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31.
Methyl-galactosides were oxidized at room temperature by galactose oxidase in a one-step reaction and afforded methyl-galactoaldehyde
in excellent yield and high purity. The resulting galactoaldehyde as a useful intermediate can be directly used in glycopeptide
synthesis. 相似文献
32.
The results of a general theoretical investigation of three commonly used types of inductive conductivity sensors, i.e., the single transformer, the double transformer, and the double transformer with an additional loop, are presented. The resulting formulas describe the dependence of the sensor output signal not only on the conductivity of the seawater but also on the parameters of the electrical circuit, among them the permeability of the transformer core(s), which-unlike the other parameters-shifts considerably during oceanographic in situ measurements. A mathematical discussion of these formulas shows that for certain circuit configurations, the sensor output is independent of changes in permeability. Most of these configurations form the basis of existing oceanographical conductivity sensors, among them the "classical" sensors developed by H. Hinkelmann [3], [4], and by N. L. Brown [14], while some others make evident further possibilities for eliminating the unwanted effects of shifting permeability. In the era of microelectronics, the latter might lead to a reassessment, especially of the single transformer-type sensor. 相似文献
33.
A formula for the thickness of a shear band formed in saturated soils under a simple shear or a combined stress state has been proposed. It is shown that the shear band thickness is dependent on the pore pressure properties of the material and the dilatancy rate, but is independent of the details of the combined stress state. This is in accordance with some separate experimental observations. Copyright © 2004 John Wiley & Sons, Ltd. 相似文献
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35.
Zhan-Le Du Hua-Ning Wang Xiang-Tao He National Astronomical Observatories Chinese Academy of Sciences Beijing Department of Astronomy Beijing Normal University Beijing 《中国天文和天体物理学报》2006,6(4):489-494
The maximum amplitudes of solar activity cycles are found to be well anti-correlated (r = -0.72) with the newly defined solar cycle lengths three cycles before (at lag -3) in 13-month running mean sunspot numbers during the past 190 years. This result could be used for predicting the maximum sunspot numbers. The amplitudes of Cycles 24 and 25 are estimated to be 149.5±27.6 and 144.3±27.6, respectively. 相似文献
36.
Abstract— Martian meteorites (MMs) have been launched from an estimated 5–9 sites on Mars within the last 20 Myr. Some 80–89% of these launch sites sampled igneous rock formations from only the last 29% of Martian time. We hypothesize that this imbalance arises not merely from poor statistics, but because the launch processes are dominated by two main phenomena: first, much of the older Martian surface is inefficient in launching rocks during impacts, and second, the volumetrically enormous reservoir of original cumulate crust enhances launch probability for 4.5 Gyr old rocks. There are four lines of evidence for the first point, not all of equal strength. First, impact theory implies that MM launch is favored by surface exposures of near‐surface coherent rock (≤102 m deep), whereas Noachian surfaces generally should have ≥102 m of loose or weakly cemented regolith with high ice content, reducing efficiency of rock launch. Second, similarly, both Mars Exploration Rovers found sedimentary strata, 1–2 orders of magnitude weaker than Martian igneous rocks, favoring low launch efficiency among some fluvial‐derived Hesperian and Noachian rocks. Even if launched, such rocks may be unrecognized as meteorites on Earth. Third, statistics of MM formation age versus cosmic‐ray exposure (CRE) age weakly suggest that older surfaces may need larger, deeper craters to launch rocks. Fourth, in direct confirmation, one of us (N. G. B.) has found that older surfaces need larger craters to produce secondary impact crater fields (cf. Barlow and Block 2004). In a survey of 200 craters, the smallest Noachian, Hesperian, and Amazonian craters with prominent fields of secondaries have diameters of ?45 km, ?19 km, and ?10 km, respectively. Because 40% of Mars is Noachian, and 74% is either Noachian or Hesperian, the subsurface geologic characteristics of the older areas probably affect statistics of recognized MMs and production rates of secondary crater populations, and the MM and secondary crater statistics may give us clues to those properties. 相似文献
37.
Xie Rui-xiang Wang Min Shi Shuo-biao Xu Chun Li Wei-hua Yan Yi-hua 《Chinese Astronomy and Astrophysics》2003,27(4):426-434
Using the decimetric (700–1500 MHz) radio spectrometer and the synchronous observational system with high temporal resolution at four frequencies (1420, 2130, 2840 and 4260 MHz) of Yunnan Observatory, two rare events were observed on 2001 June 24 and 1990 July 30. The former was a small radio burst exhibiting pulsations with short periods (about 29, 40 and 100 ms) in the impulsive phase. The latter was a large radio burst, which at 2840 MHz produced radio pulsations with period of about 30 ms. This paper focuses on pulsations with very short periods in the range of 29–40 ms. The mechanism of generation of such pulsations may be modulation of radio radiation by the periodic trains of whistler packets originating in unstable regions of the corona. Alternatively, these pulsations can be attributed to wave-wave non-linear interactions of electrostatic upper hybrid waves driven by beams of precipitating electrons in flaring loops. 相似文献
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