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对采自河北省迁西县太平寨ＨＢＴ１麻粒岩中的辉石、角门石、斜长石进行了４０Ａｒ－３９Ａｒ年龄测定，并对上述三种矿物做了４０Ｋ－４０Ａｒ同位素封闭温度计算，进而根据封闭温度与年龄的关系，研究了该区麻粒岩体的冷却抬升历史。分别得到辉石坪年龄为２．１６Ｇａ，封闭温度为６２０℃；角闪石坪年龄为１．９７Ｇａ，封闭温度为５１７℃；斜长石坪年龄为１．６６Ｇａ，封闭温度为２６５℃。从２．５Ｇａ（麻粒岩相变质年龄）到２．１６Ｇａ，岩体抬升速率为１４．１ｍ／Ｍａ，冷却速率为０．３９℃／Ｍａ；从２．１６Ｇａ到１．９７Ｇａ岩体抬升速率为１８．５ｍ／Ｍａ，冷却速率为０．５５℃／Ｍａ，从１．９７Ｇａ至１．６６Ｇａ岩体抬升速率为２９．１ｍ／Ｍａ，冷却速率为０．８１℃／Ｍａ。Ａｒ－Ａｒ法给出的这些同位素证据，反映了冀东太古代麻粒岩体变质作用晚期多阶段冷却抬升的漫长历史。 相似文献
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新疆要拉套山花岗岩类的K—Ar和^40Ar—^39Ar同位素定年 总被引：3，自引：1，他引：3
新疆西北部阿拉套山南坡的花岗岩体的＾４０Ａｒ－＾３９Ａｒ和Ｋ－Ａ定年结果表明它们都是海西期侵入体，侵入活动可分为三个阶段：最早的东部的岩基，岩性为花岗闪长岩和钾长花岗岩，年齿约３０５Ｍａ；而后是西部的二长花岗岩和钾长花岗岩，与钨锡成矿有关，年龄约２９０Ｍａ；最晚的是最西部的二长花岗岩，年龄约２８０－２７０Ｍａ。岩浆活动中心有自动东或北东向西或南西迁移的趋势。 相似文献
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浙江省陈蔡群的^40Ar—^39Ar年龄与变质年代 总被引：2，自引：0，他引：2
本文对陈蔡群变质岩进行了４０Ａｒ－３９Ａｒ年龄测定。其中在诸暨陈蔡测得的４１５．１Ｍａ的坪年龄代表了主变质晚期的冷却年代。采自义乌尚阳的样品受燕山期火山活动影响有明显的氩丢失，与主变质有关的年龄亦明显降低，仅３１５．３Ｍａ。在龙泉东书获得的年龄谱和当地广泛发育的混合岩化作用有关，２７６．９Ｍａ的坪年龄为这次热事件的冷却年代。根据对现有年代资料的讨论，可以认为不同衰变体系记录了陈蔡群主变质事件的演化。Ｒｂ－Ｓｒ体系在变质早中期实现均匀化，年龄值为５５２．４～６６０．６Ｍａ。锆石、磷灰石在变质高峰期形成的铅丢失年龄为５０８，４～５７８Ｍａ。上述资料表明陈蔡群主变质年代属加里东期。 相似文献
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青藏高原西部的抬升速率：叶城—狮泉河花岗岩^40Ar—^39Ar年龄的地质解释 总被引：19，自引：2，他引：17
通过对叶城－狮泉河剖面花岗岩中黑云母４０Ａｒ－３９Ａｒ法年龄研究,获得西昆仑北岩带库地岩体海拔高度２９５０ｍ和２８５０ｍ黑云母的封闭年龄分别为３９６．９Ｍａ和３８８．９Ｍａ,西昆仑南岩带塔西土路克、三十里营房和奇台大坂岩体黑云母的封闭年龄为１９５．８～１８３．９Ｍａ,班公湖－喀喇昆仑北岩带日土岩体黑云母封闭年龄为８０．３～７９．６Ｍａ,其时代分别为加里东期、印支期和燕山晚期。年龄结果表明,同一岩体海拔高的黑云母封闭年龄大于海拔低的黑云母封闭年龄,根据海拔高程差和坪年龄差计算出岩体的抬升速率,表明青藏高原西部从加里东期到燕山晚期,隆起速度有增大的趋势,而且具脉动性。 相似文献
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连续激光探针质谱^40Ar／^39Ar法测定单颗粒矿物年龄 总被引：14，自引：0，他引：14
Ｎｄ：ＹＡＧ激光器与高精密ＭＭ１２００质谱计－电子倍增器连网，应用连续激光质谱对单颗粒矿物、光片样品进行微区４０Ａｒ／３９Ａｒ测年、坪年龄和等时线年龄研究。在光片上测定南极乔治王岛（Ｋｉｎｇ Ｇｅｏｒｇｅ Ｉｓｌａｎｄ Ａｎｔａｒｃｔｉｃａ）北海岸玄武岩等时线年龄（５２．３８±１．０５Ｍａ）和贵州绿豆岩年龄（２３９．１６±１４．１３Ｍａ），两者与实际地质背景吻合。对两个中生代和太古宙单颗粒黑云母进行连续激光质谱阶段升温（４０）Ａｒ／（３９）Ａｒ坪年龄谱测定，获得与常规法相一致的坪年龄谱。 相似文献
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K.A. Foland Jeffrey S. Linder Thomas E. Laskowski Norman K. Grant 《Chemical Geology》1984,46(3):241-264
Nine glauconite samples with relatively high K concentrations and which appear to be well crystallized using normal X-ray diffraction techniques have been studied using the method. The glauconite apparent ages exceed their KAr, RbSr and, in most cases, stratigraphic ages by substantial amounts. release spectra sometimes yield plateaus but these apparent ages have no geological significance. The results indicate that 39Ar is lost by recoil from mineral grains during neutron irradiation, consistent with previously reported observations. The amount of 39Ar loss was measured by isotope dilution for four samples and varied from 29% to 17%. In contrast, radiogenic 40Ar is quantitatively retained during irradiation. The very fine blades which make up glauconite grains yield the mineral susceptible to large amounts of 39Ar loss and unsuitable for dating. 相似文献
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激光显微探针~(40)Ar/~(39)Ar同位素定年 总被引：10，自引：0，他引：10
已有 5 0年历史的K Ar定年法 ,由于过剩Ar和Ar丢失的普遍发现 ,使其最广泛的应用面临着严重挑战。40 Ar/ 3 9Ar分步加热释氩法是常规K Ar定年法的发展 ,它克服了常规K Ar定年法的一些局限 ,又可以测定岩浆构造热事件。激光显微探针40 Ar/ 3 9Ar定年法是在 2 0世纪末把聚焦激光束应用在40 Ar/ 3 9Ar分步加热释氩法中而发展起来的一种定年方法。它既具有常规K Ar定年法和40Ar/ 3 9Ar分步加热释氩法的所有优越性 ,又把定年引入微观领域。特别是在 2 0世纪的最后几年 ,以激光显微探针40 Ar/ 3 9Ar定年方法的完善和精度的提高为标志 ,把K Ar年代学研究推向了一个新的里程碑。微区微量高精度高分辨定年 ,把定年时限扩展到人类历史范畴 ,精细的分析技术拓宽了年代学的应用范围 ,使之解决的地质问题更广泛和深入 ,并且开始冲击着地球科学中的某些热点和难点课题。 相似文献
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Marvin A. Lanphere 《Quaternary Research》2000,53(3):294
K–Ar and 40Ar/39Ar ages have been measured on nine mafic volcanic rocks younger than 1 myr from the Snake River Plain (Idaho), Mount Adams (Washington), and Crater Lake (Oregon). The K–Ar ages were calculated from Ar measurements made by isotope dilution and K2O measurements by flame photometry. The 40Ar/39Ar ages are incremental-heating experiments using a low-blank resistance-heated furnace. The results indicate that high-quality ages can be measured on young, mafic volcanic rocks using either the K–Ar or the 40Ar/39Ar technique. The precision of an 40Ar/39Ar plateau age generally is better than the precision of a K–Ar age because the plateau age is calculated by pooling the ages of several gas increments. The precision of a plateau age generally is better than the precision of an isotope correlation (isochron) age for the same sample. For one sample the intercept of the isochron yielded an 40Ar/36Ar value significantly different from the atmospheric value of 295.5. Recalculation of increment ages using the isochron intercept for the composition of nonradiogenic Ar in the sample resulted in much better agreement of ages for this sample. The results of this study also indicate that, given suitable material and modern equipment, precise K–Ar and 40Ar/39Ar ages can be measured on volcanic rocks as young as the latest Pleistocene, and perhaps even the Holocene. 相似文献
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Ar同位素体系定年矿物的封闭温度范围广,并且可以获得650℃～150℃温度段的非线性冷却历史,因此~(40)Ar/~(39)Ar热年代学成为研究地质体热演化历史过程中最有效的工具之一。但是由于矿物中Ar同位素扩散机制还有一些问题没有清楚地被认识,因此在一定程度上制约了~(40)Ar/~(39)Ar热年代学的发展。本文介绍了目前应用最广泛的两种~(40)Ar/~(39)Ar热年代学模式:多重扩散域模式和多路径扩散模式,讨论了它们的发展现状、存在的问题、可能解决的方法以及今后的发展方向。 相似文献
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The mineral separate GA1550 biotite has become an international standard for K/Ar and 40Ar/39Ar dating studies, although it was prepared as an intralaboratory standard at ANU to monitor tracer depletion from a gas pipette. It is one of a small number of samples that has been calibrated against 38Ar tracers, some of which had been mixed with known amounts of atmospheric argon, so that a so-called primary calibration has been performed. By measuring GA1550 biotite against additional tracers from the same batch we have determined the radiogenic argon content of this sample as 1.342 (± 0.007) × 10? 9 mol/g, and together with the measured K content of 7.645 (± 0.050) weight percent, we derive a best estimate for the K/Ar age as 98.5 ± 0.5 Ma, where the error is derived from averaging the ages determined relative to the 38Ar tracer. 相似文献
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P. Alexandre 《Geochimica et cosmochimica acta》2011,75(15):4260-4272
In the case of volume diffusion, the closure temperature of a mineral is function of, among other factors, the characteristic diffusion dimension, which can be approximated by the grain size of the mineral analysed for grains smaller than or similar in size to the diffusion domains. The theoretical possibility of single mineral grain size thermochronology had been demonstrated empirically in earlier studies, mostly using biotite. In order to examine the potential of this method, it was tested alongside the widely used multi-mineral 40Ar/39Ar thermochronology. The sample comes from the granitic McLean pluton, in the south section of the Grenville orogeny. Seven grain size separates of biotite (ranging between 90 and 1000 μm), eight size fractions of amphibole (between 63 and 1000 μm), and three size fractions of K-feldspar (250-600 μm) were extracted and dated by the laser step-heating 40Ar/39Ar method. The total gas ages obtained behave as theoretically predicted, with increasing ages for increasing grain sizes, including for K-feldspar, but with the exception of the smallest and the largest grains for biotite and amphibole. The calculated cooling rates are ca. 0.7 °C/Ma for K-feldspar, ca. 2.5 °C/Ma for biotite, and ca. 11 °C/Ma for amphibole, corresponding very well to a monotonic cooling of the McLean pluton. A quick initial thermal re-equilibration with the cooler host-rocks is followed by a much slower cooling on a thermal path parallel to that of the Frontenac Terrain situated immediately to the southeast. The validity of the single mineral grain size thermochronology is demonstrated by comparison with the thermal evolution of the adjacent units and with the cooling history derived from a multi-mineral thermochronology, suggesting that it can be routinely used. The application of this method can be hampered by insufficiently low analytical uncertainties. 相似文献
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激光显微探针40Ar/39Ar 定年方法研究 总被引：12，自引：0，他引：12
实验结果表明，在激光探针40Ar/36Ar年龄和常规40Ar/39Ar年龄之间有较好的吻合性，多次测定BSP-1角闪石国际标样年龄值大部分在2020-20900Ma之间，多次测定周口店花岗岩中ZBH-25国内标样年龄值大部分在130-135.9Ma。分析区域可小到30μm以下（激光束本身可被聚集到10μm以下）。研究表明，激光显微探针技术在下述工作中将是一个极有前途的工具①测定不易大量获取的样品年龄；②研究遭受多期地质历史事件作用因而有复杂Ar状态的岩石年代；③研究在岩石样品中填充在不同结构位置上的矿物年 相似文献
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The effects of deformation on radiogenic argon (40Ar∗) retentivity in mica are described from high pressure experiments performed on rock samples of peraluminous granite containing euhedral muscovite and biotite. Cylindrical cores, ∼15 mm in length and 6.25 mm in diameter, were drilled from granite collected from the South Armorican Massif in northwestern France, loaded into gold capsules, and weld-sealed in the presence of excess water. The samples were deformed at a pressure of 10 kb and a temperature of 600 °C over a period 29 of hours within a solid medium assembly in a Griggs-type triaxial hydraulic deformation apparatus. Overall shortening in the experiments was approximately 10%. Transmitted light and secondary and backscattered electron imaging of the deformed granite samples reveals evidence of induced defects and for significant physical grain size reduction by kinking, cracking, and grain segmentation of the micas.Infrared (IR) laser (CO2) heating of individual 1.5-2.5 mm diameter grains of muscovite and biotite separated from the undeformed granite yield well-defined 40Ar/39Ar plateau ages of 311 ± 2 Ma (2σ). Identical experiments on single grains separated from the experimentally deformed granite yield results indicating 40Ar∗ loss of 0-35% in muscovite and 2-3% 40Ar∗ loss in biotite. Intragrain in situ ultraviolet (UV) laser ablation 40Ar/39Ar ages (±4-10%, 1σ) of deformed muscovites range from 309 ± 13 to 264 ± 7 Ma, consistent with 0-16% 40Ar∗ loss relative to the undeformed muscovite. The in situ UV laser ablation 40Ar/39Ar ages of deformed biotite vary from 301 to 217 Ma, consistent with up to 32% 40Ar∗ loss. No spatial correlation is observed between in situ40Ar/39Ar age and position within individual grains. Using available argon diffusion data for muscovite the observed 40Ar∗ loss in the experimentally treated muscovite can be utilized to predict average 40Ar∗ diffusion dimensions. Maximum 40Ar/39Ar ages obtained by UV laser ablation overlap those of the undeformed muscovite, indicating argon loss of <1% and an average effective grain radius for 40Ar∗ diffusion ?700 μm. The UV laser ablation and IR laser incremental 40Ar/39Ar ages indicating 40Ar∗ loss of 16% and 35%, respectively, are consistent with an average diffusion radius ?100 μm. These results support a hypothesis of grain-scale 40Ar∗ diffusion distances in undeformed mica and a heterogeneous mechanical reduction in the intragrain effective diffusion length scale for 40Ar∗ in deformed mica. Reduction in the effective diffusion length scale in naturally deformed samples occurs most probably through production of mesoscopic and submicroscopic defects such as, e.g., stacking faults. A network of interconnected defects, continuously forming and annealing during dynamic deformation likely plays an important role in controlling both 40Ar∗ retention and intragrain distribution in deformed mica. Intragrain 40Ar/39Ar ages, when combined with estimates of diffusion kinetics and distances, may provide a means of establishing thermochronological histories from individual micas. 相似文献
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^40Ar／^39Ar测年中的冷却年龄和变形年龄 总被引：3，自引：1，他引：2
^40Ar／^39Ar法年龄数据的解释与Ar同位素在矿物中的封闭温度有关。冷却年龄只能限制变质——变形事件发生的时间区间,不能真正代表地质事件的发生时间。因此,必须想办法得到变形年龄。本文从封闭温度概念出发,探讨了压力、冷却速率、有效扩散范围和几何形态、颗粒大小、动力学参数等对矿物封闭温度的影响,介绍了新近提出的“封闭窗”概念,并讨论了在什么情况下可以获得变形年龄。 相似文献