钛（Ⅳ）的反相萃取柱色层新体系研究及应用     

谭龙华  唐祖光 《矿物岩石》1997,17(3):94-97

本文研究了以ｃＨＣｌ＝８ｍｏｌ·Ｌ－１盐酸为移动相，以聚四氟乙烯负载的钽试剂－ＣＨＣｌ３为固定相反相萃取层析钛（Ⅳ）的新体系，柱上层析的钛用ｃＨＣｌ＝３ｍｏｌ·Ｌ－１盐酸洗脱后经二安替比林甲烷光度法测定，不仅钛回收率可达１００％，并可使钛（Ⅳ）与多种离子分离。能用于矿物岩石类复杂样品及其他物质中钛的分离富集与测定，方法简便快速。  相似文献   

巨型钢结构抗震研究综述   总被引：1，自引：0，他引：1  

刘洁平  李小东  张令心 《世界地震工程》2004,20(4):42-46

介绍了巨型结构及其特点，着重总结、论述了巨型钢结构在分析方法和抗震研究方面的发展现状，指出了这种钢结构形式在抗震研究中存在的主要问题及今后进一步的研究方向。  相似文献   

煤矿开采在煤系砂岩中形成现代陷落柱的实例     

王革纯  刘金国 《中国煤田地质》2004,16(Z1):61-62

通 过 钱家 营井 田 203泥石 流 突发 事故 ,对 陷落 柱 的形 成机 理 作进 一步 的 研究 ,巷 道临 空 空间 、构 造破 碎带 、高压 地下 水 的存 在是 煤 系砂 岩地 层 中形 成现 代 陷落 柱的 主 要控 制因 素 。  相似文献   

顶空气相色谱法测定地层水中的苯系物   总被引：10，自引：2，他引：10  

饶竹 李松佟柏龄  吴淑琪李迎春 《岩矿测试》2004,23(2):97-101

利用极性聚乙二醇弹性石英毛细管柱分离苯系物，在线顶空气相色谱法测定地层水中的苯系物。讨论了色谱柱、载气压力、液相体积、顶空压力、顶空加热温度等因素对测定的影响。该方法实现了地层水中苯、甲苯、乙苯、对二甲苯、间二甲苯、邻二甲苯、异丙苯、苯乙烯等各组分的完全分离，方法的检出限在0．07—0．23μg／L，8次测定相对标准偏差在2．98％-4．91％，加标回收率为95．2％-104％。方法可用于地层水等液体样品中苯系物的测定。  相似文献   

非饱和土中镉离子传输模型参数反演   总被引：6，自引：0，他引：6       下载免费PDF全文

崔凯  李宝元  李兴斯  杨国伟 《水科学进展》2004,15(6):700-705

使用自行设计的的真空实验装置,采用一维实验室土柱实验方法在不同实验条件下进行了15组实验,并基于实验所得的穿透曲线,使用梯度正则化方法反演得到了镉离子在8种葡萄牙土样和1种比利时土样中相应的传输模型参数。同时通过数值模拟实验验证了梯度正则化方法的有效性和可靠性,进而证明所得结果是有效的。  相似文献   

Mitigation of liquefaction and associated ground deformations by stone columns   总被引：3，自引：0，他引：3  

Korhan Adalier  Ahmed Elgamal   《Engineering Geology》2004,72(3-4):275-291

Soil liquefaction and associated ground failures have been a major source of damage during the past earthquakes. The risk of liquefaction and associated ground deformation can be reduced by various ground-improvement methods including the stone column (gravel drain) technique. This paper presents the current state of the stone column technologies as a liquefaction countermeasure. A comprehensive review is provided aiming to: (a) identify key considerations for the general use of stone columns as a liquefaction countermeasure, (b) provide insights for design and construction, (c) compile the latest research developments, and (d) identify sources of useful information. Case histories of field applications and observed field performance are cited to portray different stone column applications and observed effectiveness. The paper identifies areas where more research is needed and includes recommendations for future research and development.  相似文献   

Analytical modeling on consolidation of stiffened deep mixed column-reinforced soft soil under embankment     

Zhen Zhang  Fengrui Rao  Guanbao Ye 《国际地质力学数值与分析法杂志》2020,44(1):137-158

Stiffened deep mixed (SDM) column is a new ground improvement technique to improve soft soil, which can be used to increase bearing capacity, reduce deformation, and enhance stability of soft soil. This technique has been successfully adopted to support the highway and railway embankments over soft soils in China and other countries. However, there have been limited investigations on its consolidation under embankment loading. This paper developed an analytical solution for the consolidation of embankment over soft soil with SDM column in which core pile is equal to or shorter than outer DM column. The consolidation problem was simplified as a consolidation of composite soil considering the load shear effect of core pile. The developed solution was verified by a comparison with the results computed by three-dimensional (3-D) finite element analysis. A parametric study based on the derived solution was conducted to investigate influence factors—length of core pile, diameter of core pile, diameter of SDM column, modulus of DM column, and permeability coefficient of DM column—on the consolidation behavior of SDM column-supported embankment over soft soil. The developed solution was applied to a case history of SDM column-supported embankment, and a good agreement was found between the predictions and the field measurements.  相似文献   

Effects of Column Diameter on Setting Behavior of Dredged Slurry in Sedimentation Experiments     

Yu-Feng Gao  Yuan Zhou  Da-yong Li 《Marine Georesources & Geotechnology》2016,34(5):431-439

This article investigates the influence of dimensions of a settling column on the settling mode and the settling rate. End conditions of the settling stage in the hindered settling were also analyzed. It was found that the settling mode in a column with a smaller diameter tends to be consolidation settling. The effect of a settling column wall decreases with increasing column diameter, and it can be ignored provided the column diameter is larger than 14.5 centimeters. For the difference in initial water content, the settling behavior of the slurry develops a different sensitivity to the diameter effect. The influence of column diameter reduces as the initial water content of the slurry becomes higher. It is suggested that the internal diameter of the column used in a sedimentation experiment should be 14.5 centimeters.  相似文献   

The terrestrial fauna of the Late Triassic Pant-y-ffynnon Quarry fissures,South Wales,UK and a new species of Clevosaurus (Lepidosauria: Rhynchocephalia)     

Emily Keeble  David I. Whiteside  Michael J. Benton 《Proceedings of the Geologists' Association. Geologists' Association》2018,129(2):99-119

Pant-y-ffynnon Quarry in South Wales yielded a rich cache of fossils in the early 1950s, including articulated specimens of new species (the small sauropodomorph dinosaur Pantydraco caducus and the crocodylomorph Terrestrisuchus gracilis), but no substantial study of the wider fauna of the Pant-y-ffynnon fissure systems has been published. Here, our overview of existing specimens, a few described but mostly undescribed, as well as freshly processed material, provides a comprehensive picture of the Pant-y-ffynnon palaeo-island of the Late Triassic. This was an island with a relatively impoverished fauna dominated by small clevosaurs (rhynchocephalians), including a new species, Clevosaurus cambrica, described here from a partially articulated specimen and isolated bones. The new species has a dental morphology that is intermediate between the Late Triassic Clevosaurus hudsoni, from Cromhall Quarry to the east, and the younger C. convallis from Pant Quarry to the west, suggesting adaptive radiation of clevosaurs in the palaeo-archipelago. The larger reptiles on the palaeo-island do not exceed 1.5?m in length, including a small carnivorous crocodylomorph, Terrestrisuchus, and a possible example of insular dwarfism in the basal dinosaur Pantydraco.  相似文献   

长江中下游六省大气甲烷柱浓度时空分布   总被引：2，自引：0，他引：2  

冯敏玉  张根  夏玲君  熊劦  李柏贞  孔萍  占明锦  张玉霞 《地球化学》2021,50(1):121-132

甲烷(CH4)是造成气候变暖的主要温室气体之一。为了了解长江中下游水稻种植区CH4浓度的分布情况,本次研究基于温室气体观测卫星(greenhouse gases observing satellite,GOSAT)和大气红外探测仪(atmospheric infrared sounder,AIRS)卫星反演的数据产品,对我国长江中下游六省大气CH4柱浓度的时空分布特征进行了研究。研究结果表明,由GOSAT反演的长江中下游六省大气CH4浓度呈逐年增长趋势,其年均浓度由2011年的1817×10^?9增长至2018年的1875×10^?9,高于东三省、华北平原和全国平均水平。区域平均年增长量为8.2×10^?9 a^?1。各省年际增长幅度略有差异,纬度偏低的江西、湖南和浙江三省大气CH4浓度高且增长量偏大,纬度偏高的湖北、安徽和江苏三省大气CH4浓度略低且增长量偏小。长江中下游六省大气CH4呈现较强的季节变化特征,湖北、湖南、江西和浙江峰值出现在9月,安徽、江苏峰值出现在8月。垂直方向上长江中下游六省CH4浓度随气压降低,浓度逐渐减小,呈现出明显的季节变化特征,近地面层GOSAT反演的最高值出现在夏季,最低值出现在春季;高层最高值出现在秋季,最低值出现在春季。AIRS反演的大气CH4浓度空间分布上北高南低,与GOSAT反演结果不一致,可能由于AIRS主要反映了对流层中层大气状况而GOSAT更多的反映了近地面层大气CH4的变化。其垂直方向上呈现高度越高,浓度越低,不同高度上秋季浓度均最高。  相似文献