X射线粉晶衍射法在片麻岩鉴定与分类中的应用     

邵九龙  迟广成  史雨辰 《地质与资源》1992,29(5):490

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Geotechnical properties of a chemically stabilized soil from Malaysia with rice husk ash as an additive   总被引：1，自引：0，他引：1  

F. Haji Ali  A. Adnan  Chew Kam Choy 《Geotechnical and Geological Engineering》1992,10(2):117-134

Summary The stabilization of Malaysian soil by mixing with rice husk ash, a locally available waste material, to improve its engineering properties is described. Stabilizing agents, i.e. cement and lime, were added to produce the reaction products which are responsible for the enhancement of the engineering properties. Based on the strength development, it seems that lime is the more effective stabilizing agent. However, the cheap waste material can be used as partial replacement for the more expensive cement in the cement-treatment of the soil. A durability study was carried out to evaluate the effectiveness of this stabilization method.  相似文献   

累托石的结晶度研究   总被引：1，自引：0，他引：1  

张荣英 《矿物岩石》1993,13(3):62-67

本文用峰形分析法分析累托石的001X射线衍射峰特征;用001峰的半峰宽(W)测定累托石的结晶度(G),并令G=K/W=1为最大结晶度。文中测定了5个矿区10件累托石样品的结晶度,详细描述了不同结晶度累托石的X射线衍射、红外谱及差热曲线特征,讨论了研磨、热处理和改型对结晶度的影响,并阐明累托石的结晶度与造浆率之间呈正相关性。  相似文献   

743离子交换快速分离—等离子体光谱法同时测定十五个稀土元素   总被引：1，自引：0，他引：1  

吴锡凤  蒋铁珊 《铀矿地质》1993,(5)

本文研制了适用于地质样品中15个稀土元素分析的快速方法。样品经碱熔沉淀分离和743阳离子交换树脂分离富集将稀土元素制备成溶液用等离子体光谱法(ICP-AES)进行测量。方法检出限为0.002-0.3μg/g,当稀土元素含量为0.5-80,μg/g时,方法相对标准偏差为15％-2％。本方法经过多年的样品分析考验以及不断的改进和完善,证明方法简便快速,分析数据稳定可靠,能很好地满足地质样品中15个稀土分量测定的要求。  相似文献   

多波段类星体巡天观测     

何香涛  吴江华 《紫金山天文台台刊》1999,18(3):211-216

在发现类星体的方法中,最有效的４ 种方法是：颜色方法,无缝光谱方法,射电方法和Ｘ射线方法。覆盖的波段为：射电波段,光学波段和Ｘ 射线波段。我们将４ 种方法联合在一起,应用于４ 个ＵＫＳｃｈｍｉｄｔ 天区。其目的是尽量减少选择效应,建立更完备的类星体巡天样本。本工作从１００２ 天区入手。已完成了Ｘ 射线选和部分光学选的分光观测工作。发现了一颗Ｂ＝ １５ ．０ 的亮类星体和一个Ｓｅｙｆｅｒｔ 对,其强Ｘ 射线辐射,是迄今首次观测到的。  相似文献   

High-temperature X-ray investigation of natural columbites     

S. C.?Tarantino  M.?ZemaEmail author  M.?Pistorino  M. C.?Domeneghetti 《Physics and Chemistry of Minerals》2003,30(10):590-598

Structural investigations at high temperature were carried out on natural columbite samples across the join Fe(Nb_0.95Ta_0.05)₂O₆–Mn(Nb_0.95Ta_0.05)₂O₆. The samples were preliminarily annealed to attain the complete cation-ordered state and avoid the superimposition of the effects of cation ordering during high-temperature studies. Unit-cell parameters of three columbites with different X_Fe content were measured at regular intervals in the temperature range 25–900 °C using single-crystal X-ray diffraction techniques. The crystal structures of completely ordered ferrocolumbite and manganocolumbite were also refined from intensity data collected at room temperature, 300 and 600 °C. Structural thermal expansion coefficients show positive, linear expansion of a, b, c lattice constants and cell volume. In general, slightly higher expansion occurs along a and c directions. However, anisotropy decreases sharply with decreasing Fe content. Reversibility of thermal expansion in the investigated temperature range was checked by high-temperature diffraction studies under heating-up and cooling-down conditions. Impurities do not play an important role in thermal expansion of columbites; expansion coefficients measured on two crystals of the same sample characterized by different Ti content are in fact almost identical. Structural changes with temperature essentially affect bond lengths: volumes of both A and B octahedral sites increase linearly with temperature, whereas interpolyhedral geometrical parameters do not vary significantly.  相似文献   

X射线荧光光谱分析检出限问题的探讨与建议   总被引：12，自引：5，他引：7  

梁国立邓赛文  吴晓军甘露 《岩矿测试》2003,22(4):291-296

对有关X射线荧光光谱分析低含量元素的检出限问题进行了多方面的探讨。从检出限的定义及其定义下的相对标准偏差到各种不同测量、校准与校正方法的检出限及其相对应的相对标准偏差进行计算。提出了以定义检出限的相对标准偏差为基准,对各种测量方法计算出的检出限进行重新界定,从而确认一个具有可比性的、精度一致的检出限。同时还讨论了仪器与X光管固有杂质元素谱线对该元素检出限的影响;测量仪器、测量条件与测量时间对检出限的影响;不同岩性试样对检出限的影响;检出限与测定限等问题。  相似文献   

X-Ray Interferometry     

Webster Cash 《Experimental Astronomy》2003,16(2):91-136

For the astronomer, X-ray interferometry is the theory and practice of building dilute aperture telescopes for studying celestial X-ray sources. The short wavelengths and high surface brightness of X-ray sources will make the eventual scientific payoff very high, with direct imaging of the event horizons of black holes as the centerpiece. In this article, we review the history of X-ray interferometry and discuss the recent technical developments toward astronomical applications. We present several mission concepts and show they are achievable with todays technology.  相似文献   

低质量X射线双星的毫秒级准周期信号——最近的进展     

YU Wen-fei 《天文研究与技术》2003,(1):12-15

最近对低质量X射线双星中的千赫兹准周期振动的研究表明 ,是辐射压力 ,而不是盘和磁球的相互作用以及处于盘内边界的广义相对论效应在短时标的盘切断机制上起作用。本文给出了一些研究结果及讨论。  相似文献   

X-ray emission from accretion disks in active galactic nuclei     

V. F. Suleimanov  K. K. Ghosh  R. A. Austin  B. D. Ramsey 《Astronomy Letters》2002,28(11):745-754

We constructed a grid of relativistic models for standard high-relative-luminosity accretion α-disks around supermassive Kerr black holes (BHs) and computed X-ray spectra for their hot, effectively optically thin inner parts by taking into account general-relativity effects. They are known to be heated to high (～10⁶–10⁹ K) temperatures and to cool down through the Comptonization of intrinsic thermal radiation. Their spectra are power laws with an exponential cutoff at high energies; i.e., they have the same shape as those observed in active galactic nuclei (AGNs). Fitting the observed X-ray spectra of AGNs with computed spectra allowed us to estimate the fundamental parameters of BHs (their mass and Kerr parameter) and accretion disks (luminosity and inclination to the line of sight) in 28 AGNs. We show that the Kerr parameter for BHs in AGNs is close to unity and that the disk inclination correlates with the Seyfert type of AGN, in accordance with the unification model of activity. The estimated BH masses M_x are compared with the masses M_rev determined by the reverberation mapping technique. For AGNs with luminosities close to the Eddington limit, these masses agree and the model under consideration may be valid for them. For low-relative-luminosity AGNs, the differences in masses increase with decreasing relative luminosity and their X-ray emission cannot be explained by this model.  相似文献