碘－钒盐催化下合成的四溴邻苯二甲酸酐     

彭启强  夏宗凤  陈德昌 《中国海洋大学学报(自然科学版)》1994,(1)

报道一种新的有效催化剂－碘－钒盐和在一定条件下合成四溴邻苯二甲酸酐的方法。探讨催化剂的组成配比、用量、温度及废酸循环使用等因素对合成方法的影响。该催化剂的催化效果和常用的碘、碘－铁催化剂相同，适用于四溴邻苯二甲酸酐的合成。  相似文献   

中国东海的地震振幅合成     

Blake  RW 潘秋霞 《海洋地质信息通报》1996,(1):16-17

  相似文献   

N,N''''-双癸酰基乙二胺二乙酸钠的合成与性能研究     

毕彩丰  马少华  薛尧森  言亮亮 《中国海洋大学学报(自然科学版)》2006,36(3):473-476

以乙二胺和氯乙酸为原料,在低温常压下合成乙二胺二乙酸(EDDA),再以EDDA与癸酰氯反应制得N,N'-双癸酰基乙二胺二乙酸钠.采用核磁共振波谱确证了其结构;对产品的临界表面张力、起泡及稳泡能力、乳化能力及润湿渗透性能进行表征.在25℃时,N,N'-双癸酰基乙二胺二乙酸钠溶液的临界表面张力为28.1mN/m,临界胶束浓度为1.6×10-3 mol/L.显示出该产品有优良的起泡稳泡性能、乳化性能及润湿渗透性能,是1种优良的表面活性剂.  相似文献   

苜蓿转化细胞系核酸和蛋白质合成的研究     

谢经良  唐学玺 《中国海洋大学学报(自然科学版)》2003,33(2):249-252

以苜蓿转化细胞系和对照细胞系为材料 ,利用同位素标志方法研究了 3种大分子物质——DNA、RNA和蛋白质的合成动态。结果表明 ,与对照细胞系相比 ,转化细胞系的生长速度明显加快 ,DNA、RNA和蛋白质的合成旺盛 ,合成速度显著提高。同时 ,转化细胞系 DNA、RNA和蛋白质出现最大合成速度的时间均相应地延迟。  相似文献   

从海水中提取铀的发展现状   总被引：8，自引：0，他引：8  

金可勇  俞三传  高从阶 《海洋通报》2001,20(2):78-82

综述了几种常见海水中提取的方法和途径，并对其进行了分析和比较，对于具有开发价值的新方法和新作途径进行了较详细的讨论，对重要的吸附剂如肟胺类吸附剂的合成，优化等作为较详细的介绍，通过本文可以为从事该类工作的科技人员提供一个较全面的参考。  相似文献   

肝素酶Ⅰ对合成的肝素五糖的酶解作用及对其抗Xa因子活性的影响     

于广利  管华诗  Jawed Fareed 《中国海洋大学学报(自然科学版)》2001,31(4):529-535

研究肝素酶Ⅰ(来源于Flavobacterumheparinase，EC4.2.2.7)对人工合成的且含有与抗凝血酶Ⅲ特定结合位点的肝素五糖(SHP)的酶解作用，并对酶解作用的动力学进行研究。利用强阴离子高效液相色谱(SAX-HPLC)对酶解混合物进行分离，利用质谱(ESIMS)和核磁共振波谱(1H-NMR)技术对得到的二糖和三糖的结构进行确证。研究结果表明，这种被作为肝素反向试剂的肝素酶Ⅰ可水解人工所合成的肝素五糖，从而使之丧失抗Xa因子活性。  相似文献   

碳水化合物的组合合成     

王群  于广利 《中国海洋大学学报(自然科学版)》2001,31(1):45

碳水化合物的组合合成是一项新兴技术，该技术可以在短时间内合成大量用于进行生物活性筛选的寡糖及拟糖物。液相与固相合成技术可以极大地加快药物研究与开发进程。作者针对该技术在碳水化合物合成方面的研究进展情况进行讨论。  相似文献   

特定海域台风路径在中,低层环境场上的简明指征     

周学群  ？张翔 《海洋预报》1994,11(4):64-67

本文用合成分析方法，研究了台风（热带气旋）各种不同路径中，低层环境高度场和风场上的差异，提出了可用于业务科指征，经独立样本预报试验表明这些简明指征有较好的预报能力。对这些简明指征可用行业务预报的理论依据和局限性也作了粗略讨论。  相似文献   

Carbon and oxygen isotopic composition of car- bonate cements of different phases in terrigenous siliciclastic reservoirs and significance for their origin： A case study from sandstones of the Triassic Yanchang Formation, southwestern Ordos Basin, China     

Qi Wang  Xizhun Zhuo  Guojun Chen  Xiaoyan Li 《中国地球化学学报》2008,27(3):249-256

Early carbonate cements in the Yanchang Formation sandstones are composed mainly of calcite with relatively heavier carbon isotope （their δ^18O values range from -0.3‰- -0.1‰） and lighter oxygen isotope （their δ^18O values range from -22.1‰- -19.5‰）. Generally, they are closely related to the direct precipitation of oversaturated calcium carbonate from alkaline lake water. This kind of cementation plays an important role in enhancing the anti-compaction ability of sandstones, preserving intragranular volume and providing the mass basis for later disso- lution caused by acidic fluid flow to produce secondary porosity. Ferriferous calcites are characterized by relatively light carbon isotope with δ^13C values ranging from -8.02‰ to -3.23‰, and lighter oxygen isotope with δ^18O values ranging from -22.9‰ to -19.7‰, which is obviously related to the decarboxylation of organic matter during the late period of early diagenesis to the early period of late diagenesis. As the mid-late diagenetic products, ferriferous cal- cites in the study area are considered as the characteristic authigenic minerals for indicating large-scaled hydrocarbon influx and migration within the clastic reservoir. The late ankerite is relatively heavy in carbon isotope with δ^13C values ranging from -1.92‰ to -0.84‰, and shows a wide range of variations in oxygen isotopic composition, with δ^18O values ranging from -20.5‰ to -12.6‰. They are believed to have nothing to do with decarboxylation, but the previously formed marine carbonate rock fragments may serve as the chief carbon source for their precipitation, and the alkaline diagenetic environment at the mid-late stage would promote this process.  相似文献   

Helium-argon isotopic tracing for the Pb-Zn-Ag polymetallic ore deposits in the central-south segment of the Da Hinggan Ling Range     

Baode Wang  Shuyin Niu  Aiqun Sun  Huabin Hu  Yaming Liu  Lijun Guo  Shuo Wang 《中国地球化学学报》2008,27(3):235-241

In recent years big strides have been made in the exploration of ores in the central-south segment of the Da Hinggan Ling Range, though some debates still exist on the metallogenesis and sources of ore-forming materials. Pyrite and other sulfides in direct relation to the Pb-Zn-Ag ore deposits were chosen for the He and Ar isotopic analysis of ore-forming fluids, and the first He and Ar isotope data have been obtained from the study region. ^3He/^4He ratios in 14 samples collected from 7 mining districts are 2.17×10^-6-12.52×10^-6, averaging 6.86×10^-6 and their R/Ra ratios are 1.56-9.01 Ra, averaging 4.37 Ra. By projecting the data points onto the ^3He-^4He concentrations diagram, all the points fall near the mantle helium area. The calculated mantle-source helium ratios are within the range of 19.58%-76.96%, with an average of 49.52%. Argon isotopic characteristics are close to those of mantle source, indicating that the ore-forming material was transport upwards via the multi-stage evolution of mantle plume and concentrated as ores in the favorable loci of mantle branch structures.  相似文献