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191.
Shuhei Sakata Kentaro Hattori Hideki Iwano Takaomi D. Yokoyama Tohru Danhara Takafumi Hirata 《Geostandards and Geoanalytical Research》2014,38(4):409-420
We have developed new analytical procedures to measure precise and accurate 238U–206Pb and 235U–207Pb ages for young (~ 1 Ma) zircons using laser ablation‐ICP‐mass spectrometry. For young zircons, both careful correction for the background counts and analysis of very small Pb/U ratios (i.e., 206Pb/238U < 0.00016 and 207Pb/235U < 0.0001 for 1 Ma zircons) are highly desired. For the correction of the background, the contribution of the background signal intensities for the analytes, especially for the residual signal intensities for 206Pb and 207Pb, was defined through laser ablation of synthesised zircons (ablation blank) containing negligible Pb. The measured signal intensities for 202Hg, 206Pb and 207Pb signals obtained by the ablation blank were slightly higher than those obtained by data acquisition without laser ablation (gas blank). For the wider dynamic range measurements on Pb/U ratios, an attenuator device for the ion detection system was employed to extend the capability to monitor high‐intensity signals (i.e., > 3 Mcps). Through the attenuator device, the ion currents were reduced to 1/450 of the signal intensity without the attenuator. Because the switching time for the attenuator was shorter than 1 ms, signal intensities for only specific isotopes could be reduced. With attenuation of the 238U signal, counting statistics on 206Pb and 207Pb isotopes could be improved and counting loss on the 238U signal could be minimised. To demonstrate the reliability of this new analytical technique, 238U–206Pb and 235U–207Pb ages for three young zircon samples (collected from Osaka Group Pink Volcanic Ash, Kirigamine and Bishop Tuff) were measured. The data presented here demonstrate clearly that the present technique could become a major analytical tool for in situ U–Pb age determination of young zircons (~ 1 Ma). 相似文献
192.
Yasuto Itoh Keiji Takemura Toshio Nakamura Shin Hasegawa Hideki Takada 《Geoarchaeology》2011,26(4):461-478
In order to elucidate the paleoenvironment associated with the early Holocene Mawaki archaeological site on the Noto Peninsula of central Japan, a high‐resolution stratigraphic study was conducted of 17 boreholes drilled at the archaeological site. We selected three boreholes for which lithological and/or chronological data are reported. Initial magnetic susceptibility was utilized for correlation of clastic core samples with the assistance of 26 radiocarbon dates. Four lithological units (A, B, C, and D in ascending order) were identified and interpreted as a sequence in a cycle of marine transgression and regression. Dated coastal horizons were chosen to indicate former sea levels. A Holocene relative sea level curve was generated on the basis of the geological data, and a rapid rise from 8000cal. yr B.P. to 7000cal. yr B.P. and a succeeding minor sea level fall represent the basic eustatic trend around the Sea of Japan because hydroisostatic and tectonic effects are moderate in the study area. Abundant dolphin bones lay just above the top of the marine sequence (boundary between Units C and D), located in the seashore environment. Cultural artifacts are found in a subaerial deposit (Unit D) near the dolphin bone level that is assigned to a period of high, stable sea level after the post‐glacial eustatic highstand. Dolphin bones are associated with stone artifacts (arrowheads, knives, and scrapers) and ritual wood columns, indicating the presence of a longstanding fishery during the early Holocene on the Sea of Japan coast. © 2011 Wiley Periodicals, Inc. 相似文献
193.
Hayao Morinaga Hiroo Inokuchi Hideki Yamashita Akira Ono Takashi Inada 《Geoarchaeology》1999,14(5):377-399
We present a methodological approach to detect heated soil on ancient sites, using magnetic measurements. The method is based on changes in magnetic signals of soil by heating. The following three types of soil were used for testing the method: silty soil (SS), weathered volcanic ash (WVA, = loam) and fairly fresh volcanic ash (VA) called Odori tephra. On heating above 250–600°C, the magnetic susceptibility and remanent magnetization intensity increased for the SS and WVA samples, reflecting chemical alteration of magnetic minerals (from goethites to magnetites through hematites). The VA sample showed no susceptibility change suggesting the absence of goethites within it. On heating below 250°C, only the intensities of all the samples increased. This is possibly due to acquisition of thermal remanent magnetization. The largest change of the magnetic signals was identified for the SS sample and the smallest one was seen for the VA sample. Therefore, the in situ susceptibility measurement, which is the nondestructive and indirect method, seems to be effective to detect heated soil for sites of aqueous deposits as the SS. On the other hand, for sites of aeolian deposits as the WVA (loam) and VA, the intensity measurement of collected soils seems to be the most reliable method to detect evidence of heating. The degree of the magnetic stability (coercivity) against progressive alternating-field demagnetization was also an important parameter, indicating whether the investigated soils were heated or unheated. © 1999 John Wiley & Sons, Inc. 相似文献