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1.
泡沫塑料吸附分离富集-电感耦合等离子体质谱法测定稀土矿石中的镓 总被引：1，自引：1，他引：0
采用电感耦合等离子体质谱法(ICP-MS)测定稀土矿石中的镓,高含量的稀土元素会造成严重的质谱干扰。本文采用聚氨酯泡沫塑料在6 mol/L盐酸介质中吸附样品溶液中的镓后,以0.5 mol/L氯化铵水浴加热解脱30 min,镓的吸附-解脱效率超过99%,稀土元素等干扰物质基本不进入解脱液中,即在富集镓的同时实现了镓与基体元素的高效分离,降低了质谱干扰。本方法检出限低(0.022μg/g),经土壤及水系沉积物标准物质验证,镓的测定值与标准值吻合(绝对偏差为0.38%~4.70%),实际稀土矿石样品的加标回收率为94.1%~100.6%,精密度(RSD)低于4%(n=12),可应用于分析一般地质样品以及稀土矿石中的镓。 相似文献
2.
以固体废弃物粉煤灰基地质聚合物为基本骨架,通过水热合成法将其原位转化为自支撑Na P型沸石分子筛型体,并研究了水热过程中碱液浓度、碱液体积、水热温度和水热时间对NaP型沸石分子筛结晶程度、形貌和机械强度的影响,得到粉煤灰基地质聚合物原位转化Na P型沸石分子筛型体的适宜条件为水热温度100℃、NaOH浓度2.0mol/L、NaOH体积50 m L、水热时间24 h。所得Na P型沸石分子筛型体的抗压强度为23.21 MPa,BET比表面积为50.46 m~2/g,已达到工业生产P型沸石的水平。该法工艺简单,环境友好,可控成型。在此方法的基础上通过改变原料配比和反应条件,可以合成其他类型的沸石分子筛型体。 相似文献
3.
本文系统总结了湖北宜昌地区省级及省级以上地质遗迹资源,认为该地区地质遗迹分布规律主要可概括为两个方面,一是受控于地形和河流的综合作用,以各类地貌景观遗迹为特点;二是各个地质时代地层剖面齐全,古生物化石产地聚集。其中可归类为世界级地质遗迹点为5个,均以“古生物化石”为核心,分别为三峡地区埃迪卡拉生物群、长阳寒武纪清江生物群、黄花场中奥陶统大坪阶“金钉子”、王家湾上奥陶统赫南特阶“金钉子”和远安三叠系南漳—远安动物群。立足于此,文中首次详细总结了这些地质遗迹点的化石代表、科学及科普意义,并从地质遗迹自身保护和应用方式、地质遗迹载体、地学研学、地质文化的传播和文创科普产品5个方面对古生物地质遗迹资源的发展模式进行了详细探讨,从而为宜昌地区全域地质遗迹开发和旅游提供新思路。 相似文献
4.
Identification of the Main Control Factors and Failure Modes for the Failure of Baiyuzui Landslide Control Project 总被引：1，自引：0，他引：1
Du Yi Yan Echuan Gao Xu Mwizerwa Schadrack Yuan Liwei Zhao Song 《Geotechnical and Geological Engineering》2021,39(5):3499-3516
Geotechnical and Geological Engineering - The failure of landslide control project presents a deformation that continues to develop along the crack system, and the continuous failure of mechanical... 相似文献
5.
三叠系沉积物广泛覆盖青藏高原东北缘,其中松潘—甘孜地区三叠系的沉积物得到了较系统的研究,但是青藏高原北缘的祁连山三叠系盆地的研究却较为缺乏。为了丰富相关研究和揭示区域构造演化的特点,通过古水流方向统计、砂岩中碎屑矿物统计和碎屑锆石U-Pb测年等方法对祁连山三叠纪盆地物源进行系统研究。结果表明,祁连山三叠系盆地的古流向主要有南东向、正南向、南西向,物源来自岩浆弧和大规模褶皱造山作用的混合区。祁连山三叠系砂岩中的碎屑锆石的年龄谱主要峰值集中在250~290 Ma、360~460 Ma、1 600~2 000 Ma和2 200~2 600 Ma这4个年龄段。通过对比分析华北板块、华南板块中和秦祁昆中央造山带中岩浆锆石年龄谱特征可知:1 600~2 000 Ma和2 200~2 600 Ma年龄段的锆石来自华北板块,360~460 Ma年龄段的锆石来自北祁连造山带,250~290 Ma年龄段的锆石来自东昆仑的火山岛弧。此外,600~1 000 Ma年龄段锆石很少,这些锆石来自扬子板块,表明在三叠纪扬子克拉通和华北克拉通发生碰撞形成了秦岭造山带,阻断了来自扬子克拉通的物源。 相似文献
6.
The Triassic hothouse world experienced dynamic changes in climate and ecosystems that set the Earth's climate and biotic states for much of the Mesozoic Era. A critical time interval was the Carnian Stage (~237–227 Ma), which not only saw the first appearance of dinosaurs in the fossil record but witnessed a large igneous province eruption (Wrangellia LIP) and a sudden climate shift, the Carnian Pluvial Episode (CPE). Compelling hypotheses suggest that the Wrangellia eruptions caused the CPE, which in turn set the stage for the origin and initial diversification of dinosaurs. Unfortunately, testing these hypotheses is difficult because most relevant Carnian sedimentary archives possess few if any absolute age constraints, and there are little detailed paleoclimatic data for the CPE outside of the Tethys region. There is little existing evidence for the CPE in Gondwana, even though this region contains by far the best fossil record of early dinosaurs and their close relatives. We present new high-resolution geochronologic and paleoclimatic data from Carnian-aged strata in the Ischigualasto-Villa Unión Basin of northwest Argentina, which also preserves fossils of the earliest-known dinosaurs. New CA-TIMS UPb zircon age of 234.47 ± 0.44 Ma from the lower Los Rastros Formation demonstrates that most of the overlying lacustrine strata within this basin was deposited during or after the CPE, including large dinosauriform footprints. Multiproxy paleoenvironmental data (sedimentology, clay mineralogy, C and O stable isotopes, and fossils) from the same strata are the first detailed paleoclimate data for the CPE in Gondwana, and provide evidence that the CPE interval in western Gondwana was indeed warmer and more humid than before or after. These data are consistent with the interpretation of the CPE as a global event, but direct linkages in Gondwana and the Tethys with the origin and initial diversification of dinosaurs are less clear. 相似文献
7.
山东土堆－沙旺金矿床同位素组成特征及矿床成因讨论 总被引：2，自引：0，他引：2
土堆－沙旺金矿床位于胶莱盆地东北缘, 为胶东东部牟平－即墨成矿带的重要组成部分。石英流体包裹体Rb－Sr等时线年龄为119±10 Ma,与胶东大规模成矿时间一致。矿石硫化物硫同位素组成δ34S介于8.50‰～12.72‰之间, 成矿热液δ34S∑S=10.03‰, 铅同位素组成中206Pb/204Pb＝17.12～17.86, 且具有低μ高ω特征, 指示成矿物质来源于下地壳或地幔。氢氧同位素δ18OH2O值为+1.96‰～＋7.71‰, δD为–68.64‰～–86.47‰, 显示成矿流体主体为岩浆水, 并有部分后期大气水的参与。矿石铅同位素与同期脉岩组成接近, 且具有线性特点, 指示二者可能与早白垩世华北克拉通东部构造体制转化所引起的壳幔岩浆混合作用有关。 相似文献
8.
《Gondwana Research》2014,25(3-4):1203-1222
Reactivation of cratonic basement involves a number of processes including extension, compression, and/or lithospheric delamination. The northern margin of the North China Craton (NCC), adjacent to the Inner Mongolian Orogenic Belt, was reactivated in the Late Paleozoic to Early Mesozoic. During this period, the northern margin of the NCC underwent magmatism, N–S compression, regional exhumation, and uplift, including the formation of E–W-trending thick-skinned and thin-skinned south-verging folds and south-verging ductile shear zones. zircon U–Pb SHRIMP ages for mylonite protoliths in shear zones which show ages of 310–290 Ma (mid Carboniferous–Early Permian), constraining the earliest possible age of deformation. Muscovite within carbonate and quartz–feldspar–muscovite mylonites from the Kangbao–Weichang and Fengning–Longhua shear zones defines a stretching lineation and gives 40Ar/39Ar ages of 270–250 Ma, 250–230 Ma, 230–210 Ma, and 210–190 Ma. Deformation developed progressively from north to south between the Late Paleozoic and Triassic. Exhumation of lower crustal gneisses, high-pressure granulites, and granites occurred at the cratonic margin during post-ductile shearing (~ 220–210 Ma). An undeformed Early Jurassic (190–180 Ma) conglomerate overlies the deformed rocks and provides an upper age limit for reactivation and orogenesis. Deformation was induced by convergence between the southern Mongolia and North China cratonic blocks, and the location of this convergent belt controlled later deformation in the Yanshan Tectonic Province. This province formed as older E–W-trending Archean–Proterozoic sequences were reactivated along the northern margin of the NCC. This reactivation has features typical of cratonic basement reactivation: compression, crustal thickening, remelting of the mid to lower crust, and subsequent orogenesis adjacent to the orogenic belt. 相似文献
9.
随着新型城镇化和国土空间规划工作的推进,半城市化地区的科学发展与治理已成为城乡融合发展的重要环节。基于文献计量分析方法,运用CiteSpace和VOSviewer可视化工具,对近30年来国内半城市化研究进行知识图谱分析。结果表明：1）作者与机构研究力量分散,地域分布特征明显;2）研究热点聚焦于分析北京、广州、上海等发达城市的土地利用、景观格局、失地农民、影响因素等问题,其内容可聚类为形态特征、空间界定、驱动机制、协调发展4类主题;3）半城市化研究发展经历了3个阶段,研究区域从东南沿海向内陆转移,内容从定性理论分析向定量实证探讨转化,视角也由自然特性分析向社会发展研究转变,体现出更多人文关怀。最后,从半城市化地区空间范围界定、人居环境建设、农业转移人口市民化路径探讨和基本公共服务均等化实施4个方面进行展望,旨在为中国半城市化地区的发展提供参考。 相似文献
10.
ZHANG Yanwen ZHANG Xiaofei CHEN Lixin PANG Zhenshan CHEN Hui XUE Jianling ZHOU Yi TENG Chao CHEN Guochao 《《地质学报》英文版》2023,97(4):1094-1111
The southern Great Xing’an Range is the most critical Sn-polymetallic metallogenic belt in northeast China. However, the tectonic setting of the Early Cretaceous magmatic-metallogenic ”flare-up“ event remains uncertain. This paper presents an integrated study on the occurrence, petrology, zircon U-Pb ages, whole-rock geochemistry, and in situ zircon Hf isotopes for Wenduerchagan granites of Xi Ujimqin Banner, central-eastern Inner Mongolia. These granites consist primarily of granite porphyry(wi... 相似文献