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141.
The two Bragg crystal spectrometers on board Hinotori provide a new technique for measuring linear polarization of the soft X-ray line emission from solar flares. The results of the measurements of large (X class) flares are given in this paper, and the polarization degree averaged over the soft X-ray maximum phases is estimated to be less than 4%. 相似文献
142.
143.
Accurate Isotopic and Concentration Analyses of Small Amounts of Pb Using Isotope Dilution Coupled with the Double Spike Technique 总被引:1,自引:0,他引:1
Takeshi Kuritani Tomohiro Usui Tetsuya Yokoyama Eizo Nakamura 《Geostandards and Geoanalytical Research》2006,30(3):209-220
A new method has been developed for the simultaneous determination of Pb abundance and Pb isotopic composition with high precision and accuracy for small test portion masses by thermal ionisation mass spectrometry. In this method, a 205 pb-204 pb double spike is added to samples prior to the chemical separation of Pb, and the isotopic composition of the spike-sample mixture is determined rigorously by the double spike technique using a 207 Pb-204 Pb spike. The isotopic composition and concentration of Pb in the sample are then obtained by utilising the principle of isotope dilution. Using this technique, replicate determinations of Pb from NIST SRM 981 and GSJ JP-1 (peridotite; 0.07 μg g−1 Pb) were performed. The measured concentration and isotopic data were identical, within uncertainty, to published data or to data that were determined independently in this study. The application of this method to U-Pb dating and the determination of the "initial" Pb isotopic composition was also tested. Lead isotopic compositions and the concentrations of Pb, Th and U were determined for a single batch of samples, through the addition of 205 pb-204 pb, 230 Th and 235 U spikes to samples prior to chemical separation. Also in these experiments, we confirmed that this routine gives accurate data for Pb, Th and U concentrations and Pb isotopic compositions. 相似文献
144.
Effect of the development of notches and tension cracks on instability of limestone coastal cliffs in the Ryukyus, Japan 总被引:1,自引:0,他引:1
Tetsuya Kogure Hisashi Aoki Akira Maekado Takashi Hirose Yukinori Matsukura 《Geomorphology》2006,80(3-4):236-244
Notches cut by waves are currently developing at the base of vertical coastal limestone cliffs in Okinawa, Japan. The cliff height varies from 3.0–22.1 m, and the maximum notch depth is 8.8 m. Many rectangular or cubic blocks, which appear to have originated from cliff failures, are found on platforms in front of the cliffs. On the flat top surface of the cliff, tension cracks often run parallel to the cliff face. The vertical face of the cliffs displays small undulations but no sliding striation, suggesting that cliff failures have been caused by toppling rather than by shearing or sliding. We use slope stability analysis to determine the critical condition for toppling failure. Physical and mechanical properties of the cliff material were first obtained from laboratory tests. The results indicate that the strength of limestone shows a scale effect, such that the strength decreases with increasing size of the test specimens. Based on this result, we estimated the strength of a rock mass corresponding to the size of the coastal cliff. Cliff stability was then analyzed using a cantilever beam model. Comparison of the stability analysis and the dimension of fallen blocks indicates that toppling failure is strongly associated with the development of notches and tension cracks. 相似文献
145.
Investigating the Influence of Non‐Spectral Matrix Effects in the Determination of Twenty‐Two Trace Elements in Rock Samples by ICP‐QMS 下载免费PDF全文
Tetsuya Yokoyama Yuichiro Nagai Yu Hinohara Tomohiko Mori 《Geostandards and Geoanalytical Research》2017,41(2):221-242
The influence of non‐spectral matrix effects on the determination of twenty‐two trace elements (Rb, Sr, Y, Cs, Ba, lanthanides, Pb, Th and U) in rock samples using ICP‐MS was investigated. Three types of multi‐element solutions were synthesised containing the twenty‐two trace elements, In, Tl and ten major rock‐forming elements with varying mass fractions mimicking the compositions of basalt, peridotite and dolomite. The synthetic solutions were conditioned to have dilution factors (DF) of 1000–10000. The extent of sensitivity suppression relative to the DF = 10000 solution became more significant for smaller DF solutions, which was not constant across different elements in a single solution but displayed general dependence on m/z. This indicates that at least two internal standards (e.g., In and Tl) are required for the correction of sensitivity variation. On the basis of the results, a new isotope dilution‐internal standardisation method for the determination of twenty‐two trace elements with ICP‐MS was developed, in which the sensitivity variation was corrected by monitoring two enriched isotopes, 113In and 203Tl. This method, coupled with the quantitative correction of interference from oxides and hydroxides, achieved precise determination of twenty‐two trace elements in some rock reference materials with reproducibilities of ±2% for basaltic to andesitic samples. 相似文献