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991.
992.
悬浮进样石墨炉原子吸收法测定纳米氧化锆粉体中的微量铝 总被引:2,自引:0,他引:2
采用水介质直接分散纳米氧化锆粉体悬浮进样,以水标准溶液绘制校正曲线,石墨炉原子吸收法测定其中的微量Al。系统研究了Al的原子化和灰化行为,不同分散介质及基体元素对测定Al的影响,获得了测定Al的优化条件。方法对Al的检测限为0.5ng/g,Al的线性范围为0~2.5mg/L,基体ZrO2的质量浓度小于2g/L时,对Al的测定无干扰,悬浮进样直接测定的RSD(n=5)为6.0%。样品的测定结果与其他方法对比基本一致。 相似文献
993.
活性炭对无机汞和苯基汞的吸附行为探讨 总被引:3,自引:0,他引:3
试验了活性炭对无机汞和苯基汞的吸附和解吸行为。结果表明,在活性炭用量为0.2g,ψ=0.5%的王水介质中搅拌1.5h,无机汞和苯基汞的吸附率均达96%以上,无机汞和苯基汞的吸附容量分别为82.5μg/g和66.0μg/g。吸附后的无机汞和苯基汞分别用含有60mg EDTA的2.8mol/L HNO3溶液和5.6mol/L HNO3-1.0mol/L H2SO4溶液定量洗脱,用冷原子吸收光谱法测定,实现了无机汞和苯基汞的定量分离。对2μg/L的无机汞和苯基汞进行测定,相对标准偏差(n=11)分别为5.4%和6.2%。在实际水样中加标回收和测定,无机汞和苯基汞的回收率分别为97.8%~108%、94.0%~106%。 相似文献
994.
Short-wave infrared (SWIR) reflectance spectroscopy was used to characterize hydrothermal minerals and map alteration zones
in the Tuwu Cu–Au deposit, Xinjiang, China. The Palaeozoic hydrothermal system at Tuwu is structurally controlled, developed
in andesitic volcanic rocks and minor porphyries. Hydrothermal alteration is characterized by horizontally zoned development
of quartz, sericite, chlorite, epidote, montmorillonite and kaolin about individual porphyry dykes and breccia zones, as is
shown by changes outward from a core of quartz veining and silicification, through an inner zone of sericite + chlorite to
a marginal zone of chlorite + epidote. The alteration system comprises several such zoning patterns. Silicification and sericitization
are spatially associated with Cu–Au mineralization. Zoning is also shown by compositional variations such that Fe-rich chlorite
and Al-rich sericite occur preferentially toward the core and the most intensely altered parts, whereas Mg-rich chlorite and
relatively Al-poor sericite are present on the margin and the relatively weakly altered parts of the hydrothermal alteration
system. The compositions of chlorite and sericite, therefore, can be potentially used as vectors to Cu–Au mineralization.
Montmorillonite and kaolinite, of probable weathering origin, are located near the surface, forming an argillic blanket overlying
Cu–Au mineralization. Sporadic montmorillonite is also present at depth in the hydrothermal alteration system, formed by descending
groundwater. Presence of a well-developed kaolinite-bearing zone on the surface is an indication of possible underlying Cu–Au
mineralization in this region. Epidote occurs widely in regional volcanic rocks, as well as in variably altered rocks on the
margin of the hydrothermal mineralization system at Tuwu. The widespread occurrence of epidote in volcanic country rocks probably
reflects a regional hydrothermal alteration event prior to the localized, porphyry intrusion-related hydrothermal process
that led to the Cu–Au mineralization at Tuwu. 相似文献
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999.
M. EISINGER A. RICHTER A. LADSTÄTTER-WEIßENMAYER J. P. BURROWS 《Journal of Atmospheric Chemistry》1997,26(1):93-108
Observations of stratospheric BrO over Bremen (53°N) are reported for winter and early spring periods of 1993 and 1993/94. The BrO was observed by ground-based near-UV absorption spectroscopy of sunlight scattered in the zenith. Differential slant column densities for solar zenith angles 90°/80° in the range of9× 1013 (detection limit) to 4.5×1014 molecules/cm2 having a high day-to-day variability were found. For the majority of the measurements no significant difference was observed between the morning and evening behaviour of BrO. Exceptions are the morning measurements from the winter of 1992/93 where an accelerated production of BrO was observed. We believe the latter best to be explained by the early morning rapid photolysis of elevated amounts of photo-labile Br-reservoirs formed during the night. The largest differential slant column densities of BrO were measured in December 1993 when the temperatures at 30 hPa dropped below 205 K. This might be an indication of heterogeneous conversion of bromine compounds on sulfate and other aerosols. 相似文献
1000.
本文是关于云和云天大气对太阳辐射吸收异常问题的一个综述,总结了到目前为止的对水云异常吸收的一些解释,指出这些解释的合理性和缺陷。本文的重点在于介绍近年来论争激烈的有云大气的异常吸收问题,对存在和不存在增强吸收的两种截然相反的观点都做了较详细的评述。 相似文献