How Real(ist) Can You Get?*     

Judy R. Walton 《The Professional geographer》1995,47(1):61-65

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A water-leach procedure for estimating bioaccessibility of elements in soils from transects across the United States and Canada   总被引：1，自引：1，他引：0  

Robert G. Garrett  G.E.M. Hall  J.E. Vaive  P. Pelchat 《Applied Geochemistry》2009,24(8):1438

An objective of the North American Soil Geochemical Landscapes Project is to provide relevant data concerning bioaccessible concentrations of elements in soil to government and other institutions undertaking environmental studies. A protocol was developed that employs a 1-g soil sample agitated overnight with 40 mL of reverse-osmosis de-ionized water for 20 h, and determination of 63 elements following three steps of centrifugation by inductively coupled plasma–atomic emission spectrometry and inductively coupled plasma–mass spectrometry the following day. Statistical summaries are presented for those 48 elements (Ag, Al, As, B, Ba, Be, Br, Ca, Cd, Ce, Co, Cr, Cs, Cu, Dy, Er, Eu, Fe, Ga, Gd, Ge, Hf, Ho, I, K, La, Li, Lu, Mg, Mn, Mo, Na, Nb, Nd, Ni, P, Pb, Pr, Rb, Re, S, Sb, Si, Sm, Sn, Sr, Tb, Ti, Tl, Tm, U, V, W, Y, Yb, Zn, Zr, and pH) for which <20% of their data were reported as below the detection limit. The resulting data set contains analyses for 161 A-horizon soils collected along two transects, one along the 38th parallel across the USA and the other from northern Manitoba to the USA–Mexico border. The spatial distribution of three selected elements (Ca, Cu, and Pb) along the two transects is discussed in this paper both as absolute amounts liberated by the leach and expressed as a percentage of the total, or near-total, amounts determined for the elements. The Ca data reflect broad trends in soil parent materials, their weathering, and subsequent soil development. Calcium concentrations are generally found to be lower in the older soils of the eastern USA. The Cu data are higher in the eastern half of the USA, correlating with soil organic C, with which it is sequestered. The Pb data exhibit little regional variability due to natural sources, but are influenced by anthropogenic sources. Based on the Pb results, the percentage water-extractable data demonstrate promise as a tool for identifying anthropogenic components. The soil–water partition (distribution) coefficients, K_ds (L/kg), were determined and their relevance to estimating bioaccessible amounts of elements to soil fauna and flora is discussed. Finally, a possible link between W concentrations in human urine and water-extractable W levels in Nevada soils is discussed.  相似文献   

Neither friends nor foes: Thoughts on ethnographic distance     

Ju Hui Judy Han 《Geoforum》2010,41(1):11-14

As a critical ethnographer of proselytizing missions led by conservative Korean/American evangelicals, I discuss the difficulties arising from conducting research in a hostile group setting, negotiating the dynamics of empathetic proximity and critical distance.  相似文献   

Distributed snow process modelling: An image processing approach     

Robert E. Davis  Judy Ceretha McKenzie  Rachel Jordan 《水文研究》1995,9(8):865-875

An approach to spatially distribute a snow process model by segmenting images of land cover, terrain and snow properties is reported. A small 1.7 ha study area with an existing database was selected for this preliminary evaluation. The methodology was carried out over a relatively flat valley bottom at Camp Grayling, Michigan. Meteorological measurements on two sides of the area showed only small differences, so uniform meteorological variables were assumed over the site. Initial snow cover conditions were reconstructed and were distributed over the area using snow maps and sparse snow pit measurements. One metre resolution terrain, soil, vegetation and snow type maps were individually processed into class maps. These layers were then combined to produce a segmented class map, where the attributes from the data layers were known for each class. A one-dimensional model of snow processes was run for each class, then the results were mapped back into images. Shallow snow conditions provided high sensitivity of ablation patterns to meteorological conditions over a 72 h period. The model performance was assessed by comparing predicted and observed ablation patterns. The error in total snow-covered area was less than 9%. However, the location errors were greater (predicted snow where no snow was observed and observed snow where no snow was predicted). Extensive error analysis was not justified because of the lack of multiple point measurements of snow properties.  相似文献   

DETERMINATION OF SULPHUR AT LOW LEVELS IN STANDARD REFERENCE MATERIALS BY PYROHYDROL YSIS/LON CHROMATOGRAPHY     

Gwendy E.M. HALL  Judy A. VAIVE 《Geostandards and Geoanalytical Research》1989,13(1):1-4

The determination of sulphur in rocks, soils and sediments by pyrohydrolysis/ion chromatography has been modified to reach lower detection limits of the order of 2 μg g⁻¹. Thirty-one standard reference materials containing sulphur at levels ranging from 3 to about 900 μg g⁻¹ have been analysed in triplicate. In general, the comparison of the results with those published is favorable. The method is also applicable to organic-rich samples as demonstrated by the analysis of NBS samples (citrus leaves, tomato leaves, bovine liver).  相似文献   

Bias in the analysis of geological materials for gold using current methods     

G. E. M. Hall  J. E. Vaive  J. A. Coope  E. F. Weiland   《Journal of Geochemical Exploration》1989,34(2)

A consistent pattern has been observed in the results obtained for Au in three soil and two porphyry copper ore samples serving as control reference standards in geochemical analyses. The mean reported by wet chemical methods (regardless of the measurement technique) was less than the mean by fire assay-based methods which, in turn, was less than the mean reported by laboratories using direct instrumental neutron activation analysis (INAA). These data have been obtained from 16 laboratories, some employing more than one method. Compared to INAA, values obtained for Au (at the 30–300 ppb level) using aqua regia (AR) dissolution were low by 24–42%, while those reported by fire assay-based methods were low by 14–26%.Studies of these samples and 32 rocks of widely varying composition revealed that the amount of Au remaining in the residue after AR attack ranged from 4% to 59% of the total. Gold dissolved by AR was determined by graphite furnace atomic absorption spectrometry (GFAAS) after extraction into MIBK (methyl isobutyl ketone), whereas Au remaining in the residue was determined by INAA. The slope of the line obtained by plotting Au by INAA vs. the sum of Au by AR/GFAAS and Au in the residue was not significantly different from 1.0.Modifications to the AR procedure such as prior attack by HCl or HF did not improve the recovery of Au in the three reference soils. However, reduction of sample size from 10 g to 1 g while maintaining the volume of AR at about 30 ml did increase results for Au. Furthermore, addition of HF in the attack on 1-g samples yielded results virtually identical to those obtained by INAA. It is thought that the poor extraction efficiency by AR is due to non-wetting of the larger sized sample, a lack of intimate, prolonged contact between the grains of the sample and the acid mixture and the presence of insoluble gangue surrounding Au particles. Constant agitation of the sample during evaporation with AR is desirable.The mean values obtained for Au in the soils by fire assay methods were not significantly different from the results by INAA (low by 14–19%); this was not the case for the two copper ore samples (low by 26%). This probably reflects the difficulties encountered in fire assay by high concentrations of Cu which hinder effective collection and separation of Au into the Pb button. However, the accuracy of the INAA method has not been established and is dependent upon measurement procedures and the degree of certainty associated with the Au values assumed for the reference materials employed for calibration. While estimation of precision does not present a problem, accuracy is difficult to assess in the absence of certified reference materials for Au at concentrations in the 10–300 ppb range. However, it is concluded that methods based upon AR dissolution can lead to low results, the magnitude being dependent upon the sample matrix and the mineralogical association of the Au present.  相似文献   

A unified approach to a fragmental problem: Petrological and geochemical studies of lithic fragments from Apollo 15 soils     

Michael J. Drake  Judy W. Stoeser  Gordon G. Goles 《Earth and Planetary Science Letters》1973,20(3):425-439

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Marine research in Israel     

Judy Carr 《Marine Policy》1977,1(4):343-344

A note on the main projects and concerns of the Israel Oceanographic and Limnological Research Institute at Haifa.  相似文献   

Textural and isotopic development of marble assemblages during the Barrovian-style M2 metamorphic event,Naxos, Greece     

Judy Baker  Alan Matthews 《Contributions to Mineralogy and Petrology》1994,116(1-2):130-144

A detailed petrological analysis of the marble assemblages observed within the M2 metamorphic complex on Naxos is presented. Two distinct periods of mineral growth are documented; the first is associated with prograde M2 metamorphism and the second with retrograde M2 metamorphism occurring during ductile extensional thinning of the complex. The textural and miner-alogical characteristics and the carbon and oxygen isotope compositions of each generation are described, and the P-T-X _{CO 2} conditions at which these two mineral generations were stable, and the compositions of the fluids present during metamorphism are characterised. Whereas the low variance and stable isotope compositions of prograde siliceous dolomite assemblages are consistent with internally buffered fluid evolution, the retrograde mineral generation is shown to have grown as a result of the infiltration of a water-rich fluid phase that transported silica, Al₂O₃, Na₂O and FeO into the host rocks. This observation, together with the stable isotope compositions of the retrograde calcite, and the fact that occurrences of veins of this type are limited to marbles in the highest grade areas (T>600° C) of the metamorphic complex, suggests that the fluids responsible for vein formation were generated during the crystallisation of melts as the metamorphic complex cooled from peak temperatures. The existence of this second generation of minerals has significant implications for previous studies of heat transport by fluid flow on Naxos, because many of the unusually low ¹⁸O compositions of pelites at high grades may be ascribable to the effects of interaction with retrograde M2 fluids, rather than with prograde fluids.  相似文献   

A forefin of Leptonectes solei from the Lower Jurassic (Pliensbachian) of Dorset,UK     

Dean R. Lomax  Judy A. Massare 《Proceedings of the Geologists' Association. Geologists' Association》2018,129(6):770-773

An incomplete forefin in the collections of the National Museum of Wales, Cardiff, is herein assigned to the rare leptonectid species, Leptonectes solei, known only from the west Dorset coast. It is only the third specimen of the species and is smaller than both the holotype and referred specimen. The new specimen is from the Lower Jurassic (lower Pliensbachian, Charmouth Mudstone Formation, Tragophylloceras ibex Ammonite Zone, Acanthopleuroceras valdani Ammonite Subzone) of Seatown, Dorset, UK. It confirms that all three species of Leptonectes were present in the Pliensbachian and expands the known diversity of ichthyosaurs for that time period. We show that isolated forefins of Leptonectes can be assigned to a species with a high degree of confidence.  相似文献