论氢化物的形成及其在分析测试领域的应用          下载免费PDF全文

郑大中  王惠萍  郑若锋 《江苏地质》2008,32(1):5-11

论述了氢化物形成的普遍性、氢化物的物理化学性质、元素周期系各类元素的氢化物类型。认为一些金属离子、非金属离子在酸性介质中与硼氢化钾（钠）作用及金属锌等强还原剂作用生成氢化物。综述了氢化物的形成在分析测试领域的应用：试样分解、分离富集、容量分析、光度分析、原子光谱分析、质谱分析。  相似文献   

MS SQL Server渗透测试方法     

谢朝海  王建法  董平 《国土资源信息化》2008,(5):35-38

当前电子政务、电子商务和企业内部的很多数据和敏感信息都存放在MS SQL Server数据库中,但是SQL Server数据库的安全性却一直没有像操作系统和网络设备那样受到应有的重视,得到恰当的测试评估。鉴于此,本文提出可以利用两类不同的安全漏洞对SQL Server数据库进行渗透测试,给出具体的测试方法,用以指导信息系统数据库管理员进行自测试评估,及时发现存在的严重安全漏洞,以进一步采取措施,进行漏洞修补。  相似文献   

电容测试法判断测井电缆系统故障     

马世稳  张著军 《中国煤炭地质》2008,(12):44-45

测井电缆因长途颠簸、拉伸及绞车缠绕挤压,电缆连接器、电缆、绞车滑环、滑环连线等部位极易出现故障。电容测试法是一种简易、快速的检测方法,该法可在现场准确诊断出故障电缆的位置。以四芯铠装电缆为例,每根缆芯的正常阻值约为80Ω/1 000m,两缆芯间的分布电容约为170PPF/1 000m。在实际检测中,根据电容较小时测点的位置,可以有效判断故障部位;而电缆故障位置则可利用电阻及电容的线性关系进行计算予以确定。  相似文献   

Timing effects on the fragmentation of small scale blocks of granodiorite     

P. D. Katsabanis  A. Tawadrous  C. Braun  C. Kennedy 《Fragblast: International Journal for Blasting and Fragmentation》2006,10(1):83-93

A series of small scale tests, simulating multi-hole blasts have been performed to establish the effect of delays on blast fragmentation. The blasts were performed in high quality granodiorite blocks, which were cut from stone prepared by dimensional stone quarry operations. The pattern used was equilateral triangular, with a distance of 10.2 cm between boreholes, which had a diameter of 11 mm, were loaded with detonating cord and the coupling medium was water. The delays used were achieved using different lengths of detonating cord for the cases of delays between 0 and 100 μs between holes and a sequential blasting machine firing seismic detonators for larger delays up to 4 ms. All fragments were collected and screened. The experiments showed that the worst fragmentation was achieved with simultaneous initiation of all charges. Fragmentation improved with the delay time between holes up to 1 ms between holes. If the experiments are scaled up, the results show that in granodiorite, fragmentation optimization requires delays of few milliseconds per metre of burden. The findings, agree with previously published work, involving larger scale experiments and other rock types.  相似文献   

Damage risk assessment of breakwaters under tsunami attack     

Ayşen Ergin  Can Elmar Balas 《Natural Hazards》2006,39(2):231-243

Turkey was struck by two major events on 17 August and 12 November 1999, named Izmit (M _w = 7.4) and Düzce (M _w = 7.2) earthquakes, respectively. Rubble mound breakwaters in Izmit Bay experienced little damage, as forecasted by the new risk assessment model in which tsunami occurrence risk was included in the damage estimations. In order to determine the occurrence probability of structural damage under design conditions, including the environmental loading parameters of tsunami and storm waves, tidal range and storm surge, the Conditional Expections Monte Carlo simulation was applied in the risk assessment model developed in this study for the Esenköy Fishery Harbour, Turkey. A tsunami was not the key design parameter when compared to storm waves for the main breakwater of the harbour, however, in places with great seismic activity, the tsunami risk should be important depending on the occurrence probability and magnitude of the tsunami.  相似文献   

新近沉积粉细砂层地基的试验与评价     

赵本肖  游占军 《中国煤田地质》2006,18(4):45-46,48

通过对邯郸市某车间地基的勘察．分析和探讨了新近沉积粉细砂地层的勘察手段、其物理力学性质，及其利用载荷试验确定承载力的标准取得了较为满意的结果，提出的一些分析方法，对新近沉积的粉细砂地层的勘察具有一定的借鉴作用。  相似文献   

Site Investigation for the Effects of Vegetation on Ground Stability     

John R. Greenwood  Joanne E. Norris  Jo Wint 《Geotechnical and Geological Engineering》2006,24(3):467-481

The procedure for geotechnical site investigation is well established but little attention is currently given to investigating the potential of vegetation to assist with ground stability. This paper describes how routine investigation procedures may be adapted to consider the effects of the vegetation. It is recommended that the major part of the vegetation investigation is carried out, at relatively low cost, during the preliminary (desk) study phase of the investigation when there is maximum flexibility to take account of findings in the proposed design and construction. The techniques available for investigation of the effects of vegetation are reviewed and references provided for further consideration. As for general geotechnical investigation work, it is important that a balance of effort is maintained in the vegetation investigation between (a) site characterisation (defining and identifying the existing and proposed vegetation to suit the site and ground conditions), (b) testing (in-situ and laboratory testing of the vegetation and root systems to provide design parameters) and (c) modelling (to analyse the vegetation effects).  相似文献   

非等截面桩超声波成孔质量检测     

韩亮 《物探与化探》2005,29(2):185-188

分析了非等截面超声波成孔质量检测的几个主要影响因素,给出了相应得改进措施。用工程实例说明超声波反射技术是一种保证非等截面桩成孔质量和成桩质量必不可少的检测方法。  相似文献   

G-Probe-1 - An International Proficiency Test for Microprobe Laboratories - Report on Round 1 : February 2002 (TB-1 Basaltic Glass)     

Philip J. Potts  Michael Thompson  Stephen Wilson 《Geostandards and Geoanalytical Research》2002,26(2):197-235

Results are presented for round one of a new international proficiency testing programme designed for microprobe laboratories involved in the routine analysis of silicate minerals. The sample used for this round was TB-1, a basaltic glass fused and prepared by the USGS. Thirty nine laboratories contributed data to this round, the majority of major element results being undertaken by EPMA and the majority of trace elements by LA-ICP-MS. Assigned values were derived from the median of results produced by nine selected laboratories that analysed powdered material by conventional ICP-MS, INAA and XRF techniques using bulk powders of the sample. Submitted microprobe results were evaluated using a target precision calculated using the Horwitz function, adopting the same criteria as those used for "applied" geochemistry laboratories in the companion GeoPT proficiency testing programme for laboratories involved in the routine bulk analysis of silicate rocks. An evaluation of results from participating microprobe laboratories indicated that overall, data were compatible with this precision function. A comparison between the performance of bulk and microprobe techniques used in the analysis of the basaltic glass showed remarkably good agreement, with significant bias only observed for the major oxide MgO.  相似文献   

嵌岩桩与含沉渣桩低应变动力检测曲线理论计算方法与特征研究   总被引：2，自引：3，他引：2  

刘煜洲  刘东甲  王杰英 《物探化探计算技术》2003,25(2):97-104

根据文献[1]、[2]介绍了基桩反射波法动测正演问题的数理模型、计算方法及其通用性，并据此计算了完整嵌岩桩及有不同厚度沉渣的嵌岩桩与摩擦桩的理论曲线。提出了在一定物性参数条件下判断沉渣是否超过规定标准的方法，并给出了数个实例。  相似文献