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51.
D.?AnfossiEmail author D.?Oettl G.?Degrazia A.?Goulart 《Boundary-Layer Meteorology》2005,114(1):179-203
When the wind speed decreases below a certain value (1–2 m s-1) meandering (low frequency horizontal wind oscillations) starts to prevail. In these conditions it becomes difficult to define a precise mean wind direction and to estimate the airborne dispersion. To study the wind and turbulence characteristics during meandering, two sonic anemometer datasets, containing hourly wind observations, were analysed: the first one, lasting 1 year, was recorded in complex terrain (Graz, Austria) and the second one, lasting about 1month, was recorded in a rather flat area (Tisby, Sweden). It was found that meandering seems to exist under all meteorological conditions regardless of the stability or wind speed and it was confirmed that meandering sets a lower limit for the horizontal wind component variances. Further, it was found that the autocorrelation functions of the horizontal wind components, computed for the low wind cases, show an oscillating behaviour with the presence of large negative lobes. Two different relationships from the literature, and relevant to these oscillatory aspects, were fitted to the data. They contain two parameters: one associated and relevant to the classical integral time scale and the second with meandering occurrence. Based on these relationships, expressions for the mean square displacement of particles y2(t) were also derived. 相似文献
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An effective novel ultrasonic extraction procedure coupled with gas chromatography and negative chemical ionization mass spectroscopy has been developed for quantitative recovery of polar herbicides in soil. This rapid one-step sample preparation methodology was named accelerated ultrasonic extraction (AUE), and is based on elevated temperatures, increased power and dispersing intimate contact. Simultaneously, in-situ derivatization was achieved by the addition of derivatization reagent, chelating agent and dispersing agent. The extraction efficiency was enhanced by the multiple applied force and elevated ultrasonic temperature. The in-situ derivatization efficiency was enhanced considerably by the use of ultrasonic energy. Dozens of samples can be extracted simultaneously with this method. The sensitivity was improved because of the remarkable reduced background noise achieved using GC-MS in negative chemical ionization (NCI) mode. The amount of reagent and various ultrasonic parameters, such as ultrasonic energy, ultrasonic time and ultrasonic temperature, were optimized. The reproducibility of replicate soil extraction determination of 9 herbicides in different matrix samples and at different concentrations (n=7) was in the range of 4.9-12.6% of the relative standard deviation. The obtained LOD values ranged between 0.02-0.37 g/kg for all herbicides. Here, we present an improved ultrasonic extraction procedure, which we have termed AUE, can serve as a rigorous high efficiency preparation methodology for polar organic contaminants and can be applied to solid sample pre-treatment extensively 相似文献
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Ultrasonic wave extraction and simultaneous analysis of polycyclic aromatic hydrocarbons (PAHs) and phthalic esters in soil 下载免费PDF全文
ZHANG Yong-tao ZHAO Guo-xing LIU Jing-shang ZHANG Li LI Xiao-ya GUI Jian-ye ZHANG Chen-ling 《地下水科学与工程》2017,5(3):249-253
A method is developed for detection of polycyclic aromatic hydrocarbons(PAHs) and Phthalic Acid Esters(PAEs) in soil samples. Ultrasonic Wave Extraction under airtight circumstances is adopted to extract the analytes in soil samples with n-hexane–acetone(V:V=1:1) as extraction solvent. This method has several advantages, including high extraction efficiency, short time, convenience and simplicity. It can be used to detect polycyclic aromatic hydrocarbons(PAHs) and Phthalic Acid Esters(PAEs) in soil. 相似文献
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The elastic properties of CaSnO3 perovskite have been measured by both ultrasonic interferometry and single-crystal X-ray diffraction at high pressures. The single-crystal diffraction data collected using a diamond-anvil cell show that CaSnO3 perovskite does not undergo any phase transitions at pressures below 8.5?GPa at room temperature. Ultrasonic measurements in the multianvil press to a maximum pressure of ~8?GPa at room temperature yielded S- and P-wave velocity data as a function of pressure. For a third-order Birch-Murnaghan EoS the adiabatic elastic moduli and their pressure derivatives determined from these velocity data are K S0=167.2±3.1?GPa, K ′ S0=4.89±0.17, G 0=89.3±1.0?GPa, G ′ 0=0.90±0.02. The quoted uncertainties include contributions from uncertainties in both the room pressure length and density of the specimen, as well as uncertainties in the pressure calibration of the multianvil press. Because the sample is a polycrystalline specimen, this value of K S0 represents an upper limit to the Reuss bound (conditions of uniform stress) on the elastic modulus of CaSnO3 perovskite. If the value of αγT is assumed to be 0.01, the value of K S0 corresponds to K T0=165.5±3.1?GPa. The 10 P-V data obtained by single-crystal diffraction were fit with a third-order Birch–Murnaghan equation-of-state to obtain the parameters V 0=246.059±0.013 Å3, K T0=162.6±1.0?GPa, K ′ T0=5.6±0.3. Because single-crystal measurements under hydrostatic conditions are made under conditions of uniform stress, they yield bulk moduli equivalent to the Reuss bound on a polycrystalline specimen. The results from the X-ray and ultrasonic experiments are therefore consistent. The bulk modulus of CaSnO3 perovskite lies above the linear trend of K 0 with inverse molar volume, previously determined for Ca perovskites. This prevents an estimation of the bulk modulus of CaSiO3 perovskite by extrapolation. However, our value of G 0 for CaSnO3 perovskite combined with values for CaTiO3 and CaGeO3 forms a linear trend of G 0 with octahedral tilt angle. This allows a lower bound of 150?GPa to be placed on the shear modulus of CaSiO3 by extrapolation. 相似文献
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在小型垂直过冷云风洞中引进和改装了亚都工业用超声波加湿器,使其成为风洞实验的造雾系统,在实验中测量了其雾滴谱,模拟了冰雪晶生长过程,结果表明,此造雾系统符合实验要求。 相似文献
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New Equations For Sonic Temperature Variance And Buoyancy Heat Flux With An Omnidirectional Sonic Anemometer 总被引:2,自引:0,他引:2
Many new types of sonic anemometer obtain sonic temperature from an average value of temperature measured along three paths, unlike previous sonic anemometers that generally used one path. New equations are derived to calculate temperature variance from sonic temperature variance and sensible heat flux from buoyancy flux considering the influence of a crosswind. These equations can be applied to CSAT3, Solent R2, R3, R3A, HS, and USA-1 sonic anemometers with the corresponding correction factors given in this paper. The equations are verified by data measured by a CSAT3 sonic anemometer in the LITFASS-1998 field study. 相似文献