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对某省5个产地21种烟叶样品用微波密闭消解,电感耦合等离子体直角加速时间飞行质谱(ICP-oaTOF-MS)测定砷、镉、汞、铅的含量。对称样量、微波消解及质谱检测参数、同位素及内标、方法准确性及可行性进行了研究,确定了最佳的实验条件。标准曲线的相关系数>0.9998,方法回收率为91.49%~106.25%,精密度(RSD)<2%,检出限为0.093~0.168μg/L。对在同一品种、同一部位、不同地区的烟叶样品进行测定,结果显示各地区样品中被测元素的含量存在较大差异,As为0.503~1.737 mg/kg,Pb为1.826~4.969 mg/kg,Cd为0.656~2.641 mg/kg,Hg为0.042~0.584 mg/kg;As、Hg含量差异较小,Pb、Cd含量差异较大。相比于其他分析方法,ICP-oaTOF-MS适合对浓度低至ng/L级超痕量组分的分析,具有简便快速、准确、灵敏度高、检出限低等优点,可用于烟叶重金属的检测及质量控制,对于判断烟株的丰缺情况、鉴别烟叶制品的品质具有一定的意义。 相似文献
84.
Analytic treatments of a particle encountering a collisionless shock have commonly been based on the assumption that the shock surface is quasi-planar with length scales larger than the particle gyroradius. Within this framework, the particle distribution function width is supposed to be conserved in any shock reflection process. It is well known, however, that the thermal energy associated with backstreaming ions upstream of Earth's bow shock is significantly larger than the incident solar wind thermal energy. In a previous study, we found that non-thermal features of ions reflected quasi-adiabatically can be accounted for by considering the effect of small, normally distributed fluctuations of the shock normal over short temporal or spatial scales. The strong dependence of the particle acceleration on shock geometry leads to an increase in the temperature and to a non-thermal tail. Here, we conduct a similar analysis to investigate the effects of small, normally distributed fluctuations in the shock normal direction for specularly reflected ions. This later mechanism is considered of first importance in the dissipation process occurring at quasi-perpendicular shocks. We have derived the probability distribution functions f(v∥) and f(v⊥) of ions issued from a specular reflection of incident solar wind in the presence of normal direction fluctuations. These distributions deviate weakly from a Maxwellian, in agreement with the observations. In particular, a qualitative agreement with the ion thermal energy is obtained for fluctuations of the normal orientation in the 5-8° range about the nominal direction. Also, we have found that the shock θBn has a weak effect on the shape of the distribution. While, not a strong determinant of the reflected distribution characteristics, the dynamical shock structure at ion scales cannot be ignored when accounting for the shock-accelerated particle thermal energy. 相似文献
85.
A series of wave‐flume experiments was conducted to closely look at characteristics of geometry and migration of wave‐generated ripples, with particular reference to the effect of velocity ‘hiatuses’ during which the near‐bed flow velocity becomes much smaller than the threshold of sediment movement. Three types of wave patterns were generated: two types for simulating waves with intervening velocity hiatuses; and regular waves for comparison purposes. In the former two types, two different wavelengths of water waves were generated alternately in the course of a wave test: the wave with a longer wavelength was set large enough to mobilize the bottom sediment, whereas the wave with a shorter wavelength was set too small to mobilize the sediment. The former two types were designed to be different in sequence of convexity and concavity of wave patterns. The sequence with the convex–concave longer wave and successive convex–concave shorter wave was described as a ‘zero‐up‐crossing’ wave pattern, and the inverse sequence was described as a ‘zero‐down‐crossing’ wave pattern. The ripples developed under oscillatory flow with intervening hiatuses manifested the following characteristics in geometry and migration. (i) The morphological characteristics of ripples, namely wavelength, height and the ripple steepness, are unaffected by the intervening hiatuses of velocity. (ii) The directions of ripple migration under the zero‐up‐crossing and zero‐down‐crossing wave patterns corresponded well with the directions of the flow immediately before onset of the hiatuses. (iii) The observation of sand particle movement on the ripple surface indicated that, under the zero‐up‐crossing waves, the velocity hiatus prevents the entrained sediment cloud from being thrown onshore, and thus the sediment grains thrown onshore are fewer than those thrown offshore. As a result of the sediment movement over one wave‐cycle, the net sediment transport is directed offshore under the zero‐up‐crossing wave pattern. (iv) The velocity of ripple migration was highly correlated with acceleration skewness. Under most of the zero‐up‐crossing (zero‐down‐crossing) wave patterns, flow acceleration skewed negative (positive) and ripples migrated offshore (onshore). 相似文献
86.
Discontinuous deformation analysis (DDA) is a numerical approach used to simulate the post-failure behavior of a blocky assembly. Three available algorithms incorporate seismic impacts into DDA simulations for earthquake-induced slope failure. The following methods are used: directly applying time-dependent accelerations to falling/sliding blocks (Method 1); adding time-dependent accelerations to base block (Method 2); and time-dependently constraining seismic displacements of the base block (Method 3). However, incorrect absolute movements of falling/sliding and base blocks were obtained using Method 1. Additionally, relative movements between falling/sliding blocks and the base block are opposite to those simulated by the other two algorithms—Methods 2 and 3. Since locating an earthquake-induced landslide before an earthquake is extremely difficult, the seismic movements of base rock are recorded. Method 1 applies recorded seismic data to sliding blocks in conflict with d’Alembert’s principle of mechanics. Additionally, in Method 2, when the computation time step must be longer than the time in seismic data, computational results reveal abnormal base block displacements due to the non-zero velocity recorded at the end time of seismic data in seismic DDA. In this study, a novel algorithm to diminish the velocity of the base rock in the seismic analysis is utilized to modify Method 2. Furthermore, this work confirms that DDA with the modified Methods 2 and 3 is a practical approach for earthquake-induced landslide simulations. 相似文献
87.
The prediction of near-shore morphology on the time scale of a storm event and the length scale of a few surf zone widths is an active area of research. Intense wave breaking drives offshore-directed currents (undertow) carrying sediment seawards, resulting in offshore bar migration. In contrast, higher order nonlinear properties, such as wave asymmetry (velocity skewness) and velocity asymmetry, are drivers for shoreward transport. These wave processes are included in phase-resolving models such as Boussinesq-type wave models (e.g., TRITON). Short-wave averaging in the wave model yields wave-induced forces (e.g., radiation stress gradients) and a wave asymmetry term. The wave-induced forces are used in a hydrostatic model (e.g., Delft3D flow module) to drive the current and undertow, resulting in a 3D velocity profile. The wave model and hydrostatic model are coupled online with a morphodynamic model (e.g., Delft3D morphology module). The latter computes, based on the 3D flow profile and the wave asymmetry term, the sediment transport and performs the bathymetry updates. The updates are transferred directly back to the hydrodynamic models. The coupling of the wave model TRITON and the Delft3D modules is validated by comparing against extensive laboratory data sets (LIP and Boers) and a field case (Duck94), and show a good performance for the hydrodynamics and a reasonable/fair performance for the bar movements. 相似文献
88.
This paper investigates the evolution of wave shape over a low-crested structure (LCS) using a 2-D RANS-VOF model. The model predictions of surface elevation and wave skewness and asymmetry are in good agreement with the recent measurements collected in a small scale wave channel at the University of Cantabria (UCA). The empirical formulae relating wave skewness and asymmetry to local Ursell number by Peng et al. (2009) have been extended to include the effect of wave reflection and the ramp in front of LCS and a wider range of Ursell number in the present study. In the presence of LCS, wave skewness decreases slightly above the seaward slope, then increases rapidly up to a maximum value above the structure crest, and decreases drastically above the leeward slope. Wave asymmetry decreases sharply above the seaward slope to a negative minimum value at the structure crest, and then increases rapidly to a positive value above the leeward slope. Our bispectral analysis indicates that sum interactions increase skewness and decrease asymmetry while difference interactions have opposite effects and that the former dominate above the seaward slope and on the structure crest but the latter dominate above the leeward slope of LCS. The observed wave shape evolution over a LCS can be attributed to the changes in the interplay of sum and difference interactions. We found that incident wave height and wave period, relative structure freeboard, structure crest width and structure porosity are the controlling factors for wave shape evolution over LCS. This study provides new insights on the role of wave skewness and asymmetry in the breakwaters stability and sediment transport around the structure and on the beaches behind it. 相似文献
89.
A simplified process-based approach for evaluating onshore sandbar migration is presented in this study. This approach takes wave-averaged parameters as input and computes sediment transport processes using a reconstructed intra-wave orbital velocity signal. The proposed method guarantees good predictive skills for multiple onshore sandbar migration cases without an ad hoc calibration for each scenario. The study differs from previous onshore sandbar migration models, where calibration and testing are performed on just one or few events, and model assessment for uncalibrated realizations is rarely carried out. The present version of the model only addresses onshore sandbar migrations. For the onshore migration cases analyzed, the model has better predictive skills than state-of-the-art morphodynamic models (XBeach and Unibest-TC). 相似文献
90.