岩石矿物及粉尘中游离二氧化硅的测定     

席进萍  沈燕君等 《岩矿测试》2002,21(1):71-73

改进了游离二氧化硅（fSiO2)测定中试样的分解方法，采用硫－磷混酸替代单独使用磷酸分解试样，防止了焦磷酸盐的形成，同时，氟硼酸对fSiO2的溶解率符合测定要求。改进的方法用于标准物质中fSiO2的测定，结果与标准值或磷酸溶矿重量法相符。对于ω(fSiO2)=3.26%的标样10次测定的RSD为2．4％。  相似文献   

2—（2，3，5—三氮唑偶氮）—1，8—二羟基—3，6—萘二磺酸与钴的显色反应及应用     

韩德满  蒋华江  叶巧云 《岩矿测试》2002,21(2):155-157

介绍了新水溶性显色剂 2 - ( 2 ,3,5 -三氮唑偶氮 ) - 1 ,8-二羟基 - 3,6-萘二磺酸与钴的显色反应及应用 ,建立了测定钴的新方法。在 pH 9.9的Na2 B4O7 NaOH缓冲液中该试剂与钴形成 1∶1蓝色稳定络合物 ,λmax为 5 88.8nm ,Co的质量浓度在 0～ 1 .0mg/L内符合比尔定律 ,表观摩尔吸光系数为 3.46× 1 0 4 L·mol- 1 ·cm- 1 。所拟方法用于环境水样及维生素B1 2 注射液中的微量钴测定 ,结果与原子吸收法相符 ,5次测定的RSD <1 %。  相似文献   

Self‐purification in Upland and Lowland Streams     

Ines Heidenwag  Uta Langheinrich  Volker Lüderitz 《洁净——土壤、空气、水》2001,29(1):22-33

Ecological investigations at four streams in Saxony‐Anhalt have shown that there are considerable differences between the self‐purification power of upland and lowland streams. This result is reflected in chemistry and in microbiology. The structure of the bottom substrate mainly influences the degree of self‐purification in connection with rate of flow and flow velocity. The results and differences are demonstrated using the example of Katzsohlbach in the landscape unit “Mittel‐ and Unterharz” and the stream Olbe in the landscape unit “Magdeburger Börde”.  相似文献   

Oxidation Experiment of Natural Megacrystal Clinopyroxene: Implications for Assignment of Mössbauer Spectra     

ZHI Xiachen  CHEN Peng  LIN Chengzhong  CHEN Shuqing  ZHANG Guilan  LI Yuzhi  LIN Lei 《《地质学报》英文版》2001,75(1):51-58

The Mössbauer spectra of natural megacrystal clinopyroxene are usually fitted by 4 sets of symmetric doublets, A‐A', B‐B', C‐C' and D‐D', respectively, in terms of increasing Qs value in literature. But the assignments of those doublets are quite different, except the D‐D' doublet assigned to Fe³⁺at the lattice site M***1 in previous papers. Particularly, the assignment and interpretation of the C‐C' doublet are diverse. The oxidation experiments of natural megacrystal clinopyroxene collected from the Hannuoba basalt, North China, were performed under controlled conditions of temperature at 1000°C and oxygen fugacity of FMQ buffer in 1, 2, ***3 and 5 days respectively. The oxidized samples were then measured by X‐ray diffraction spectrometry and Mössbauer spectrometry. The oxidation of clinopyroxene is characterized by Fe²⁺ → Fe³⁺at M1 under the subsolidus conditions, which is consistent with the increase of the area of the D‐D' doublet when the heating time increases. Accordingly, the area of the A‐A' and B‐B' doublets decreases with the increasing heating time. However, the area of C‐C' keeps almost constant. Therefore, the 4 sets of doublets can be assigned correctly as follows: A‐A' doublet to Fe⁺²at M1, B‐B' Fe²⁺at M1, C‐C' Fe²⁺at M2, and D‐D' Fe³⁺at M1. The M1 site splitting is due to the NNN (Next Nearest Neighbour) effect of the M2 site. The amount of Fe³⁺at the tetrohedral site of megacrystal clinopyroxene is negligible according to this study.  相似文献   

The use of sintered diamond anvils in the MA8 type high-pressure apparatus     

Tadashi Kondo  Hiroshi Sawamoto  Akira Yoneda  Manabu Kato  Akihito Matsumuro  Takehiko Yagi  Takumi Kikegawa 《Pure and Applied Geophysics》1993,141(2-4):601-611

A new multi-anvil type high-presure apparatus has been developed using sintered diamond anvils to generate pressures over 30 GPa and temperatures up to about 2000°C. A maximum sample volume of about 1 mm³ is available in this system. The pressure was confirmed by dissociation of forsterite into Mg-perovskite and periclase. The basic techniques and problems in utilizing sintered diamond in the MA8 type high-pressure apparatus are discussed with an emphasis on the future prospect of incorporating simultancous X-ray diffraction observation.  相似文献   

利用IRS-P6卫星数据制作遥感影像地图     

张幼莹 《国土资源信息化》2006,29(1):30-32,5

本文介绍了以IRS-P6卫星数据作为信息源完成大兴安岭林区的遥感影像地图制作的方法, 通过试验初步认识到:利用IRS-P6卫星数据制作遥感影像地图,可以满足1:50000、 1:25000比例尺的平面制图精度要求,在一些专业和专题应用中可以放大到1:15000比例尺使用。  相似文献   

Rational function model for sensor orientation of IRS-P6 LISS-4 imagery     

V. Nagasubramanian    P. V. Radhadevi    R. Ramachandran    R. Krishnan 《The Photogrammetric Record》2007,22(120):309-320

  相似文献   

湖泊水位资料与模型模拟恢复的6000年前全球湿润状况的对比研究     

秦伯强  于革  SandyPHarison 《气象学报》1998,56(3):272-283

本项研究是ＰＭＩＰ（ＰａｌａｅｏｃｌｉｍａｔｅＭｏｄｅｌｉｎｇＩｎｔｅｒｃｏｍｐａｒｉｓｏｎＰｒｏｊｅｃｔ）国际合作项目中有关模型模拟与观测资料对比的一部分。模型试验对象是６０００ｙｒ．ＢＰ的全球湿润状况。模拟试验以检测太阳辐射变化对全球大尺度气候系统的影响为主要目的。观测资料是利用地质证据恢复的古湖泊水位变化,实际上是某一地区的有效降水（降水减蒸发）的变化。通过两者的比较发现,所有模拟试验均能重现６０００ｙｒ．ＢＰ在亚洲南部与非洲北部的湿润环境,从而证实了因太阳辐射变化导致的亚洲与非洲季风的增强。但模拟的季风增强无论是强度还是范围均小于地质记录。原因很可能是模拟试验中下垫面特征用“现代”的来处理。模拟试验对北半球夏季辐射增加造成的西风带北移及由此引起的中纬度地区的气候变化不够成功。绝大多数模拟对受洋流与海温影响较大的地区是失败的。主要原因可能是所有ＰＭＩＰ中的模拟试验都未考虑海洋的作用。  相似文献   

鄂尔多斯盆地南部旬邑-宜君地区中生界储层特征   总被引：1，自引：0，他引：1  

张学例  王代国  陈淑惠 《地球科学与环境学报》2000,22(4)

对鄂尔多斯盆地南部旬邑 -宜君地区中生界主要储集层——直罗组、延安组、延长组储层特征从沉积相、砂体纵向展布、岩性和物性等几方面进行了简要论述。通过研究指出本区储层具有低孔、低渗的特点。在纵向上以直罗组储层相对最好 ,延安组次之 ,之后才是三叠系延长组。储集层普遍具有岩性细、成岩后生变化强烈的特点。由于储层低孔、低渗 ,因此 ,油层的压裂改造措施必不可少  相似文献   

Exploring the X-ray spectral variability of MCG–6-30-15 with XMM–Newton     

J. Larsson  A. C. Fabian  G. Miniutti  R. R. Ross 《Monthly notices of the Royal Astronomical Society》2007,376(1):348-352

We present a study of the spectral variability of the Seyfert I galaxy MCG–6-30-15 based on the two long XMM–Newton observations from 2000 and 2001. The X–ray spectrum and variability properties of the 2001 data have previously been well described with a two-component model consisting of a variable power-law and a much less variable reflection component, containing a broad relativistic iron line from the accretion disc around a rapidly rotating Kerr black hole. The lack of variability of the reflection component has been interpreted as an effect of strong gravitational light bending very close to the central black hole. Using an improved reflection model, we fit the two-component model to time-resolved spectra of both observations. Assuming that the photon index of the power law is constant, we reconfirm the old result and show that this does not depend on the time-scale of the analysis.  相似文献