变性(强度)的初步试验结果. 相似文献
2.
富铁橄榄石的高温变形实验研究 总被引：1，自引：3，他引：1
利用高精度Paterson气体介质变形装置对(Mg0.5,Fe0.5)2SiO4和(Mg0.7,Fe0.3)2SiO4橄榄石集合体进行了高温三轴压缩变形试验。首先用人工合成了纯铁橄榄石Fe2SiO4,然后用合成的纯铁橄榄石与天然圣卡罗橄榄石按一定比例混合烧结合成了含铁量分别为50％和30％的富铁橄榄石集合体Fo50和Fo70。三轴压缩蠕变变形试验在温度1223-1473 K和围压 300 MPa的条件下进行,差应力为10-300 MPa,应变率为10-7-10-4s-1,每个试件的最大变形量为20％．利用三维非线性方法对蠕变数据进行拟合,得出的流动律中,Fo50应力指数为4．1,活化能为499kJ／mol;Fo70应力指数为4．3,活化能为510kJ／ mol。将实验结果与Fo90圣卡罗橄榄石集合体的强度进行对比,发现含铁量的增加使橄榄石的强度明显下降,Fo50橄榄石集合体比Fo70的粘性低一个量级,Fo70比Fo90的粘性低一个量级。从而得到了含铁量对橄榄石的粘性(强度)影响的初步试验结果。 相似文献
3.
橄榄石集合体的简单剪切形变实验研究 总被引：1，自引：1，他引：0
本文利用高精度Paterson气体介质变形装置对富铁橄榄石集合体(Mg_(0.5),Fe_(0.5))_2SiO_4进行了高温简单剪切变形试验.试验在温度1473K和围压300MPa的条件下进行,差应力为64～153MPa,应变率为10~-5～10~-3s~-1.一共进行了三组试验,试件的剪切变形量分别为89%,131%和200%,通过对变形后试件的反射光学显微结构分析,得到富铁橄榄石集合体动态重结晶的微观机制,由结晶各向异性分析给出晶格最优取向和波速各向异性的分布及随应变的增加而表现出的演化特征. 相似文献
4.
铁橄榄石集合体为无根岩石。外观呈铁黑色,风化面呈亮栗褐色。本文对铁橄榄石集合体的形态特征、物理性质和化学成分进行了研究。通过化学式的计算,其化学式为:(Mg_(0.0168)Fe_(0.9802)Mn_(0.003))_2[SiO_4],证明其为铁橄榄石的端员组份。此外,还对其进行了穆斯堡尔谱分析、X射线粉晶衍射分析和红外光谱分析。其穆斯斑堡尔谱分析结果与人工合成的铁橄榄石数据相近,它的衍射数据及计算的晶胞参数也与JCPDS所提供的标准数据非常接近,这些进一步证明了铁橄榄石集合体的成分接近于铁橄榄石端员组份。 相似文献
5.
压力对橄榄石流变性的影响 总被引：2，自引：4，他引：2
本文给出细粒橄榄石集合体在位错蠕变域中压力效应的实验结果。对干燥、人工合成的橄榄石集合体进行了三轴压缩实验,试验在一台高分辨率的气体介质试验机上进行。典型的常载荷蠕变试验温度为1473K或1523K,围压为400MPa、200MPa、400MPa、200MPa。当差压力和温度给定时,试件在400MPa围压下,变形速度较200MPa围压下要慢。实验得出的细粒橄榄石集合体在位错蠕变域中的活化体积值为(23±3)×10~(-6)m~3/mol。最后,对实验结果在地幔动力学中的应用进行了讨论。 相似文献
6.
橄榄石集合体中与位错蠕变相伴随的粒间滑动 总被引：2，自引：0，他引：2
为了研究橄榄岩位错蠕变过程中粒间滑动所起的作用,对经脱水干燥的橄榄石集合体试件进行了一系列的变形试验。三轴压缩蠕变试验在T=1473K、P=200和400MPa条件下使用一台高分辨率气体介质变形装置进行,每个试件在介于100~250MPa之间的不同应力水平下变形,得到的应变率介于10-4 ~10-6S-1之间。随着差应力的增加,得到扩散蠕变到位错蠕变的过渡,在位错蠕变域,易滑动体系在~50MPa和颗粒尺寸为15μm时伴随粒间滑动。这一粒径敏感蠕变域由应力指数3.2±0.1和粒径指数1.8±0.2来刻划。将这一流动律与其他扩散和位错蠕变结果进行对比,表明本文得出的流动律可应用于粒度小于100μm和差应力大于20MPa时的岩石流动。因此,与粒间滑动相伴的位错蠕变可能是上地幔岩石圈剪切带变形局部化的主要变形机制。 相似文献
7.
本文介绍了采用透射电子显微镜观察研究福建明溪大洋窠上第三系玻基玄武岩中的包体橄榄石的位错结构。研究表明,该地幔源包体橄榄石中存在位错壁、自由位错、位错弓弯和位错环等,它们是该橄榄石在上地幔的高温低应力条件下发生复杂蠕变的产物。根据该地包体橄榄石中自由位错密度(统计值为2.0×10~8cm~(-2)和共生辉石的化学成分,估算出福建明溪大洋窠玻基玄武岩中幔源包体的变形条件为:温度(T)为1070℃;压力(P)为2480MPa;深度(Z)为79.3km;流变应力(σ_1-σ_3)为136MPa;流变速率(ε)为7.6×10~(-13)s~(-1);粘稠度(η)为0.8×10~(20)poise。 相似文献
8.
西藏罗布莎地幔橄榄岩变形显微构造特征及其地质意义 总被引：1，自引：0，他引：1
地幔橄榄岩是罗布莎蛇绿岩的主要组成成分之一,通过显微构造特征可对其变形特征进行分析,确定流变学参数,探讨地幔橄榄岩的变形历史。以蛇纹石化程度较低的二辉橄榄岩和方辉橄榄岩为研究对象,橄榄石位错特征研究显示,本区橄榄石主要发育了低温常见的直线型自由位错,局部可见位错弓弯、位错环、位错壁等高温位错,反映罗布莎地幔橄榄岩变形以低温塑性流变为主,局部经历了高温塑性流变,主导变形机制为位错蠕变。橄榄石自由位错统计结果表明,二辉橄榄岩中的橄榄石自由位错密度为4.422×107/cm2,方辉橄榄岩中的橄榄石为9.137×107/cm2,变形过程中所受差异应力分别为65MPa和93MPa。橄榄石和斜方辉石显微组构测量采用了电子背散射衍射技术(EBSD),分析结果表明,橄榄石均发育A型组构,为浅部地幔常见的组构类型,该结果与金刚石、柯石英等超高压矿物所指示的形成深度不一致。 相似文献
9.
橄榄石集合体扭转大变形实验研究 总被引：5，自引：4，他引：1
对(Mg0.5,Fe0.5)2SiO4和(Mg0.7、Fe0.3)2SiO4橄榄石集合体进行了高温高压扭转大变形实验研究.试验在高精度和高分辨率Paterson气体介质变形试验机上进行,试验温度为1473K,围压为300MPa,应变率为10-4～10-5S-1,剪切应力为82～124MPa,剪切应变为～400%,将变形后试件沿轴向切开进行了显微结构分析,确定了不同纵截面上橄榄石的颗粒尺寸.由蠕变数据拟合出的流动律中,应力指数为与三轴压缩实验给出的应力指数吻合.利用EBSD方法分别对变形前后试件中橄榄石的晶格最优取向(LPO)进行了测定.在富铁橄榄石样品中观测到的最优晶格取向表明滑动属于(okl)[100]滑动系统.这个结果与Bystficky等人在Fo90种观测到的最优晶格取向特征是一致的. 相似文献
10.
鉄鱗石产于北京延庆超基性岩体中,1961年暑期,在野外曾暫定名为“絹石”(Bastite),它是斜方輝石族矿物水热蝕变的产物。矿物呈暗棕綠色鳞片状集合体,化学結构式为:(Mg_(4.6)Fe(0.5))_(5.1)Fe_(0.6)(Si_4O_(10))(OH)_8。根据它的物理性貭和光学性貭,在A.N.文 相似文献
11.
Deformation experiments on olivine aggregates were performed under hydrous conditions using a deformation-DIA apparatus combined with synchrotron in situ X-ray observations at pressures of 1.5–9.8 GPa, temperatures of 1223–1800 K, and strain rates ranging from 0.8 × 10?5 to 7.5 × 10?5 s?1. The pressure and strain rate dependencies of the plasticity of hydrous olivine may be described by an activation volume of 17 ± 6 cm3 mol?1 and a stress exponent of 3.2 ± 0.6 at temperatures of 1323–1423 K. A comparison between previous data sets and our results at a normalized temperature and a strain rate showed that the creep strength of hydrous olivine deformed at 1323–1423 K is much weaker than that for the dislocation creep of water-saturated olivine and is similar to that for diffusional creep and dislocation-accommodated grain boundary sliding, while dislocation microstructures showing the [001] slip or the [001](100) slip system were developed. At temperatures of 1633–1800 K, a much stronger pressure effect on creep strength was observed for olivine with an activation volume of 27 ± 7 cm3 mol?1 assuming a stress exponent of 3.5, water fugacity exponent of 1.2, and activation energy of 520 kJ mol?1 (i.e., power-law dislocation creep of hydrous olivine). Because of the weak pressure dependence of the rheology of hydrous olivine at lower temperatures, water weakening of olivine could be effective in the deeper and colder part of Earth’s upper mantle. 相似文献
12.
High-temperature creep behavior in Ni2GeO4 spinel was investigated using synthetic polycrystalline aggregates with average grain sizes ranging from submicron to 7.4
microns. Cylindrical samples were deformed at constant load in a gas-medium apparatus at temperatures ranging from 1223 to
1523 K and stresses ranging from 40 to 320 MPa. Two deformation mechanisms were identified, characterized by the following
flow laws:
where σ is in MPa, d is in μm and T is in Kelvin. These flow laws suggest that deformation was accommodated by dislocation creep and grain-boundary diffusion
(Coble) creep, respectively. A comparison with other spinels shows that an isomechanical group can be defined for spinels
although some differences between normal and inverse spinels can be identified. When creep data for olivine and spinel are
normalized and extrapolated to Earth-like conditions, spinel (ringwoodite) has a strength similar to olivine in the dislocation
creep regime and is considerably stronger than olivine in the diffusion creep regime at coarse grain size. However, when grain-size
reduction occurs, spinel can become weaker than olivine due to its high grain-size sensitivity (Coble creep behavior). Analysis
of normalized diffusion creep data for olivine and spinel indicate that spinel is weaker than olivine at grain sizes less
than 2 μm.
Received: 18 June 2000 / Accepted: 3 April 2001 相似文献
13.
对超高压变质带中橄榄岩变形显微构造的研究, 有助于了解板块边界构造环境中地幔物质的流变性质和变形机制, 进而探讨其在深俯冲/折返过程中的地球动力学过程的作用.采用光学显微镜、电子探针、红外光谱、电子背散射衍射(EBSD)、位错氧化缀饰等多种方法系统研究了来自中国大别碧溪岭的石榴异剥橄榄岩中的变形显微构造.研究结果表明: (1)碧溪岭石榴异剥橄榄岩发育较好的形状优选方位, 但只有单斜辉石显示了强晶格优选方位, 而橄榄石晶格优选方位很弱, 与常见上地幔橄榄岩中单斜辉石组构弱而橄榄石组构强的特点差异显著, 反映了单斜辉石经历位错蠕变而橄榄石经历位错调节的颗粒边界滑移变形; (2)碧溪岭异剥橄榄岩中单斜辉石和橄榄石均含有一定量的结构水, 其中单斜辉石含水量124×10-6~274×10-6, 橄榄石含水量38×10-6~80×10-6, 高于常见造山带橄榄岩中各矿物的含水量, 可能反映了壳源物质混染引起的高含水量变形环境; (3)橄榄石中发育显著位错显微构造, 根据位错显微构造计算的变形差异应力为230~600 MPa, 高于正常上地幔稳态流变应力, 反映了俯冲带中的相对低温变形环境.综合分析研究表明, 超高压变质带中的高压、低温、高差异应力和高结构水含量是形成碧溪岭相对独特的橄榄石、单斜辉石变形显微构造的原因. 相似文献
14.
Experimental deformation of partially melted granitic aggregates 总被引：16，自引：1，他引：16
Abstract The effects of varying amounts of partial melt on the deformation of granitic aggregates have been tested experimentally at conditions (900°C, 1500 MPa, 10-4 to 10-6/s) where melt-free samples deform by dislocation creep, with microstructures approximately equivalent to those of upper greenschist facies. Experiments were performed on samples of various grain sizes, including an aplite (150 μm) and sintered aggregates of quartz-albitemicrocline (10–50 and 2–10 μm). Water was added to the samples to obtain various amounts of melt (1–15% in the aplite, 1–5% in the sintered aggregates). Optical and TEM observations of the melt distribution in hydrostatically annealed samples show that the melt in the sintered aggregates is homogeneously distributed along an interconnected network of triple junction channels, while the melt in the aplites is inhomogeneously distributed. The effect of partial melt on deformation depends an melt amount and distribution, grain size and strain rate. For samples deformed with ? 1% melt, all grain sizes exhibit microstructures indicative of dislocation creep. For samples deformed with 3–5% melt, the 150 μm and 10–50 μm grain size samples also exhibit dislocation creep microstructures, but the 2–10 μm grain size samples exhibit abundant TEM-scale evidence of dissolution-precipitation and little evidence of dislocation activity, suggesting a switch in deformation mechanism to predominantly melt-enhanced diffusion creep. At natural strain rates melt-enhanced diffusion creep would predominate at larger grain sizes, although probably not for most coarse-grained granites. The effects of melt percentage and strain rate have been studied for the 150 μm aplites. For samples with ? 5 and 10% melt, deformation at 10–6/s squeezes excess melt out of the central compressed region allowing predominantly dislocation creep. Conversely, deformation at 10-5/s produces considerable cataclasis presumably because the excess melt cannot flow laterally fast enough and a high pore fluid pressure results. For samples with 15% melt, deformation at both strain rates produces cataclasis, presumably because the inhomogeneous melt distribution resulted in regions of decoupled grains, which would produce high stress concentrations at point contacts. At natural strain rates there should be little or no cataclasis if an equilibrium melt texture exists and if the melt can flow as fast as the imposed strain rate. However, if the melt is confined and cannot migrate, a high pore fluid pressure should promote brittle deformation. 相似文献
15.
R. J. M. Farla H. Kokkonen J. D. Fitz Gerald A. Barnhoorn U. H. Faul I. Jackson 《Physics and Chemistry of Minerals》2011,38(5):363-377
The rate of static dislocation recovery in Fo90 olivine has been studied under conditions of high temperature and controlled atmosphere in compressively deformed polycrystals
hot-pressed from synthetic (sol–gel) and natural (San Carlos) precursor powders. The sol–gel olivine, containing a small fraction
of orthopyroxene, was deformed to a final strain of 19% with a maximum differential stress of 266 MPa whereas the San Carlos
specimen was deformed to 15% strain and 260 MPa differential stress. Small samples cut from these deformed materials were
annealed under high-temperature, controlled atmosphere conditions, for different durations to allow partial recovery of the
dislocation sub-structures. Oxidative-decoration of the microstructural features, followed by backscattered electron imaging
at 5 kV and image analysis, was used to determine dislocation density. The variation of dislocation density ρ with time t at absolute temperature T was fitted to a second-order rate equation, in integral form, 1/ρ(t) − 1/ρ(0) = kt with k = k
0 exp(−E
a/RT). The activation energy E
a of the recovery process is 240 ± 43 and 355 ± 81 kJ mol−1 for sol–gel and San Carlos olivine polycrystals, respectively. The measured rates are one to two orders of magnitude lower
than those reported in previous studies on natural single crystal olivine. The difference may be explained by several factors
such as high dislocation densities measurable from large areas at high magnification for the SEM and the technique used to
estimate dislocation densities. Comparison between fine-grained sol–gel olivine and the coarser-grained San Carlos olivine
aggregate did not indicate that grain boundaries play an important role in dislocation recovery, but the absence of grain
boundaries might also have contributed to the high dislocation recovery rates previously measured for single crystals. 相似文献
16.
We show that naturally-deformed hematite from the Quadrilátero Ferrífero Province, Minas Gerais, Brazil, develops CPOs by dislocation creep, strongly influenced by basal plane parallel glide, even when this is not the favored slip system. Characterization of microstructure and texture, particularly intragranular misorientations, of naturally deformed hematite aggregates by EBSD allowed us to determine the importance of different slip systems, and confirm dislocation creep as the dominant deformation mechanism. Viscoplastic self-consistent (VPSC) models were constructed to constrain the slip systems required to operate for the observed CPO to develop, and its rheological implications. Changes in the CRSS ratio of hematite prism and basal slip systems and deformation regime lead to the development of distinct patterns of hematite crystallographic orientations. The basal slip-dominated simple shear model is the only one that can develop quasi-single-crystal CPO of the kind observed in highly deformed rocks from Quadrilátero Ferrífero. Comparison between naturally deformed hematite aggregates and VPSC models shows that CPO development of hematite is strongly influenced by a highly viscoplastic anisotropy through dislocation creep on hematite basal plane. Nonetheless, our results demonstrate that even the unfavorable slip systems should be regarded when the bulk rheology of mineral aggregates is evaluated. 相似文献
17.
Deformation microstructures of olivine in peridotite from Spitsbergen, Svalbard and implications for seismic anisotropy 总被引：1，自引：0，他引：1
To understand the deformation mechanism and seismic anisotropy in the uppermost mantle beneath Spitsbergen, Svalbard, in the Arctic, the deformation microstructures of olivine in the peridotite of Spitsbergen were studied. Seismic anisotropy in the upper mantle can be explained mainly by the lattice-preferred orientation (LPO) of olivine. The LPOs of the olivine in the peridotites were determined using electron backscattered diffraction patterns. Eight specimens out of 10 showed that the [100] axis of the olivine was aligned subparallel to the lineation and that the (010) plane was subparallel to the foliation, showing a type A LPO. In the other two specimens the [100] axis of olivine was aligned subparallel to the lineation and both the [010] and [001] axes were distributed in a girdle nearly perpendicular to the lineation, showing a type D LPO. The dislocation density of the olivine in the samples showing a type D LPO was higher than that in the samples showing a type A LPO. The result of an Fourier transformation infrared study showed that both the types A and D samples were dry. These observations were in good agreement with a previous experimental study ( Tectonophysics , 421 , 2006, 1 ): samples showing a type D LPO for olivine were observed at a high stress condition and samples showing both types A and D LPO were deformed under dry condition. Observations of both strong LPOs and dislocations of olivine indicate that the peridotites studied were deformed by dislocation creep. The seismic anisotropy calculated from the LPOs of the olivine could be used to explain the seismic anisotropy of P - and S -waves in the lithospheric mantle beneath Spitsbergen, Svalbard. 相似文献
18.
Hydrolytic weakening of experimentally deformed Westerly granite and Hale albite rock 总被引：2，自引：0，他引：2
In order to determine the effect of water on deformation in the brittle-ductile transition region of crustal rocks, experiments have been conducted on Westerly granite and a polycrystalline albite rock, comparing samples dried at 160°C for 12 h (‘dry’) and samples with about 0.2 wt% water added (‘wet’). The deformation mechanisms and style of deformation of the wet and dry samples, determined using optical and transmission electron microscopy, have been found to depend on temperature, pressure, strain rate, and strain. At 15 kb and 10−6, the added water reduces the temperature of the transition between microcracking and dislocation glide and climb by about 150–200°C for both quartz and feldspar. However, the penetration of ‘water’ into the grains is slow compared with the time of the experiments and many of the wet samples show evidence of initial microcracking and later dislocation creep. Wet samples deformed at 10 kb show less hydrolytic weakening than wet samples deformed at 15 kb. Because the deformation mechanism and strength of silicates depend so sensitively on trace amounts of water, and because the water content of experimental samples varies with temperature and pressure and thus with time, flow laws for any samples are only meaningful if the water content has been carefully controlled or characterized. 相似文献
19.
The ductile behavior of olivine-rich rocks is critical to constrain thermal convection in the Earth's upper mantle. Classical olivine flow laws for dislocation or diffusion creep fail to explain the fast post-seismic surface displacements observed by GPS, which requires a much weaker lithosphere than predicted by classical laws. Here we compare the plasticity of olivine aggregates deformed experimentally at mantle pressures and temperatures to that of single crystals and demonstrate that, depending on conditions of stress and temperature, strain accommodated through grain-to-grain interactions – here called intergranular strain – can be orders of magnitude larger than intracrystalline strain, which significantly weakens olivine strength. This result, extrapolated along mantle geotherms, suggests that intergranular plasticity could be dominant in most of the upper mantle. Consequently, the strength of olivine-rich aggregates in the upper mantle may be significantly lower than predicted by flow laws based on intracrystalline plasticity models. 相似文献