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1.
为提高页岩油气钻进过程中钻头表面的耐磨性能及防泥包性能,采用冷喷涂(CS)和超音速火焰喷涂(HVAF)技术在35CrMo钢基体上制备了Fe48Cr15Mo14C15B6Y2非晶合金涂层,并利用紫外激光制备了涂层的疏水表面,利用扫描电子显微镜(SEM)、X射线能谱仪(EDS)、X射线衍射仪(XRD)测试分析了涂层的微观结构和力学性能,利用接触角测量仪表征涂层的润湿性,并分析其润湿机理。结果表明:利用CS技术制备的Fe基非晶合金涂层结构更加致密,非晶质量分数达到90%,且具有更好的热稳定性。激光过程中的熔融物快速冷却在涂层表面形成纳米尺寸级别的凝结物以及团聚物形成微纳复合结构,在激光扫描次数为7次时,CS涂层表面水接触角最高,具有良好的疏水性。  相似文献   

2.
深部地质钻探过程中,复杂的井下工况对钻具的钻探性能以及可靠性提出了苛刻的要求。钻具钢体表面涂覆具有耐磨耐蚀性的非晶涂层可以有效提高其服役寿命。其中Fe基非晶合金涂层因其优异的耐腐蚀抗磨损性能、较强的非晶形成能力等优势,具有重要的应用价值和较好的经济效益。本文通过大气等离子喷涂技术(Air Plasma Spray, APS)在35CrMo基体上制备得到成分为Fe48Cr15Mo14C15B6Y2 (at.%)的非晶合金涂层,并对其进行不同温度的真空热处理,探究了不同温度热处理对涂层基本性能和磨损失效机制的影响。结果表明:涂层经过真空热处理之后,生成的大量硬质相和成分均匀化使得涂层抗磨损性能提高;且随着热处理温度的提高,涂层磨损率逐渐减小。与未经热处理和750 ℃热处理的涂层相比,经过850 ℃热处理之后的涂层具有最佳的抗磨损性能,磨损率仅为未经热处理的Fe基非晶涂层的16.7%。热处理前后涂层的失效机制均为粘着磨损、磨粒磨损、疲劳磨损和氧化磨损。  相似文献   

3.
应用离子渗氮与离子渗硫技术,在钻杆接头材料35CrMo钢表面制备了硫氮复合处理层。采用M-200环块磨损试验机,对比研究了原始渗氮表面与硫氮复合表面在干摩擦条件下的抗磨损性能。结果表明,在干摩擦的条件下,由于摩擦副的接触表面缺乏润滑,硬度较高的渗氮层会加剧接触表面的磨损。而硫氮复合处理层由于在表面存在一层硫化亚铁固体润滑层,在磨损过程中可以起到一定的润滑作用,因此其在干摩擦条件下具备更好的抗磨损性能。  相似文献   

4.
为提高钻探装备用低碳高强钢材料的力学性能,可通过调节不同热处理回火温度以获得不同材料组织成分来有效实现。分别以610、630、650℃为试验设定热处理回火温度,并利用金相显微镜(OM)、扫描电镜(SEM)对回火后低碳高强钢材料显微组织进行对比分析;利用显微硬度仪、万能材料试验机、冲击试验机对试验材料显微组织硬度、拉伸性能及抗冲击性进行试验测试。研究结果表明:经过调质处理后的材料性能较原材料有所提升。当回火温度为610℃时,显微组织为回火马氏体+回火索氏体,其屈服强度最高为1 020 MPa,显微硬度为332 HV,且具有较好的塑性。随着回火温度的增加,显微组织发生回复,转变为回火索氏体。此时其屈服强度与抗拉强度下降,冲击功提升,650℃下冲击功最高。随着回火温度的变化,冲击与拉伸断口呈现出韧性断裂、准解理断裂以及混合断裂多种失效形式。回火工艺可有效提升该低碳高强钢的力学性能,且该工艺在生产中易得到大面积使用。   相似文献   

5.
王成彪  吴晓光 《现代地质》1996,10(4):558-561
5#钢泥浆泵缸套内工作表面,以碳化钨硬相镍基涂层进行真空熔烧强化处理,大幅度提高了缺套的耐磨料磨损性能。对涂层的显微组织结构及机械性能进行了试验分析,并给出了涂层缸套现场使用的试验结果  相似文献   

6.
铌铁锐钛矿是含铌、铁的锐钛矿变种。呈土黄色、褐棕色,板状或土粒状。反射率589nm,15.9%,显微硬度H_v=275.9kg/mm~2。计算比重4.4g/cm~3。主要化学成分Nb_2O_534.92—44.3%,TiO_2 29.38—37.58%,Fe_2O_3 14.94—17.19%。化学式:(Ti_(0.44)Nb_(0.31)Fe_(0.25))_(1.00)O_2X射线分析表明该矿物属四方晶系,α=3.828±0.002,c=9.682±0.009,空间群I4_1/amd,Z=4。 共生矿物钕易解石,深红色者变生现象轻微;浅黄色钕易解石与铌铁锐钛矿可能形成于稍晚、较低温度条件下的矿化过程。  相似文献   

7.
针对铝合金钻杆耐磨性和耐腐蚀性差导致其难以在深部钻井中应用的技术难题,本文以7075铝合金粉作为基体,玄武岩短纤维作为增强体,利用真空热压烧结技术制备了玄武岩纤维增强型铝基复合材料,并对其微观组织结构、密度和显微硬度等性能进行了研究。结果表明,玄武岩纤维在铝基体中分散均匀,界面处发生了化学渗透,SiO2和Al之间发生置换反应,从而获得了良好的界面结合强度,复合材料的密实度较高,玄武岩纤维的加入显著提高了复合材料的显微硬度。  相似文献   

8.
本文以CdCl_2·2.5H_2O为反应剂,采用“下垫上滴”缓冲刺的装样形式,通过大量镉盐的蒸发控制电极温度,使被测元素预先分馏,有效地改善了它们的蒸发行为,同时,减小了基体效应、光谱背景。本法其有良好的精密度和准确度,各元素的检出限(×10~(-5))分别为:Pb(1),Sn(0.37),Cr(1.8),Ni(3.51,Mo(0.1)和Co(0.38),其相对标准偏差(RSD)为±3.7—9.5%  相似文献   

9.
采用功率为2kW、扫描速度为100mm/min的工艺参数对钻杆接头材料30CrMnSiA钢进行了表面相变硬化处理,研究了相变层的组织和硬度特征,实验结果表明,30CrMnSiA钢表面相变硬化层分为完全淬硬层,过渡层和受热影响的基体组织,硬化层的显微组织明显细化,其表面层的硬度比高频淬火的硬度提高了30%,淬硬层深度达1.7mm,比高频淬火深度提高近1倍。  相似文献   

10.
刘冀 《探矿工程》2021,48(5):47-53
为提高金刚石钻头钻进钢筋混凝土、强磨性岩层的钻进效率,选择了一种耐磨性高、冷压成型好的铁预合金粉。本文设计了铁基胎体配方,研究了铁基预合金粉、Cu、Ni、Co各成分对铁基金刚石钻头胎体及钻进性能的影响。测试了不同配方下烧结试样的抗拉强度、三点抗弯强度和硬度,使用扫描电镜对断口进行微观分析,通过现场钻进实验测试钻头的钻进效率与寿命。同时分析了保温时间对铁基胎体力学性能的影响。结果表明:Cu、Ni、Co对铁基胎体的抗弯强度和硬度影响较大,且保温时间为5 min时,铁基胎体可以获得较好的力学性能。  相似文献   

11.
Pant-y-ffynnon Quarry in South Wales yielded a rich cache of fossils in the early 1950s, including articulated specimens of new species (the small sauropodomorph dinosaur Pantydraco caducus and the crocodylomorph Terrestrisuchus gracilis), but no substantial study of the wider fauna of the Pant-y-ffynnon fissure systems has been published. Here, our overview of existing specimens, a few described but mostly undescribed, as well as freshly processed material, provides a comprehensive picture of the Pant-y-ffynnon palaeo-island of the Late Triassic. This was an island with a relatively impoverished fauna dominated by small clevosaurs (rhynchocephalians), including a new species, Clevosaurus cambrica, described here from a partially articulated specimen and isolated bones. The new species has a dental morphology that is intermediate between the Late Triassic Clevosaurus hudsoni, from Cromhall Quarry to the east, and the younger C. convallis from Pant Quarry to the west, suggesting adaptive radiation of clevosaurs in the palaeo-archipelago. The larger reptiles on the palaeo-island do not exceed 1.5?m in length, including a small carnivorous crocodylomorph, Terrestrisuchus, and a possible example of insular dwarfism in the basal dinosaur Pantydraco.  相似文献   

12.
Robert L. Linnen   《Lithos》2005,80(1-4):267-280
The solubilities of columbite, tantalite, wolframite, rutile, zircon and hafnon were determined as a function of the water contents in peralkaline and subaluminous granite melts. All experiments were conducted at 1035 °C and 2 kbar and the water contents of the melts ranged from nominally dry to approximately 6 wt.% H2O. Accessory phase solubilities are not affected by the water content of the peralkaline melt. By contrast, solubilities are affected by the water content of the subaluminous melt, where the solubilities of all the accessory phases examined increase with the water content of the melt, up to 2 wt.% H2O. At higher water contents, solubilities are nearly constant. It can be concluded that water is not an important control of accessory phase solubility, although the water content will affect diffusivities of components in the melt, thus whether or not accessory phases will be present as restite material. The solubility behaviour in the subaluminous and peralkaline melts supports previous spectroscopic studies, which have observed differences in the coordination of high field strength elements in dry vs. wet subaluminous granitic glasses, but not for peralkaline granitic glasses. Lastly, the fact that wolframite solubility increases with increasing water content in the subaluminous melt suggests that tungsten dissolved as a hexavalent species.  相似文献   

13.
Lithostratigraphy, physicochemical stratigraphy, biostratigraphy, and geochronology of the 77–70 Ma old series bracketing the Campanian–Maastrichtian boundary have been investigated by 70 experts. For the first time, direct relationships between macro- and microfossils have been established, as well as direct and indirect relationships between chemo-physical and biostratigraphical tools. A combination of criteria for selecting the boundary level, duration estimates, uncertainties on durations and on the location of biohorizons have been considered; new chronostratigraphic units are proposed. The geological site at Tercis is accepted by the Commission on Stratigraphy as the international reference for the stratigraphy of the studied interval. To cite this article: G.S. Odin, C. R. Geoscience 334 (2002) 409–414.  相似文献   

14.
正The Kuqa depression deposited thick rock salt,which has a lower density than surrounding rocks.When salt bodies form a certain scale,obvious negative gravity anomalies can be detected in the surface.Therefore,gravitational method can quickly obtain the shape,plane distribution of deep-seated salt bodies and overall tectonic morphology of the basin.  相似文献   

15.
正1 Introduction The Pingluoba brine,which characterized as high concentration with sodium,potassium,boron,lithium,and rubidium,possess great development value.The main composition of the brine can be summarized to the  相似文献   

16.
正1 Introduction In the present paper,MgCl2·6H2O,FeCl3·6H2O,and CeCl3·6H2O were used as raw materials in the precipitationhydrothermal method to synthesize MgF eC e hydrotalcite.The effects of the Fe:Ce molar ratio on the composition,crystal structure,and thermal stability of hydrotalcite are examined.Energy-dispersive X-ray spectroscopy(EDS),X-  相似文献   

17.
正1 Introduction Crystallization is one of important unit operations in the chemical production process,which requires not only the crystal product with high purity and yield,but also the available particle size of the crystal products to ensure product quality.Crystallization process is affected by  相似文献   

18.
正Dear Authors and Readers:First of all,on behalf of the new Editorial Board,I would like to express our sincere appreciation for your continuing support of our journal.This journal,founded in 1922,is the oldest geological journal in China.As the flagship journal of the Geological Society of China,it has become more and more influential in earth sciences in China and beyond.The journal is now indexed by SCI,CA and more than 20 other databases,with an impact  相似文献   

19.
正20141283 Bai Daoyuan(Hunan Institute of Geological Survey,Changsha 410016,China);Zhong Xiang Nature,Origin and Tectonic Setting of Jinzhou Basin in the South Segment of Xuefeng Orogen(Geology in China,ISSN1000-3657,CN11-1167/P,40(4),2013,p.1079-1091,10 illus.,47 refs.)Key words:foreland basins,strike-slip faults,Hunan Province  相似文献   

20.
正20142093Chen Daohua(Guangzhou Marine Geological Survey,Guangzhou 510075,China);Diao Shaobo The Latest Progress of Geological Marine Testing Technology in China(Rock and Mineral Analysis,ISSN0254-5357,CN11-2131/TD,32(6),2013,p.850-859,105refs.)Key words:chemical analysis,China  相似文献   

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