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111.
A method for the determination of major, minor and trace elements in silicate samples by ICP‐QMS and ICP‐SFMS applying isotope dilution‐internal standardisation (ID‐IS) and multi‐stage internal standardisation has been developed. Samples with an enriched isotope of 149Sm (spike) were decomposed by a HF/HCIO4 mixture and stepwise drying and finally diluted. In ID‐IS for trace element analyses by Q‐pole type ICP‐MS (ICP‐QMS), the Sm concentration was determined by ID, while other trace elements (Li, Be, Rb, Sr, Y, In, Cs, Ba, La, Ce, Pr, Nd, Eu, Gd, Tb, Dy, Ho, Er, Tm, Yb, Lu, Tl, Pb, Bi, Th and U) were determined using the 149Sm intensity as an internal standard. Major and minor elements were determined by multi‐stage internal standardisation, with Na, Mg, Al, P, Ca, V, Mn, Fe and Co measured by sector magnetic field type ICP‐MS (ICP‐SFMS) at middle resolution (MR; M/AM =~ 3000) using Sr determined by ICP‐QMS in the sample as the internal standard. Potassium, Sc, Ni, Cu, Zn and Ga were measured at high resolution (HR; M/ΔM ~ 7500) using the Sr concentration obtained by ICP‐QMS or the Mn concentration obtained by ICP‐SFMS at MR as internal standard. The merit of ID‐IS is that accurate dilution of the sample is not required. Matrix effects on elemental ratios down to a dilution factor (DF) of 600 were not observed in either types of mass spectrometry. Pseudo‐flow injection (FI), where transient signals were integrated, was used in ICP‐QMS, while conventional continuous sample introduction was used in ICP‐SFMS, resulting in total required sample solutions of 0.026 ml and 0.08 ml, respectively. Detection limits were low enough to determine these elements in depleted ultramafic rocks, and typical reproducibilities for basalts were 3% (Li‐Be), 1% (Rb‐U), 5% (In, Tl and Bi), 7% (Sc‐Ga) and 3% (major elements). Carbonaceous chondrites including Orgueil (Cll), Murchison (CM2) and Allende (CV3), as well as reference materials, JB‐1, ‐2, ‐3, JA‐1, ‐2, ‐3 and JP‐1 (GSJ), BHVO‐1, AGV‐1, PCC‐1 and DTS‐1 (USGS), were analysed to show the applicability of this method. Une méthode permettant la détermination des éléments majeurs, mineurs et en trace dans les echantillons silicates par ICP‐QMS et ICP‐SFMS a été développée. Elle combine la standardisation interne par dilution isotopique (ID‐IS) et la standardisation interne en deux étapes. Les échantillons, auxquels est ajouté un spike enrichi en 149 Sm, sont décomposés par une mixture HF/HCIO4′ séchés progressivement puis dilués. Dans la phase de standardisation interne par dilution isotopique avec un ICP‐MS à quadrupôle (ICP‐QMS), la concentration en Sm est déterminée par dilution isotopique tandis que les autres éléments en trace (Li, Be, Rb, Sr, Y, In, Cs, Ba, La, Ce, Pr, Nd, Eu, Gd, Tb, Dy, Ho, Er, Tm, Yb, Lu, Tl, Pb, Bi, Th et U) sont déterminés en utilisant le signal de 149 Sm comme standard interne. Les éléments majeurs et mineurs sont déterminés par standardisation interne par étapes, avec Na, Mg, Al, P, Ca, V, Mn, Fe et Co mesurés par ICP‐MS à secteur magnétique (ICP‐SFMS) en résolution intermédiaire (MR; M/ΔM =~ 3000 en utilisant Sr, mesuré par ICP‐QMS comme standard interne. Les éléments K, Sc, Ni, Cu, Zn et Ga sont mesurés en Haute Résolution (M/ΔM ~ 7500) en utilisant comme standard interne, soit la concentration en Sr obtenue par ICP‐QMS soit la concentration en Mn obtenue par ICP‐SFMS en résolution moyenne. La technique de ID‐IS a l'avantage de ne pas nécessiter la connaissance exacte du facteur de dilution de l'Schantillon. Aucun effet de matrice sur la mesure de rapports élémentaires n'a été observé sur l'un ou l'autre des spectromètres de masse, ceci jusqu'à un facteur de dilution (DF) de 600. Les analyses par ICP‐QMS ont été effectuées par pseudo injection de flux (Fl) et intégration d'un signal transitoire tandis que les analyses par ICP‐SFMS l'ont été avec un système conventionnel d'introduction. Le volume total de solution d'échantillon nécessaire etait de 0.026 ml et 0.08 ml respectivement. Les limites de détection étaient suffisamment basses pour permettre la détermination de ces éléments dans des roches ultrabasiques et les reproductibilités pour les basaltes étaient de l'ordre de 3% (Li‐Be), 1 % (Rb‐U), 5% (In, Tl et Bi), 7% (Sc‐Ga) et 3% (tous les éléments majeurs). Des chondrites carbonées dont Orgueil (Cll), Murchison (CM2) et Allende (CV3) ainsi que des matériaux de référence JB‐1, ‐2, ‐3, JA‐1, ‐2, ‐3 et JP‐1 (GSJ), BHVO‐1, AGV‐1, PCC‐1 et DTS (USGS) ont été analysés pour démontrer l'applicabilité de la méthode. 相似文献
112.
Akio Yoshida 《Tectonophysics》1987,140(2-4):131-143
Seismic activity in the region surrounding the foci is investigated for three severe earthquakes (two with a magnitude of 6.1 and one with a magnitude of 5.3) which have occurred in Japan in recent years. The most conspicuous feature commonly noticed is precursory activation of seismic belts which include the focal regions of main shocks. The repetition of the same pattern in the space-time distribution of earthquake occurrence along the seismic belt is also observed for each case. The precursory activity of seismic belts terminates in rather a short period and, after that, the area around the focus of the forthcoming large earthquake becomes quiescent, which demonstrates the appearance of the seismic gap of the second kind (Mogi, 1979). The periods of seismic quiescence for the cases investigated in this paper are longer than those which are given by the regression relationship between earthquake magnitude and precursor time proposed for example, by Sekiya (1977). However, our definition of anomalous seismic activity is clear, and it is possible to give a physical meaning to it as an increase in the local stress field in the seismic belt. We propose that a kind of coupling between intraplate tectonic blocks, analogous to interplate coupling in the subduction region, is responsible for the formation of the stress field relevant to these earthquakes. Although this is at present only one of the possible viewpoints on the formation of the focal region of large intraplate earthquakes, it may be worthwhile to study various precursory phenomena in-connection with this hypothesis. 相似文献
113.
Preferred orientation of the dominant phyllosilicate phase (serpentine) in the matrix of the Murchison meteorite (C2) was determined by X-ray pole figure goniometry. The basal plane (001) of the phyllosilicate shows a clear preferred orientation of an axial concentration type. The preferred orientation is very weak in comparison with the orientations of known terrestrial tectonites, and it resembles the weakest case observed in the loosely consolidated clayey sediments from the deep ocean bottom. However, gentle sedimentation of platy phyllosilicate grains on a flat surface under a weak gravity field does not generate a sufficient preferred orientation. It is suggested that the preferred orientation in the matrix of Murchison was generated by uniaxial compaction, and the magnitude of strain to give rise to the observed degree of preferred orientation is evaluated as ?9%. There are two possible explanations of the deformation: dynamic compression caused by impact, and static compaction in a parent body. Though the latter case appears to be appropriate in the present case, it is not straightforward, however, to conclude that the suggested deformation is caused by burial compaction along gravity under lithostatic stress in a small primitive parent body. 相似文献
114.
Characteristics of vertical land movement and microearthquake activity in the northeastern Japan arc
Methods have been devised for analyzing vertical land movement and seismicity data using two-dimensional Chebychev functions and oblique projections. A filtering operation in the space domain is made possible by use of a two-dimensional Chebychev function. The oblique projections give an intuitive understanding of land deformation. Characteristic aspects of vertical land movement obtained by precise levelling and of the energy release of microearthquakes with depths shallower than 20 km in the northeastern Japan arc were investigated in detail applying these methods.Lineations with wavelength of about 20–60km trending towards NE—SW were found for both the land deformation and the seismicity. It should be noted that this trend is almost perpendicular to the direction of the strain migration and is related to other geophysical information. 相似文献
115.
Experimental study of syntectonic recrystallization of fine-grained quartz aggregates was carried out in order to simulate the development of some natural microstructures of quartz tectonites and to understand their formation condition. Agate was axially compressed with a constant-strain-rate apparatus. Experiments were conducted at 4 kbar solid confining pressure, 700–1000°C and 10−4-10−6 sec−1 to 10%–45% strain. In all runs, deformation has proceeded under wet condition caused by dehydration of pyrophyllite used as pressure medium.Two different types of microstructure were distinguished in the deformed specimens. One is P-type which is characterized by equant, equidimensional, and polygonal grains. The other is S-type which is characterized by the highly oblate grains with the largest dimension perpendicular to the compression axis. The P-type microstructure is developed at higher temperatures and slower strain rates, while the S-type developed at lower temperatures and faster strain rates. The transition between the S- and P-types is found to be very sharp. 相似文献
116.
Takaaki Noguchi Makoto Kimura Takahito Hashimoto Mitsuru Konno Tomoki Nakamura Michael E. Zolensky Ryuji Okazaki Masahiko Tanaka Akira Tsuchiyama Aiko Nakato Toshinori Ogami Hatsumi Ishida Ryosuke Sagae Shinichi Tsujimoto Toru Matsumoto Junya Matsuno Akio Fujimura Masanao Abe Toru Yada Toshifumi Mukai Munetaka Ueno Tatsuaki Okada Kei Shirai Yukihiro Ishibashi 《Meteoritics & planetary science》2014,49(2):188-214
On the basis of observations using Cs‐corrected STEM, we identified three types of surface modification probably formed by space weathering on the surfaces of Itokawa particles. They are (1) redeposition rims (2–3 nm), (2) composite rims (30–60 nm), and (3) composite vesicular rims (60–80 nm). These rims are characterized by a combination of three zones. Zone I occupies the outermost part of the surface modification, which contains elements that are not included in the unchanged substrate minerals, suggesting that this zone is composed of sputter deposits and/or impact vapor deposits originating from the surrounding minerals. Redeposition rims are composed only of Zone I and directly attaches to the unchanged minerals (Zone III). Zone I of composite and composite vesicular rims often contains nanophase (Fe,Mg)S. The composite rims and the composite vesicular rims have a two‐layered structure: a combination of Zone I and Zone II, below which Zone III exists. Zone II is the partially amorphized zone. Zone II of ferromagnesian silicates contains abundant nanophase Fe. Radiation‐induced segregation and in situ reduction are the most plausible mechanisms to form nanophase Fe in Zone II. Their lattice fringes indicate that they contain metallic iron, which probably causes the reddening of the reflectance spectra of Itokawa. Zone II of the composite vesicular rims contains vesicles. The vesicles in Zone II were probably formed by segregation of solar wind He implanted in this zone. The textures strongly suggest that solar wind irradiation damage and implantation are the major causes of surface modification and space weathering on Itokawa. 相似文献
117.
Tomoki Nakamura Aiko Nakato Hatsumi Ishida Shigeru Wakita Takaaki Noguchi Michael E. Zolensky Masahiko Tanaka Makoto Kimura Akira Tshuchiyama Toshihiro Ogami Takahito Hashimoto Mitsuru Konno Masayuki Uesugi Toru Yada Kei Shirai Akio Fujimura Ryuji Okazaki Scott. A. Sandford Yukihiro Ishibashi Masanao Abe Tatsuaki Okada Munetaka Ueno Junichiro Kawaguchi 《Meteoritics & planetary science》2014,49(2):215-227
The mineralogy and mineral chemistry of Itokawa dust particles captured during the first and second touchdowns on the MUSES‐C Regio were characterized by synchrotron‐radiation X‐ray diffraction and field‐emission electron microprobe analysis. Olivine and low‐ and high‐Ca pyroxene, plagioclase, and merrillite compositions of the first‐touchdown particles are similar to those of the second‐touchdown particles. The two touchdown sites are separated by approximately 100 meters and therefore the similarity suggests that MUSES‐C Regio is covered with dust particles of uniform mineral chemistry of LL chondrites. Quantitative compositional properties of 48 dust particles, including both first‐ and second‐touchdown samples, indicate that dust particles of MUSES‐C Regio have experienced prolonged thermal metamorphism, but they are not fully equilibrated in terms of chemical composition. This suggests that MUSES‐C particles were heated in a single asteroid at different temperatures. During slow cooling from a peak temperature of approximately 800 °C, chemical compositions of plagioclase and K‐feldspar seem to have been modified: Ab and Or contents changed during cooling, but An did not. This compositional modification is reproduced by a numerical simulation that modeled the cooling process of a 50 km sized Itokawa parent asteroid. After cooling, some particles have been heavily impacted and heated, which resulted in heterogeneous distributions of Na and K within plagioclase crystals. Impact‐induced chemical modification of plagioclase was verified by a comparison to a shock vein in the Kilabo LL6 ordinary chondrite where Na‐K distributions of plagioclase have been disturbed. 相似文献