电感耦合等离子体原子发射光谱法测定黄铁矿中微量元素   总被引：5，自引：7，他引：5  

常平  王松君等 《岩矿测试》2002,21(4):304-306

采用电感耦合等离子体原子发射光谱法检测了黄铁矿中Cd,Co,Cu,Mn,Pb,Zn和Ni。用干扰系数校正法消除黄铁矿中铁对上述元素的干扰，采用HCl-HNO3体系溶解矿样，不需化学分离，直接测定。方法已应用于国家标准物质GBW07267的测定。结果与标准值相符，相对标准偏差（n=8)为1.5%-7.3%。  相似文献   

地幔流体及其成矿作用   总被引：8，自引：0，他引：8  

胡圣虹  胡兆初  刘勇胜  罗彦  林守麟  高山 《地学前缘》2001,8(4):0-0

高灵敏度、高精密度、低检出限、多元素同时检测并可提供同位素组成比值信息的等离子体质谱与高空间分辨率的紫外激光采样技术结合 ,可定量地测定单个流体包裹体中常、微量元素含量 ,为成矿流体的研究提供了一个新的研究手段。文中简要地介绍了激光剥蚀电感耦合等离子体质谱 (LA ICP MS)分析仪器的发展 ,结合实验室的研究工作 ,就激光剥蚀池的设计、单个流体包裹体的剥蚀方法、元素的分馏效率、定量校正技术及其在成矿成因物理化学机制研究中的应用等进行评述 ,并阐述单个流体包裹体元素组成的LA ICP MS分析技术存在的局限和发展趋势。  相似文献   

周口电信枢纽楼基坑降水设计方案技术经济分析     

郭精超 《水文地质工程地质》2001,28(2):42-44

通过分析两种不同的基坑降水设计方案，阐述了降水技术要求，并介绍周边建筑物不均匀沉降的防治措施。  相似文献   

反相流动注射催化光度法测定废水中的亚硝酸根   总被引：3，自引：0，他引：3  

訾言勤  孟国防 《岩矿测试》2001,20(2):108-110

采用反相流动注射技术与催化光度法相结合，用微机化流动注射分析仪准确控制反应时间，优化了实验条件，克服了催化光度法反应时间难以控制引起的方法精密度、准确度不高的弱点，拟定了测定痕量亚硝酸根的流动注射催化光度方法。分析速度第小时20次，NO2^- 质量浓度在0．00－2．00mg/L，回归方程斜率为0．155。方法直接测定电厂测水中NO2^-的结果与Griess法相符合，RSD＜5．0％（n=5）。  相似文献   

电感耦合等离子体质谱法同时测定地质样品中痕量碘溴硒砷的研究：Ⅱ.土壤及沉积物标准物质分析   总被引：11，自引：8，他引：11  

李冰  史世云等 《岩矿测试》2001,20(4):241-246

样品用碳酸钠和氧化锌混合熔剂半熔，热水提取，然后用强酸性阳离子交换树脂将阴离子形式存在的分析元素与溶液中大量钠、锌等阳离子分离，采用电感耦合等离子体质谱法直接同时测定溶液中的碘、溴、硒、砷。用0.07mol/L的氨水溶液清洗进样系统，有效减少了碘等元素的记忆效应和清洗时间。方法检出限（10σ，DF=100）溴、碘分别为0.15和0.028μg/g，砷、硒分别为0.04和0.004μg/g。用土壤和沉积物等地质标准物质分析验证了方法的准确度和精密度，绝大多数分析结果在标准值的允许误差范围之内。样品10次测定的RSD为0.8%～2.8%。  相似文献   

Naturally Enhanced Ion-Acoustic Spectra And Their Interpretation     

Francis Sedgemore-Schulthess  Jean-Pierre St. Maurice 《Surveys in Geophysics》2001,22(1):55-92

Incoherent scatter radars are designed to detect scatter from thermalfluctuations in the ionosphere. These fluctuations contain, among other things,features associated with ion-acoustic waves driven by random motions within theplasma. The resulting spectra are generally broad and noisy, but neverthelessthe technique can, through a detailed analysis of spectra, be used to measure arange of physical parameters in the Earth's upper atmosphere, and provides apowerful diagnostic in studies of magnetosphere-ionosphere coupling,thermosphere dynamics and the geospace environment in general. In recent yearsthere has been much interest in naturally occurring (as opposed to artificiallystimulated) enhanced ion-acoustic spectra seen in the auroral zone andcusp/cleft region. A study of the plasma instability processes that lead tosuch spectra will help us to better understand auroral particle acceleration,wave-particle and wave-wave interactions in the ionosphere, and theirassociation with magnetospheric processes. There is now a substantial body ofliterature documenting observations of enhanced ion-acoustic spectra, but thereremains controversy over generation mechanisms. We present a review ofliterature documenting observations of naturally enhanced ion-acoustic spectra,observed mainly along the geomagnetic field direction, along with a discussionof the theories put forward to explain such phenomena.  相似文献   

Strain and tilt changes measured during a water injection experiment at the Nojima Fault zone, Japan   总被引：2，自引：0，他引：2  

Kunio Fujimori  Hiroshi Ishii  Atsushi Mukai  Shigeru Nakao  Shigeo Matsumoto  Yasuhiro Hirata 《Island Arc》2001,10(3-4):228-234

Abstract In order to make geophysical and geological investigations of the Nojima Fault on Awaji Island, Japan, three boreholes measuring 1800 m, 800 m and 500 m deep were drilled into the fault zone. The fault is one of the seismic source faults of the 1995 Hyogo-ken Nanbu earthquake of M 7.2. A new multicomponent borehole instrument was installed at the bottom of the 800 m borehole and continuous observations of crustal strain and tilt have been made using this instrument since May 1996. A high-pressure water injection experiment within the 1800 m borehole was done in February and March 1997 to study the geophysical response, behavior, permeability, and other aspects of the fault zone. The injection site was located approximately 140 m horizontally and 800 m vertically from the instrument. Associated with the water injection, contraction of approximately 0.7 × 10⁻⁷ str (almost parallel to the fault) and tilt of approximately 1 × 10^-7 rad in the sense of upheaval toward the injection site were observed. In addition to these controlled experiments, the strainmeter and tiltmeter also recorded daily variations. We interpret strain and tilt changes to be related to groundwater discharge and increased ultra-micro seismicity induced by the injected water.  相似文献   

Routine Analyses of Trace Elements in Geological Samples using Flow Injection and Low Pressure On-Line Liquid Chromatography Coupled to ICP-MS: A Study of Geochemical Reference Materials BR, DR-N, UB-N, AN-G and GH   总被引：6，自引：0，他引：6  

Jean Carignan  Pascal Hild  Guy Mevelle  Jacques Morel  Delphine Yeghicheyan 《Geostandards and Geoanalytical Research》2001,25(2-3):187-198

  相似文献   

Trace Elements Analysis of Geological Samples by Laser Ablation Inductively Coupled Plasma Mass Spectrometry     

Luo Yan Liu Yongsheng Hu Shenghong Gao Shan Open Laboratory of Constitution  Interaction  Dynamics of the Crust Mantle System  Ministry of National Lands  Resources  China University of Geosciences  Wuhan Lin Shoulin Faculty of Material Sc 《中国地质大学学报(英文版)》2001,12(3)

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低地球轨道（LEO）的大型航天器充电     

操学俊  徐跃民 《地球物理学进展》1996,11(3):104-108

本文根据ＬＥＯ中等离子体温度低，密度高，德拜长度小的特点，采用薄鞘层近似，计算了离子收集电流；根据电流平衡方程，考虑表面二次电子发射，计算了大型航天器表面在沉降电子流辐照下的充电特性。  相似文献