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Off-line solid-phase extraction procedure for the determination of polycyclic aromatic hydrocarbons from aqueous matrices 总被引：1，自引：0，他引：1
I. Limam M. R. Driss 《International Journal of Environmental Science and Technology》2013,10(5):973-982
An off-line solid-phase extraction procedure followed by high-performance liquid chromatography with ultraviolet detection for the determination of 16 priority polycyclic aromatic hydrocarbon pollutants in aqueous matrices was described. Diverse aspects determining extraction efficiency such as packing type (disk or cartridge), elution solvents and addition of organic modifiers to the sample were evaluated. Elution with acetonitrile yields the highest recoveries. Rinsing the sample bottle with acetonitrile and combining the rinse with the sample extract avoids the adsorption of polycyclic aromatic hydrocarbons on the walls of the water containers. The use of isopropanol or methanol 10 % (V/V) was the most appropriate amount for the enrichment of 2- to 6-ring aromatic compounds only on C18 cartridge. The recoveries for all studied polycyclic aromatic hydrocarbons are ranged from 71.4 to 95.2 % for a treated water samples of 500 mL. The proposed method gives very low detection limits (subnanograms per liter) and it has been applied to drinking water, surface water and industrial effluent (oil refinery) samples with good results. 相似文献
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Three analyitcal solutions of saltwater intrusion under uncertain hydrologic, hydrogeologic, and pumping conditions are presented.
These solutions extends the existing deterministic, sharp interface solutions to stochastic ones. The randomness is represented
in terms of statistical measures of mean, standard deviation and covariance. The analysis is based on perturbation using Taylor
series expansion. Simulations based on probability distribution are conducted for verification. 相似文献
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Driss Takir Joshua P. Emery Harry Y. Mcsween Jr. Charles A. Hibbitts Roger N. Clark Neil Pearson Alian Wang 《Meteoritics & planetary science》2013,48(9):1618-1637
We investigated the petrologic, geochemical, and spectral parameters that relate to the type and degree of aqueous alteration in nine CM chondrites and one CI (Ivuna) carbonaceous chondrite. Our underlying hypothesis is that the position and shape of the 3 μm band is diagnostic of phyllosilicate mineralogy. We measured reflectance spectra of the chondrites under dry conditions (elevated temperatures) and vacuum (10?8 to 10?7 torr) to minimize adsorbed water and mimic the space environment, for subsequent comparison with reflectance spectra of asteroids. We have identified three spectral CM groups in addition to Ivuna. “Group 1,” the least altered group as determined from various alteration indices, is characterized by 3 μm band centers at longer wavelengths, and is consistent with cronstedtite (Fe‐serpentine). “Group 3,” the most altered group, is characterized by 3 μm band centers at shorter wavelengths and is consistent with antigorite (serpentine). “Group 2” is an intermediate group between group 1 and 3. Ivuna exhibits a unique spectrum that is distinct from the CM meteorites and is consistent with lizardite and chrysotile (serpentine). The petrologic and geochemical parameters, which were determined using electron microprobe analyses and microscopic observations, are found to be consistent with the three spectral groups. These results indicate that the distinct parent body aqueous alteration environments experienced by these carbonaceous chondrites can be distinguished using reflectance spectroscopy. High‐quality ground‐based telescopic observations of Main Belt asteroids can be expected to reveal not just whether an asteroid is hydrated, but also details of the alteration state. 相似文献
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This paper examines the distribution and the abundance of hydrated minerals (any mineral that contains H2O or OH) on outer Main Belt asteroids spanning the 2.5 < a < 4.0 AU region. The hypothesis we are testing is whether planetesimals that accreted closer to the Sun experienced a higher degree of aqueous alteration. We would expect then to see a gradual decline of the abundance of hydrated minerals among the outer Main Belt asteroids with increasing heliocentric distance (2.5 < a < 4.0 AU). We measured spectra (0.8–2.5 μm and 1.9–4.1 μm) of 28 outer Main Belt asteroids using the SpeX spectrograph/imager at the NASA Infrared Telescope Facility (IRTF). We identified four groups on the basis of the shape and the band center of the 3-μm feature. The first group, which we call “sharp”, exhibits a sharp 3-μm feature, attributed to hydrated minerals (phyllosilicates). Most asteroids in this group are located in the 2.5 < a < 3.3 AU region. The second group, which we call “Ceres-like”, consists of 10 Hygiea and 324 Bamberga. Like Asteroid Ceres, these asteroids exhibit a 3-μm feature with a band center of 3.05 ± 0.01 μm that is superimposed on a broader absorption feature from ～2.8 to 3.7 μm. The third group, which we call “Europa-like”, includes 52 Europa, 31 Euphrosyne, and 451 Patientia. Objects in this group exhibit a 3-μm feature with a band center of 3.15 ± 0.01 μm. Both the Ceres-like and Europa-like groups are concentrated in the 2.5 < a < 3.3 AU region. The fourth group, which we call “rounded”, is concentrated in the 3.4 < a < 4.0 AU region. Asteroids in this group are characterized by a rounded 3-μm feature, attributed to H2O ice. A similar rounded 3-μm feature was also identified in 24 Themis and 65 Cybele. Unlike the sharp group, the rounded group did not experience aqueous alteration. Of the asteroids observed in this study, 140 Siwa, a P-type, is the only one that does not exhibit a 3-μm feature. These results are important to constrain the nature and the degree of aqueous alteration in outer Main Belt asteroids. 相似文献
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The observed aeromagnetic anomaly map of Southern High Plateaus provides general information about the magnetization variations that are associated with subsurface magnetic sources, but it does not bring clear information about all geological elements of the study area. In this work, we attempt, by analyzing these aeromagnetic data, to determine structures of Paleozoic basement that may indicate the presence of major deep-seated structures in this area. To better understand and outline the basement geological structures, two approaches have been performed. Such analysis includes application of a low-pass filtering and spectral analysis, which permits an enhanced visual interpretation of the magnetization sources and leads to a better knowledge of the geological structures especially basins or intrusive bodies. The results obtained show magnetic anomalies indicating geological features trending NE–SW. They also reveal two depths of magnetic sources in the area. The deeper sources range from 1074 to 4057 m and reflect the Paleozoic basement. However, the shallower sources range from 153 and 596 m reflecting magnetic sources shallower than the basement. The outcomes of this study suggest a new structure and will contribute to better understand the characteristics and organization of the basin as well as the improvement of the geological map of the area for hydrocarbon exploration. 相似文献
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Driss Khattach Pierre Keating El Mostafa Mili Touria Chennouf Pierre Andrieux Abdellah Milhi 《Comptes Rendus Geoscience》2004,336(16):1427-1432
Various techniques (horizontal and vertical derivatives, upward continuation, Euler deconvolution) have been applied to the gravity data from the Triffa's plain and the north flank of the Beni-Snassen massif to delineate various major geological structures such as faults and basins. These results allow the production of a structural map showing the fault systems for the survey area. This map forms the basis for planning future hydrogeological research in this region. To cite this article: D. Khattach et al., C. R. Geoscience 336 (2004). 相似文献
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Hannah H. Kaplan Victoria E. Hamilton Ellen S. Howell F. Scott Anderson M. Antonella Barrucci John Brucato Thomas H. Burbine Beth E. Clark Ed A. Cloutis Harold C. Connolly Elisabetta Dotto Joshua P. Emery Sonia Fornasier Cateline Lantz Lucy F. Lim Frederic Merlin Alice Praet Dennis C. Reuter Scott A. Sandford Amy A. Simon Driss Takir Dante S. Lauretta 《Meteoritics & planetary science》2020,55(4):744-765
The primary objective of the Origins, Spectral Interpretation, Resource Identification, and Security–Regolith Explorer (OSIRIS‐REx) mission is to return to Earth a pristine sample of carbonaceous material from the primitive asteroid (101955) Bennu. To support compositional mapping of Bennu as part of sample site selection and characterization, we tested 95 spectral indices on visible to near infrared laboratory reflectance data from minerals and carbonaceous meteorites. Our aim was to determine which indices reliably identify spectral features of interest. Most spectral indices had high positive detection rates when applied to spectra of pure, single‐component materials. The meteorite spectra have fewer and weaker absorption features and, as a result, fewer detections with the spectral indices. Indices targeting absorptions at 0.7 and 2.7–3 μm, which are attributable to hydrated minerals, were most successful for the meteorites. Based on these results, we identified a set of 17 indices that are most likely to be useful at Bennu. These indices detect olivines, pyroxenes, carbonates, water/OH‐bearing minerals, serpentines, ferric minerals, and organics. Particle size and albedo are known to affect band depth but had a negligible impact on interpretive success with spectral indices. Preliminary analysis of the disk‐integrated Bennu spectrum with these indices is consistent with expectations given the observed absorption near 3 μm. Our study prioritizes spectral indices to be used for OSIRIS‐REx spectral analysis and mapping and informs the reliability of all index‐derived data products, including a science value map for sample site selection. 相似文献