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采用化学分析、X射线衍射分析和MLA矿物自动检测技术等手段,对湖北地区伴生稀土磷矿选矿精矿进行元素赋存特性研究,分析了该矿物的化学成分、矿物组成、稀土元素的赋存状态等理化特征。结果表明,稀土元素Ce、Nd、Sm主要赋存在独居石中,Gd、La全部赋存在独居石中,Dy则全部赋存在磷灰石矿物中,Pr全部赋存在磷灰石和独居石的复合矿物中,Y主要赋存在易解石中。独居石是含有稀土元素最多的矿物。磷灰石与稀土矿物相互交生,独居石主要呈稀疏星散浸染状充填于黑云母、萤石和赤铁矿等脉石矿物的粒间、边缘及孔洞中,多数粒度过于细小而与脉石构成极为复杂的镶嵌关系。 相似文献
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独居石成因特征与U-Th-Pb定年及三江特提斯构造演化研究例析 总被引：8，自引：7，他引：1
独居石U-Th-Pb定年在地质年代学研究中占有重要地位,但其成因类型的识别和年龄值的合理地质解释始终是研究的难点。论文通过对比分析岩浆、热液和沉积成因独居石的内部结构、矿物组合以及稀土和微量元素地球化学特征,厘定了不同成因类型独居石的鉴别标志;并以三江特提斯构造演化研究为例,探讨了独居石的U-Th-Pb定年及其合理地质应用。不同地质环境中形成的独居石具有不同的内部结构和矿物组合及元素组成:岩浆独居石可能存在较宽且平直的岩浆环带,常与磷钙钍石共生;相对富集重稀土,具有较高的Y、Sc、Th、U、Sm、Gd等含量和Th/U比值,较低的La、Ce含量和稀土总量,显示为Eu强烈亏损的右倾斜分布模式。而热液独居石可能存在与流体作用有关的扇形环带,常与斜钍石共生;沉积独居石形态多不规则,与自生矿物相伴生。它们具有典型的四分组稀土分布模式,稀土总量较高,相对富集轻稀土(如La、Ce),贫Y、Sc、Th、U、Sm、Gd等,Th/U比值较低。独居石U-Th-Pb定年限定了松潘-甘孜造山带204~190Ma的早期变质作用和168~158Ma的局部热干扰,约140~130Ma冈底斯浅色花岗岩的形成与地壳的缩短加厚及快速隆升作用,约33~22Ma 红河断裂带与伸展作用有关的岩体侵位和左行走滑运动年代(且北部的去顶剥蚀作用要比中部早9Ma),约8~11Myr的东喜马拉雅构造结"挤出"构造变形时限。 相似文献
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东升庙矿床黄铁矿成因矿物学的研究 总被引：1，自引：0，他引：1
东升庙矿床中,从原始沉积—区域变质作用都有黄铁矿的形成。根据黄铁矿的产状、共生组合及结构构造相互关系,可划分出微晶黄铁矿、结核状黄铁矿、同心环状胶黄铁矿、重晶粗粒黄铁矿和脉状黄铁矿等五种类型。对黄铁矿化学分析、微量元素分析、晶脆参数和反射率测定均显示了五类黄铁矿成因差异的标型特征。 黄铁矿成因矿物学研究表明,该区矿化经历了原始沉积—热卤水成矿—变质重结晶及受后期岩浆作用影响局部活化等四个阶段。成矿作用表现由原始沉积向热卤水沉积成矿过渡的矿床类型。区域变质作用和局部活化只是对矿床产生了不同程度的改造,使矿体进一步富集。 相似文献
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分析了海南岛燕山晚期典型的屯昌岩体、千家岩体和保城岩体中的钾长石、斜长石、黑云母和角闪石的化学成分和成因特点。结果表明:(1)多数钾长石晶体的Or含量<90,具岩浆结晶成因特征。大部分斜长石属奥长石-中长石,An含量与岩石的SiO2成负相关关系,显示岩浆发生了较高程度的结晶分异作用。(2)黑云母为镁质黑云母,主要为岩浆结晶成因,部分为耐熔残余。角闪石均为钙质角闪石类,既有岩浆成因角闪石,也有次生交代成因角闪石,以相对贫铝、富镁、(Na+K)A低为显著特点。(3)岩体最终定位深度可能≤3.3km,温度≥750°C,具深源、高温、浅侵位特征。 相似文献
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近年来,在秦岭造山带宁陕伟晶岩区发现了数条Be-Nb稀有金属伟晶岩矿脉。本文通过扫描电镜和电子探针分析了Be-Nb伟晶岩中独居石的矿物学特征和矿物成分。研究结果表明,伟晶岩脉中的独居石可分为两类:Ⅰ类独居石主要分布在石英、长石等造岩矿物内部,在背散射图像中多数Ⅰ类独居石内部均匀,部分可见振荡环带,具有较高的Th O2含量(7.0%～13.9%,平均10.5%);Ⅱ类独居石单矿物在背散射图像下同样显示内部均匀,但亮度明显低于Ⅰ类独居石,且Th O2含量较低(0.9%～4.4%,平均2.2%)。这指示了Ⅰ类独居石的岩浆成因和Ⅱ类独居石的热液成因。岩浆成因独居石具有较高的Th O2含量与独居石中磷钙钍石的类质同象替代密切相关。岩浆成因独居石的U-Pb测年结果为200.8±2.1 Ma,代表伟晶岩的成岩年龄,该年龄结果接近宁陕岩基中的二长花岗岩。岩浆和热液成因独居石的εNd值的范围为4.6～3.0,这与二长花岗岩的εNd值范围基本一致,说明区内Be-Nb伟晶岩与上述二长花岗岩的同源性。综上所述,本研究认为宁陕地区Be-Nb伟晶岩... 相似文献
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独居石微粒微区成分分布的研究 总被引：8，自引：0，他引：8
采用电子探针(EPMA)分析研究了花岗岩、伟晶岩 和热液交 代等三种不同成因的独居石微粒微区成分分布的特征。分析数据表明,花岗岩和花岗伟晶岩 成因的独居石微粒中La和Ce的含量低, 而Sm、Gd、Y、Th的含量明显较高。热液交代成因的 独居石微粒中,La、Ce的含量高,而Gd、Th、Y的含量明显较低。根据微区剖面(0.18mm)元 素分布曲线,指出了La、Ce、Nd、P、Th、Si、Ca和U等元素表现出8～10个微环带成分不均匀分布的特点,并认为成矿溶液的地质环境、温压和微量元素含量变化是不均匀分布的主要 原因。 相似文献
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福建漳州复式岩体磁铁矿的成因矿物学特征 总被引：6，自引：0，他引：6
漳州花岗岩岩基共分两期七次(Ⅰ-Ⅶ)侵入,是中国东南沿海燕山晚期有代表性的大型复式岩体。笔者对区内各类花岗岩磁铁矿作了较深入的矿物学工作,包括晶出产状、晶体形态、X射线衍射、红外谱学、化学成分及稀土元素地球化学等方面的研究。本文重点论述磁铁矿的标型特征及成因意义,并提出区分不同成因花岗岩类岩石磁铁矿矿物学的判别标志,结合副矿物组合及岩石化学特点,对区内早、晚两期花岗岩类的成因分别判别为I型和A型花岗岩。 相似文献
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Simultaneously in-situ analyses of U–Pb isotopes and trace elements were carried out for zircons, in combination with the in-situ analyses of trace elements in coexisting minerals, from low-T/UHP metagranite in the Dabie orogen. The results provide geochemical evidence for the existence of supercritical fluid during continental subduction-zone metamorphism. The zircons are categorized into three types based on their patterns of REE distribution. Type I zircons show increasing enrichment from La to Lu, with prominent positive Ce anomalies and negative Eu anomalies, which are typical of magmatic zircon. Some of them display regular or blurred oscillatory-zoned texture and apparent 206Pb/238U ages of 341 to 780 Ma, suggesting metamorphic modification by solid-state recrystallization with no significant involvement of metamorphic fluid. Type II zircons share similar Th, U and HFSE contents and REE patterns to Type I zircons. However, they exhibit blurred oscillatory-zoned texture or are unzoned, have apparent 206Pb/238U ages of 348 to 709 Ma, and are LREE-enriched relative to Type I zircons. This suggests that they underwent metamorphic reworking by replacement recrystallization in the presence of metamorphic fluid. The LREE enrichment is due to the presence of microscale LREE-bearing mineral inclusions (such as apatite, monazite or epidote) in the zircons. Type III zircons, representing the majority of the present analyses, are characterized by spongy texture and consistent enrichment of LREE, HREE, Th, U and HFSE relative to Type I zircons. They yield nearly concordant U–Pb ages close to the discordia lower-intercept. The consistent enrichment of trace elements relative to the magmatic zircon indicates involvement of a special UHP metamorphic fluid that has a strong capacity to extract significant amounts of LREE, HREE, Th, U and HFSE from such accessory minerals as allanite, garnet, rutile and zircon. Because these minerals are stable in the field of hydrous melt in granite–water systems, they are not able to be decomposed during the exhumation of deeply subducted continental crust. Thus, a supercritical fluid is suggested to transport the LREE, HREE, Th, U and HFSE in the accessory minerals to recrystallized zircons. The mechanism of dissolution recrystallization is responsible for the spongy texture and the very high concentration of trace elements in this type of metamorphic zircons. Therefore, the action of supercritical fluid is evident under the low-T/UHP metamorphic conditions. 相似文献
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Zircon U–Pb ages and trace elements were determined for granulites and gneiss at Huangtuling, which are hosted by ultrahigh-pressure metamorphic rocks in the Dabie Orogen, east-central China. CL images reveal core–rim structure for most zircons in the granulites. The cores show oscillatory zoning, relatively high Th/U ratios, and HREE enriched patterns, consistent with a magmatic origin. They gave a weighted mean 207Pb/206Pb age of 2766 ± 9 Ma, interpreted as dating magma emplacement of the protolith. The rims are characterized by sector or planar zoning, low Th/U ratios, negative Eu anomalies and flat HREE patterns, consistent with their formation under granulite-facies metamorphic conditions. Zircon U–Pb dating yields a weighted mean 207Pb/206Pb age of 2029 ± 13 Ma, which is interpreted to record a metamorphic event, possibly during assembly of the supercontinent Columbia. The gneiss has a protolith age of 1982 ± 14 Ma, which is younger than the zircon age of the granulite-facies metamorphism, suggesting a generally delay between HT metamorphism and the intrusion of post-collisional granites. A few inherited cores with igneous characteristics have 207Pb/206Pb ages of 2.90, 3.28 and 3.53 Ga, suggesting the presence of Mesoarchean to Paleoarchean crustal remnants in the Yangtze Craton. A few Cretaceous metamorphic ages were also obtained, suggesting the influence of post-collisional collapse in response to Cretaceous extension of the Dabie Orogen. It is inferred that the recently discovered Archean basement of the Yangtze Craton occurs as far north as the Dabie Orogen. 相似文献
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滇西梁河地区钾长花岗岩锆石LA-ICP-MS U-Pb定年及其地质意义 总被引：4，自引：0，他引：4
在详细区域地质调查的基础上,对滇西梁河地区具有代表性的两件钾长花岗岩样品中的锆石进行了阴极发光图像、微区原位LA-ICP-MS微量元素分析和U-Pb定年。结果表明,梁河地区钾长花岗岩锆石显示振荡环带的内部结构,指示其岩浆成因;两件样品的锆石具有较高的Th、U含量,稀土元素总量较高,轻稀土亏损、重稀土富集,明显的的Ce正异常和Eu负异常的稀土配分模式,说明其壳源岩浆锆石特征;两件样品的锆石206Pb/238U加权平均年龄分别是(60.7±0.6)Ma和(115.8±1.0)Ma,属古新世和早白垩世花岗岩。结合区域地质特征,腾冲地块在中生代晚期-新生代早期发生多期岩浆作用,揭示滇西三江地区特提斯演化的岩浆响应,为青藏高原东缘地区地质演化的动力过程提供约束。 相似文献
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不同成因锆石阴极发光及微量元素特征:以新疆阿尔泰地区花岗岩和伟晶岩为例 总被引：2，自引：0，他引：2
新疆阿勒泰可可托海地区出露大量花岗岩和伟晶岩脉,利用阴极发光显微照相(CL)、电子探针背散射(BSE)和激光剥蚀电感耦合等离子质谱技术(LA-ICP-MS),观察和分析岩石中锆石的内部结构、稀土元素及Th,U含量后结果表明:该区花岗岩锆石具振荡环带和强烈的阴极发光特征,Th/U比值较高(Th/U=0.16～0.99),轻稀土亏损、重稀土富集,具较大的Ce正异常,为典型岩浆成因锆石。伟晶岩(KP-08-11)锆石为热液锆石,不具振荡环带和阴极发光,具低的Th/U比值(0.01～0.13),强烈富集稀土元素,尤其是轻稀土元素较花岗岩锆石高一个数量级,Ce的正异常相对较低。伟晶岩(KP3-08-1)锆石为变质重结晶锆石,Th/U比值分布范围较广(0.01～0.78),强烈亏损稀土元素,稀土元素配分模式存在显著的"REE四分组效应"。微量元素特征表明,伟晶岩(KP-08-11)锆石可能结晶自富U贫Th的残余岩浆流体,而伟晶岩(KP3-08-1)的锆石经历了蜕晶质化和变质重结晶作用,但依然保持了共存伟晶岩熔体的微量元素特征。 相似文献
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点苍山-哀牢山杂岩带多期变质作用:嘎洒地区变沉积岩锆石微量元素与U-Pb年代学制约 总被引：2，自引：2，他引：0
点苍山-哀牢山杂岩带位于青藏高原东南缘,为云南三江地区一条重要的造山带,由扬子板块和印支板块于晚二叠世-中晚三叠世碰撞拼合而成。杂岩带主要由各类副片麻岩、片岩、石英岩、大理岩和斜长角闪岩构成,岩石发育强烈糜棱岩化和深熔作用。本文选取哀牢山北段新平嘎洒地区变沉积岩为研究对象,通过对变沉积岩锆石的阴极发光图像、微量元素、矿物包裹体组合、表面形态和U-Pb年龄的综合研究,揭示出嘎洒地区哀牢山杂岩经历了两期变质事件:其中,含石榴子石斜长二云母片岩中30颗变质锆石获得了较为一致的206Pb/238U年龄215±6Ma~227±5Ma,加权平均年龄为222.3±1.2Ma(n=30,MSWD=0.27),这些锆石具有浑圆状或椭圆状形态、较为均匀的阴极发光图像、平坦的HREE配分模式((Lu/Gd)N=0.73~4.08)和弱的负Eu异常,这些特征与典型的高级变质岩中变质锆石相似,而锆石的Th/U比值较为分散为0.06~0.84,平均值为0.45,可能与变质过程中富Th矿物独居石分解有关。变质年龄与杂岩带中点苍山和元阳地区变质岩中、晚三叠世变质年龄极为吻合,指示这期变质事件与中-晚三叠世古特提斯洋闭合-造山有关,标志着点苍山-哀牢山杂岩带为三江地区一条重要的古缝合线。此外,嘎洒地区夕线石榴黑云二长片麻岩的岩相学特征显示,岩石经历了石榴子石的转熔作用,除两颗锆石年龄为35.4Ma外,28颗锆石(增生边)给出了误差范围内较为一致的206Pb/238U年龄(27.3±0.5Ma~31.9±0.5Ma),加权平均年龄为29.4±0.53Ma(n=28,MSWD=2.0)。这些锆石的增生边中的矿物包裹体组合为夕线石+钾长石+黑云母+石英+独居石,且具有较低的Th/U比值(0.01~0.1),平坦的重稀土(HREE)配分模式((Lu/Gd)N=0.45~7.59)和中等程度的负Eu异常,这些特征指示该类锆石为典型的变质锆石。变质年龄与新生代红河-哀牢山剪切带内大量发现的同剪切岩浆岩、变质岩的年龄较为一致,指示这期年轻的变质事件与岩石圈尺度大规模剪切运动有关。此外,两类变沉积岩中6颗继承性碎屑锆石的年龄分布范围为528~783Ma,这些锆石具有锥形的锆石形态,清晰的振荡环带,表面发育蚀痕和凹坑,较高的Th/U比(0.1),陡倾的HREE配分曲线,表明这些锆石为经过剥蚀-搬运-沉积的岩浆锆石,具有继承性碎屑锆石的特征,说明哀牢山杂岩变沉积岩中至少应包含新元古代和早古生代的沉积物源,指示研究区哀牢山杂岩带部分岩石并不属于真正意义上的扬子结晶基底。 相似文献
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Eclogite origin and timings in the North Qinling terrane,and their bearing on the amalgamation of the South and North China Blocks 总被引：3，自引：0，他引：3
H. WANG Y.‐B. WU S. GAO X.‐C. LIU H.‐J. GONG Q.‐L. LI X.‐H. LI H.‐L. YUAN 《Journal of Metamorphic Geology》2011,29(9):1019-1031
The amalgamation of South (SCB) and North China Blocks (NCB) along the Qinling‐Dabie orogenic belt involved several stages of high pressure (HP)‐ultra high pressure (UHP) metamorphism. The new discovery of UHP metamorphic rocks in the North Qinling (NQ) terrane can provide valuable information on this process. However, no precise age for the UHP metamorphism in the NQ terrane has been documented yet, and thus hinders deciphering of the evolution of the whole Qinling‐Dabie‐Sulu orogenic belt. This article reports an integrated study of U–Pb age, trace element, mineral inclusion and Hf isotope composition of zircon from an eclogite, a quartz vein and a schist in the NQ terrane. The zircon cores in the eclogite are characterized by oscillatory zoning or weak zoning, high Th/U and 176Lu/177Hf ratios, pronounced Eu anomalies and steep heavy rare earth element (HREE) patterns. The zircon cores yield an age of 796 ± 13 Ma, which is taken as the protolith formation age of the eclogite, and implies that the NQ terrane may belong to the SCB before it collided with the NCB. The ?Hf(t) values vary from ?11.3 to 3.2 and corresponding two‐stage Hf model ages are 2402 to 1495 Ma, suggesting the protolith was derived from an enriched mantle. In contrast, the metamorphic zircon rims show no zoning or weak zoning, very low Th/U and 176Lu/177Hf ratios, insignificant Eu anomalies and flat HREE patterns. They contain inclusions of garnet, omphacite and phengite, suggesting that the metamorphic zircon formed under eclogite facies metamorphic conditions, and their weighted mean 206Pb/238U age of 485.9 ± 3.8 Ma was interpreted to date the timing of the eclogite facies metamorphism. Zircon in the quartz vein is characterized by perfect euhedral habit, some oscillatory zoning, low Th/U ratios and variable HREE contents. It yields a weighted mean U–Pb age of 480.5 ± 2.5 Ma, which registers the age of fluid activity during exhumation. Zircon in the schist is mostly detrital and U–Pb age peaks at c. 1950 to 1850, 1800 to 1600, 1560 to 1460 and 1400 to 1260 Ma with an oldest grain of 2517 Ma, also suggesting that the NQ terrane may have an affinity to the SCB. Accordingly, the amalgamation between the SCB and the NCB is a multistage process that spans c. 300 Myr, which includes: the formation of the Erlangping intra‐oceanic arc zone onto the NCB before c. 490 Ma, the c. 485 Ma crustal subduction and UHP metamorphism of the NQ terrane, the c. 430 Ma arc‐continent collision and granulite facies metamorphism, the 420 to 400 Ma extension and rifting in relation to the opening of the Palaeo‐Tethyan ocean, the c. 310 Ma HP eclogite facies metamorphism of oceanic crust and associated continental basement, and the final 250 to 220 Ma continental subduction and HP–UHP metamorphism. 相似文献
18.
柴北缘鱼卡河榴辉岩围岩的变质时代及其地质意义 总被引：17，自引：1，他引：16
利用阴极发光和LA-ICP-MS原位分析方法,对柴北缘鱼卡河超高压榴辉岩的直接围岩——石榴石白云母角闪钠长片麻岩和含蓝晶石的石榴石云母片岩进行了详细的锆石微量元素和U-Th-Pb同位素分析。结果表明,石榴石白云母角闪钠长片麻岩中的锆石主体呈浑圆状形态,内部结构以扇状和冷杉树状为主,稀土总量和重稀土含量均较低,重稀土富集程度低,具明显正Eu异常,Th/U比值均小于0.1,指示其形成在与石榴石平衡共生而不含斜长石的变质条件下。而含蓝晶石的石榴石云母片岩中的锆石显示明显的核-边结构,核部显示碎屑锆石特征,边部为与石榴石共生的变质新生锆石。LA-ICP-MS原位定年获得两种围岩的峰期变质年龄分别为(431±3)Ma和(432±19)Ma。这两组年龄在误差范围内一致,而且与已获得的紧邻的两类超高压榴辉岩的变质年龄((436±3)Ma和(431±4)Ma)以及带内指示大陆深俯冲作用时代的都兰含柯石英副片麻岩锆石的柯石英微区年龄(424~432Ma)完全一致。参考这两类岩石与超高压榴辉岩的野外产状关系、含蓝晶石的石榴石云母片岩的原岩特征以及榴辉岩中超过变质年龄达300Ma的原岩残核的存在,共同表明,柴北缘鱼卡河超高压变质地体是典型的大陆深俯冲碰撞作用的产物,本区大陆深俯冲发生的时代为430~435Ma的早古生代。 相似文献
19.
Dehydration and anatexis of ultrahigh‐pressure (UHP) metamorphic rocks during continental collision are two key processes that have great bearing on the physicochemical properties of deeply subducted continental crust at mantle depths. Determining the time and P–T conditions at which such events take place is needed to understand subduction‐zone tectonism. A combined petrological and zirconological study of UHP metagranite from the Sulu orogen reveals differential behaviours of dehydration and anatexis between two samples from the same UHP slice. The zircon mantle domains in one sample record eclogite facies dehydration metamorphism at 236 ± 5 Ma during subduction, exhibiting low REE contents, steep MREE–HREE patterns without negative Eu anomalies, low Th, Nb and Ta contents, low temperatures of 651–750 °C and inclusions of quartz, apatite and jadeite. A second mantle domain records high‐T anatexis at 223 ± 3 Ma during exhumation, showing high REE contents, steeper MREE–HREE patterns with marked negative Eu anomalies, high Hf, Nb, Ta, Th and U contents, high temperatures of 698–879 °C and multiphase solid inclusions of albite + muscovite + quartz. In contrast, in a second sample, one zircon mantle domain records limited hydration anatexis at 237 ± 3 Ma during subduction, exhibiting high REE contents, steep MREE–HREE patterns with marked negative Eu anomalies, high Hf, Nb, Ta, Th and U contents, medium temperatures of 601–717 °C and multiphase solid inclusions of albite + muscovite + hydrohalite. A second mantle domain in this sample records a low‐T dehydration metamorphism throughout the whole continental collision in the Triassic, showing low REE contents, steep MREE–HREE patterns with weakly negative Eu anomalies, low Th, Nb and Ta contents, low temperatures of 524–669 °C and anhydrite + gas inclusions. Garnet, phengite and allanite/epidote in these two samples also exhibit different variations in texture and major‐trace element compositions, in accordance with the zircon records. The distinct P–T–t paths for these two samples suggest separate processes of dehydration and anatexis, which are ascribed to the different geothermal gradients at different positions inside the same crustal slice during continental subduction‐zone metamorphism. Therefore, the subducting continental crust underwent variable extents of dehydration and anatexis in response to the change in subduction‐zone P–T conditions. 相似文献
20.
本文通过对南阿尔金巴什瓦克基性麻粒岩中长英质脉体的岩相学、锆石U-Pb年代学、Lu-Hf同位素及全岩主微量地球化学的综合研究,首次限定了该区基性麻粒岩中长英质脉体的形成时代为491±2 Ma (MSWD=0.91),此年龄与寄主麻粒岩高压—超高温阶段(榴辉岩相)的变质时代在误差范围内近一致,表明长英质脉体形成于榴辉岩相的变质阶段。由于长英质脉体中锆石明显不同于寄主基性麻粒岩中变质锆石的形态特征,基本排除了长英质脉体中的锆石为捕获锆石的可能性。此外,该长英质脉体中的锆石具有少量的长石、石英包裹体和较低的Th/U比值(0.05-0.41),锆石稀土元素配分模式图显示其具有重稀土富集和Eu负异常的特征,这些证据表明长英质脉体中的锆石可能结晶于变质熔体之中。长英质脉体的全岩地球化学特征显示其该脉体具有相对较低的K2O值,基本上排除了其来源于围岩长英质麻粒岩的可能,而且这些锆石的Hf同位素特征与寄主岩石的锆石Hf同位素特征具有相似性,表明形成长英质脉体的熔体为内部来源。结合全岩地球化学特征,推测其可能为基性麻粒岩发生部分熔融所致。 相似文献