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81.
The study of trace metal speciation has benefited from a great deal of interest leading to the development and the diversification of sequential extraction schemes (SES), which triggered the need for harmonization by the standard, measurements and testing programme (SM & T). However, some uncertainties still persist in the application of the harmonized 3-step protocol, because of the difficulty in conceptualizing a technique that can be applied to environmental samples irrespective of their nature. The alternative method proposed in this study is based on the solubility of the sample components progressively dissolved during the course of an acidimetric titration by 1 mol L−1 HCl. The major HCl-reactive mineralogical components are identified using mass balance calculation of H+ consumed by their dissolution together with the amount of major elements released into solution. The speciation of minor and trace elements is investigated by comparing their titrations to those of the major elements. This approach is much simpler than SES because it uses simple non-selective H+ at room temperature instead of a complex experimental design of so-called specific reagents. The different mineral components of the solid are no longer operationally defined and the problem of selectivity is irrelevant to the titration approach. The method was applied to several sediment samples from the Scheldt estuary and the particulate phase was further examined by Scanning Electron Microprobe and X-ray Diffraction techniques. The nearly complete consumption of H+ in the suspension is balanced by the total dissolution of carbonates and Fe-oxyhydroxides. In contrast to the speciation inferred from the Tessier SES, the acidimetric titration has demonstrated that the carbonate phase does not significantly contain trace metals with the exceptions of 40% of the Mn and 30% of the Co. In contrast, the Fe-oxyhydroxides seem to play a major role and account for 70% of Pb and 20% of Cr, in addition to 60% of P and additional amounts of 20% Co and 40% Mn. 70% of the Cu also occur in the oxyhydroxide phase, more likely coprecipitated with gibbsite. 90% of the Cd and 85% of Zn can be attributed to the Acid Volatile Sulfide (AVS) phase as evidenced from S titration. The acidimetric titration method not only provides information on the speciation of trace metals but also allows the quantification of their reactivity and mobility, if one considers that the titration roughly mimics pH changes that may occur as a result of chemical disequilibrium in the environment. The results demonstrate the potential of the acidimetric titration as an alternative to SES protocols in geochemical and environmental regulation studies. This method is applicable to a wide variety of environmental materials with little or minor adjustments. 相似文献
82.
Erosion rates and sediment budgets in vineyards at 1-m resolution based on stock unearthing (Burgundy, France) 总被引:1,自引:0,他引:1
Jrme Brenot Amlie Quiquerez Christophe Petit Jean-Pierre Garcia 《Geomorphology》2008,100(3-4):345-355
A new and simple method is developed to efficiently quantify erosion and deposition rates based on stock unearthing measurements. This is applicable to spatial scales ranging from plot to hillslopes, and to time scales ranging from single hydrologic events to centennial scales. The method is applied to a plot area on vineyard hillslopes in Burgundy (Monthélie, France), with measurement of 4328 vine plants. A sediment budget established at the plot scale shows a mean soil lowering of 3.44 ± 1 cm over 20 years, involving a minimal erosion rate of 1.7 ± 0.5 mm yr− 1. Locally, erosion rates can reach up to 8.2 ± 0.5 mm yr− 1.This approach allows the sediment redistribution to be mapped and analyzed at 1-m resolution. It provides novel insights into the characterization of erosion patterns on pluri-decennial scales and into the analysis of spatial distribution of erosion processes on cultivated hillslopes. 相似文献
83.
84.
Paul R. J. Saey Clemens Schlosser Pascal Achim Matthias Auer Anders Axelsson Andreas Becker Xavier Blanchard Guy Brachet Luis Cella Lars-Erik De Geer Martin B. Kalinowski Gilbert Le Petit Jenny Peterson Vladimir Popov Yury Popov Anders Ringbom Hartmut Sartorius Thomas Taffary Matthias Zähringer 《Pure and Applied Geophysics》2010,167(4-5):499-515
Activity concentration data from ambient radioxenon measurements in ground level air, which were carried out in Europe in the framework of the International Noble Gas Experiment (INGE) in support of the development and build-up of a radioxenon monitoring network for the Comprehensive Nuclear-Test-Ban Treaty verification regime are presented and discussed. Six measurement stations provided data from 5 years of measurements performed between 2003 and 2008: Longyearbyen (Spitsbergen, Norway), Stockholm (Sweden), Dubna (Russian Federation), Schauinsland Mountain (Germany), Bruyères-le-Châtel and Marseille (both France). The noble gas systems used within the INGE are designed to continuously measure low concentrations of the four radioxenon isotopes which are most relevant for detection of nuclear explosions: 131mXe, 133mXe, 133Xe and 135Xe with a time resolution less than or equal to 24 h and a minimum detectable concentration of 133Xe less than 1 mBq/m3. This European cluster of six stations is particularly interesting because it is highly influenced by a high density of nuclear power reactors and some radiopharmaceutical production facilities. The activity concentrations at the European INGE stations are studied to characterise the influence of civilian releases, to be able to distinguish them from possible nuclear explosions. It was found that the mean activity concentration of the most frequently detected isotope, 133Xe, was 5–20 mBq/m3 within Central Europe where most nuclear installations are situated (Bruyères-le-Châtel and Schauinsland), 1.4–2.4 mBq/m3 just outside that region (Stockholm, Dubna and Marseille) and 0.2 mBq/m3 in the remote polar station of Spitsbergen. No seasonal trends could be observed from the data. Two interesting events have been examined and their source regions have been identified using atmospheric backtracking methods that deploy Lagrangian particle dispersion modelling and inversion techniques. The results are consistent with known releases of a radiopharmaceutical facility. 相似文献
85.
Bertrand?GuillierEmail author Jean-Luc?Chatelain Hugo?Perfettini El?Hadi?Oubaiche Christophe?Voisin Rabah?Bensalem Djamel?Machane Mustapha?Hellel 《Bulletin of Earthquake Engineering》2016,14(8):2213-2227
Building frequencies (fundamental and higher modes) are a critical parameter especially in the field of structural health monitoring mainly based on the stability of the structural dynamic parameters of individual building (frequencies, damping and modes shape). One of the most used methods to find out these parameters is based on the use on ambient vibration analysis. In this work, we study the fluctuations over a month period of the fundamental frequencies (transverse and longitudinal) of a 3.5-story RC-building made of 2 identical units connected by a structural joint. Time independent building frequencies is a strong assumption; as illustrated by our experiment showing that over an observation period of a month, building frequencies fluctuate of about 3.5 %. A clear correlation is found between the building frequency fluctuations and temperature variations, with a phase-shift interpreted as the characteristic time of heat diffusion within the walls. This allows: (1) determining the thermal diffusivity of the structure, (2) inferring its relative stiffness variations, and (3) showing that its Young modulus varies linearly with temperature. 相似文献
86.
C. C. Petit E. F. Lambin 《International journal of geographical information science》2013,27(8):785-803
The objective of this study is to develop a methodology to integrate multi-source remote sensing data into a homogeneous time series of land cover maps in order to carry out change detection. We developed a method to increase the comparability between land cover maps coming from panchromatic aerial photographs and SPOT XS (multi-spectral) data by equalizing their levels of thematic content and spatial details. The methodology was based on the hypotheses that: (1) map generalization can improve the integration of data for change detection purpose, and (2) the spatial structure of a land cover map, as measured by a set of landscape metrics, is an indicator of the level of generalization of that map. Firstly, the methodology for data integration was developed by using land cover maps generated from near-synchronous data. Results revealed that, by controlling successively the parameters that influence the level of map generalization, the percentage of agreement between the near-synchronous land cover maps can be increased from 42% to 93%. The computation of five landscape metrics for a set of generalized land cover maps and for the target map allowed us to optimize the level of generalization by measuring the similarity in landscape pattern of the maps. The optimum level of generalization of the land cover map obtained from the aerial photographs for comparison with a land cover map derived from SPOT XS data was found at a resolution of 41m for two generalization levels of the thematic content. The spatial structure of a land cover map, as measured by a set of landscape metrics, is thus a good indicator of the level of generalization of this map. Secondly, the method was applied by integrating a land cover map obtained from aerial photographs of 1954 with a land cover map obtained from a SPOT XS image of 1992. 相似文献
87.
Many seismic loss problems (such as disruption of distributed infrastructure and losses to portfolios of structures) are dependent upon the regional distribution of ground‐motion intensity, rather than intensity at only a single site. Quantifying ground‐motion over a spatially‐distributed region therefore requires information on the correlation between the ground‐motion intensities at different sites during a single event. The focus of the present study is to assess the spatial correlation between ground‐motion spectral accelerations at different periods. Ground motions from eight well‐recorded earthquakes were used to study the spatial correlations. On the basis of obtained empirical correlation estimates, we propose a geostatistics‐based method to formulate a predictive model that is suitable for simulation of spectral accelerations at multiple sites and multiple periods, in the case of crustal earthquakes in active seismic regions. While the calibration of this model and investigation of its implications were somewhat complex, the model itself is very simple to use for making correlation predictions. A user only needs to evaluate a simple equation relying on three sets of coefficients provided here to compute a correlation coefficient for spectral values at two periods and at a specified separation distance. These results may then be used in evaluating the seismic risk of portfolios of structures with differing fundamental periods. Copyright © 2012 John Wiley & Sons, Ltd. 相似文献
88.
Hilary McMillan Alberto Montanari Christophe Cudennec Hubert Savenije Heidi Kreibich Tobias Krueger 《水文科学杂志》2013,58(7):1174-1191
ABSTRACTIn 2013, the International Association of Hydrological Sciences (IAHS) launched the hydrological decade 2013–2022 with the theme “Panta Rhei: Change in Hydrology and Society”. The decade recognizes the urgency of hydrological research to understand and predict the interactions of society and water, to support sustainable water resource use under changing climatic and environmental conditions. This paper reports on the first Panta Rhei biennium 2013–2015, providing a comprehensive resource that describes the scope and direction of Panta Rhei. We bring together the knowledge of all the Panta Rhei working groups, to summarize the most pressing research questions and how the hydrological community is progressing towards those goals. We draw out interconnections between different strands of research, and reflect on the need to take a global view on hydrology in the current era of human impacts and environmental change. Finally, we look back to the six driving science questions identified at the outset of Panta Rhei, to quantify progress towards those aims.
Editor D. Koutsoyiannis; Associate editor not assigned 相似文献
89.
Eduard Saura Jean‐Christophe Embry Jaume Vergés David W. Hunt Emilio Casciello Stéphane Homke 《Basin Research》2013,25(2):149-171
The evolution from Late Cretaceous to early Eocene of the well dated Amiran foreland basin in the NW Iranian Zagros Mountains is studied based on the reconstruction of successive thickness, palaeobathymetry and subsidence maps. These maps show the progressive forelandwards migration of the mixed carbonate‐siliciclastic system associated with a decrease in creation of accommodation. Carbonate facies variations across the basin suggest a structural control on the carbonate distribution in the Amiran foreland basin, which has been used as initial constraint to study the control exerted by syndepositional folding in basin architecture and evolution by means of stratigraphic numerical modelling. Modelled results show that shallow bathymetries on top of growing folds enhance carbonate production and basin compartmentalization. As a consequence, coarse clastics become restricted to the internal parts of the basin and only the fine sediments can by‐pass the bathymetric highs generated by folding. Additionally, the development of extensive carbonate platforms on top of the anticlines favours the basinwards migration of the depositional system, which progrades farther with higher fold uplift rates. In this scenario, build‐ups on top of anticlines record its growth and can be used as a dating method. Extrapolation of presented modelling results into the Amiran foreland basin is in agreement with an early folding stage in the SE Lurestan area, between the Khorramabad and Kabir Kuh anticlines. This folding stage would enhance the development of carbonate platforms on top of the anticlines, the south‐westward migration of the system and eventually, the complete filling of the basin north of the Chenareh anticline at the end of the Cuisian. Incremental thickness maps are consistent with a thin (0.4–2 km) ophiolite complex in the source area of the Amiran basin. 相似文献
90.
Rémy Thibaud Géraldine Del Mondo Thierry Garlan Ariane Mascret Christophe Carpentier 《Transactions in GIS》2013,17(5):742-762
Defining a model for the representation and the analysis of spatio‐temporal dynamics remains an open domain in geographical information sciences. In this article we investigate a spatio‐temporal graph‐based model dedicated to managing and extracting sets of geographical entities related in space and time. The approach is based on spatial and temporal local relations between neighboring entities during consecutive times. The model allows us to extract sets of connected entities distant in time and space over long periods and large spaces. From GIS concepts and qualitative reasoning on space and time, we combine the graph model with a dedicated spatial database. It includes information on geometry and geomorphometric parameters, and on spatial and temporal relations. This allows us to extend classical measurements of spatial parameters, with comparisons of entities linked by complex relations in space and time. As a case study, we show how the model suggests an efficient representation of dunes dynamics on a nautical chart for safe navigation. 相似文献