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71.
A new sample treatment was developed for the determination of dissolved cadmium in Tagus estuarine waters, based on focused ultrasound in conjunction with small volumes in the extraction steps for Cd pre-concentration. Cadmium was first pre-concentrated using a classical approach (APDC as the complexing agent and MIBK as the organic phase) and then back-extracted into HNO3 with the aid of focused ultrasound, which reduced the acid concentration by more than one order of magnitude (from 4 to 0.1 mol L− 3). This sample treatment was accomplished in less than 5 min, using low sample volume (20 mL), and low-volume, low-concentration reagents. The pre-concentration factor used in this work was 25, but different sample/organic volume ratios may be used in order to increase that value. The limit of detection and the limit of quantification in Tagus water samples were 0.03 nmol L− 1 and 0.1 nmol L− 3, respectively. Recoveries from spiked Tagus water were higher than 90%. The procedure was validated using the reference estuarine water NRC-SLEW-3. In the solubilization of Cd particulate, bath ultrasonication was used in conjunction with HNO3 + HCl, followed by H2O2, which took about 2 instead of the usual 12 h (cooling included) when high-pressure microwave digestion is used. 相似文献
72.
Melchor Gonzlez-Dvila J. Magdalena Santana-Casiano Demetrio de Armas Jos Escnez Miguel Suarez-Tangil 《Marine Chemistry》2006,99(1-4):177
Measurements of surface partial pressure of CO2 and water column alkalinity, pHT, nutrients, oxygen, fluorescence and hydrography were carried out, south of the Canary Islands during September 1998. Cyclonic and anticyclonic eddies were alternatively observed from the northwestern area to the central area of the Canary Islands. Nutrient pumping and vertical uplifting of the deep chlorophyll maximum by cyclonic eddies were also ascertained by upward displacement of dissolved inorganic carbon. A model was applied to determine the net inorganic carbon balance in the cyclonic eddy. The fluxes were determined considering both the diffusive and convective contributions from the upward pumping and the corresponding horizontal transport of water outside the area. An increase in the total inorganic carbon concentration in the upper layers inside the eddy field of 133 mmol C m− 2 d− 1 was determined. The upward flux of inorganic carbon decreased the effect of the increased primary production on the carbon dioxide chemistry. The reduced fCO2 inside the cyclonic eddy, 15 μatm lower than that observed in non-affected surface water, was explained by thermodynamic aspects, biological activity, eddy upward pumping and diffusion and air–sea water exchange effects. 相似文献
73.
74.
François M. Costard 《Earth, Moon, and Planets》1989,45(3):265-290
In order to quantify the spatial distribution of volatiles on Mars, 2600 fluidized ejecta craters have been systematically measured, classified and mapped over the planet Mars, using 1 : 2 M scale USGS photomosaics. The latitudinal distribution of ejecta craters reveals that flower ejecta deposits (Type 1), together with low mobility ejecta, are frequently observed in the equatorial region and on ridged plains. Rampart craters (Type 2), with high mobility ejecta, occur at mid latitudes and exhibit a spatial relationship with polygonal patterns and pseudocrater areas. The increase of ejecta mobility with latitude attests for a concentration of volatiles at high latitudes. Statistical analysis shows that cratered uplands and ridged plains contain less volatile material near the surface than the underlying materials. In Chryse Planitia and Utopia Planitia the statistical study and the spatial relationships between polygonally fractured patterns, pseudocraters and the great number of high mobility ejecta deposits suggest the presence of a water-rich alluvial deposit close to the surface near the mouth of Chryse and Elysium channels. This result explains, on a more quantitative basis, the idea that fractured patterns were preferentially developed in a volatile-rich sedimentary deposits. The behaviour of volatiles, at 41 S, 257 W near Reull Vallis, exhibits a strong anomaly, with the presence of an abnormally volatile rich layer close to the surface. 相似文献
75.
Atίla Özgüç 《Solar physics》1989,123(2):381-383
After re-examination of data presented by Verma (1984), some misuse of solar parameteres published in Solar Geophysical Data is presented. Consequently some conclusions made by Verma (1984, 1986) on about the longitudinal distribution of cool solar surges based on these misuses are discussed. 相似文献
76.
The Bayesian detection of discontinuities in a polynomial regression and its application to the cycle-slip problem 总被引:4,自引:1,他引:3
Maria Clara de Lacy Mirko Reguzzoni Fernando Sansò Giovanna Venuti 《Journal of Geodesy》2008,82(9):527-542
This paper deals with the problem of detecting and correcting cycle-slips in Global Navigation Satellite System (GNSS) phase
data by exploiting the Bayesian theory. The method is here applied to undifferenced observations, because repairing cycle-slips
already at this stage could be a useful pre-processing tool, especially for a network of permanent GNSS stations. If a dual
frequency receiver is available, the cycle-slips can be easily detected by combining two phase observations or phase and range
observations from a single satellite to a single receiver. These combinations, expressed in a distance unit form, are completely
free from the geometry and depend only on the ionospheric effect, on the electronic biases and on the initial integer ambiguities;
since these terms are expected to be smooth in time, at least in a short period, a cycle-slip in one or both the two carriers
can be modelled as a discontinuity in a polynomial regression. The proposed method consists in applying the Bayesian theory
to compute the marginal posterior distribution of the discontinuity epoch and to detect it as a maximum a posteriori (MAP)
in a very accurate way. Concerning the cycle-slip correction, a couple of simultaneous integer slips in the two carriers is
chosen by maximazing the conditional posterior distribution of the discontinuity amplitude given the detected epoch. Numerical
experiments on simulated and real data show that the discontinuities with an amplitude 2 or 3 times larger than the noise
standard deviation are successfully identified. This means that the Bayesian approach is able to detect and correct cycle-slips
using undifferenced GNSS observations even if the slip occurs by one cycle. A comparison with the scientific software BERNESE
5.0 confirms the good performance of the proposed method, especially when data sampled at high frequency (e.g. every 1 s or
every 5 s) are available. 相似文献
77.
Modelling Positional Uncertainty of Line Features by Accounting for Stochastic Deviations from Straight Line Segments 总被引:1,自引:0,他引:1
Sytze de Bruin 《Transactions in GIS》2008,12(2):165-177
The assessment of positional uncertainty in line and area features is often based on uncertainty in the coordinates of their elementary vertices which are assumed to be connected by straight lines. Such an approach disregards uncertainty caused by sampling and approximation of a curvilinear feature by a sequence of straight line segments. In this article, a method is proposed that also allows for the latter type of uncertainty by modelling random rectangular deviations from the conventional straight line segments. Using the model on a dense network of sub‐vertices, the contribution of uncertainty due to approximation is emphasised; the sampling effect can be assessed by applying it on a small set of randomly inserted sub‐vertices. A case study demonstrates a feasible way of parameterisation based on assumptions of joint normal distributions for positional errors of the vertices and the rectangular deviations and a uniform distribution of missed sub‐vertices along line segments. Depending on the magnitudes of the different sources of uncertainty, not accounting for potential deviations from straight line segments may drastically underestimate the positional uncertainty of line features. 相似文献
78.
Groundwater flow systems in turbidites of the Northern Apennines (Italy): natural discharge and high speed railway tunnel drainage 总被引:2,自引:0,他引:2
Alessandro Gargini Valentina Vincenzi Leonardo Piccinini Gian Maria Zuppi Paolo Canuti 《Hydrogeology Journal》2008,16(8):1577-1599
Turbidites crop out extensively in the Northern Apennine mountains (Italy). The huge amounts of groundwater drained by tunnels, built for the high speed railway connection between Bologna and Florence, demonstrate the aquifer-like behaviour of these units, up to now considered as aquitards. A conceptual model of groundwater flow systems (GFS) in fractured aquifers of turbidites is proposed, taking into account both system natural state and the perturbation induced by tunnel drainage. Analysis of hydrological data (springs, streams and tunnel discharge), collected over 10 years, was integrated with analysis of hydrochemical and isotopic data and a stream-tunnel tracer test. Hydrologic recession analysis of undisturbed conditions is a key tool in studying turbiditic aquifer hydrogeology, permitting the discrimination of GFS, the estimation of recharge relative to the upstream reach portion and the identification of springs most vulnerable to tunnel drainage impacts. The groundwater budgeting analysis provides evidence that the natural aquifer discharge was stream-focused through GFS, developed downslope or connected to main extensional tectonic lineaments intersecting stream beds; now tunnels drain mainly active recharge groundwater and so cause a relevant stream baseflow deplenishment (approximately two-thirds of the natural value), possibly resulting in adverse effects on local ecosystems. 相似文献
79.
80.
Stephen V. Smith Silvia E. Ibarra-Obando Victoria Díaz-Castañeda Francisco Javier Aranda-Manteca José D. Carriquiry Brian N. Popp Oscar Gonzalez-Yajimovich 《Estuaries and Coasts》2008,31(4):719-727
Sediment grain size and organic carbon (OC) data collected over the past 50 years, together with δ13C values of OC in recently collected samples, were analyzed to improve understanding of sediment OC distribution and abundance in Todos Santos Bay. Sediments in the submarine canyon at the mouth of the bay and in quiet-water locations along the shore are fine grained, high in OC, and have generally low δ13C values; sediments in high-energy environments are low in OC and have high δ13C values. A bivariate isotopic mixing model indicates that none of the sediments contain >50% terrigenous OC (average ~30%), and that the terrigenous OC content of the sediments is a small proportion of the OC content of local soils. Sediment OC composition is apparently controlled by energy-related sorting and deposition, oxidation of much of the original terrigenous OC, and replacement of some terrigenous OC by marine OC. 相似文献