微波消解-火焰原子吸收光谱法测定石英砂中的氧化钙和氧化镁     

鲁青庆 《岩矿测试》2005,24(4):314-316

采用微波消解-硼酸络合-火焰原子吸收光谱法测定石英砂中的氧化钙和氧化镁。样品在MK-Ⅲ型实验室微波炉上消解,消解压力为2.0 MPa、消解时间为5 m in,以硼酸络合消除氢氟酸的影响。方法已用于实际样品的测定,7次测定的相对标准偏差(RSD)小于5%,加标回收率为95.0%~104.2%。  相似文献   

Investigating the propagation mechanism of unmodelled systematic errors on coordinate time series estimated using least squares   总被引：6，自引：8，他引：6  

M. P. Stewart  N. T. Penna  D. D. Lichti 《Journal of Geodesy》2005,79(8):479-489

The propagation of unmodelled systematic errors into coordinate time series computed using least squares is investigated, to improve the understanding of unexplained signals and apparent noise in geodetic (especially GPS) coordinate time series. Such coordinate time series are invariably based on a functional model linearised using only zero and first-order terms of a (Taylor) series expansion about the approximate coordinates of the unknown point. The effect of such truncation errors is investigated through the derivation of a generalised systematic error model for the simple case of range observations from a single known reference point to a point which is assumed to be at rest by the least squares model but is in fact in motion. The systematic error function for a one pseudo-satellite two-dimensional case, designed to be as simple but as analogous to GPS positioning as possible, is quantified. It is shown that the combination of a moving reference point and unmodelled periodic displacement at the unknown point of interest, due to ocean tide loading, for example, results in an output coordinate time series containing many periodic terms when only zero and first-order expansion terms are used in the linearisation of the functional model. The amplitude, phase and period of these terms is dependent on the input amplitude, the locations of the unknown point and reference point, and the period of the reference point's motion. The dominant output signals that arise due to truncation errors match those found in coordinate time series obtained from both simulated data and real three-dimensional GPS data.  相似文献   

大气边界层湍流温度序列的信息熵分析   总被引：2，自引：0，他引：2  

汪景烨  付遵涛  张霖  刘式达 《高原气象》2005,24(1):38-42

利用大气边界层内近地面的大气湍流温度时间序列，运用功率谱分析、信息熵分析等方法，分析了大气边界层内近地面的大气湍流特点，并对稳定层和不稳定层的大气湍流进行了对比。结果表明，信息熵和功率谱指数是区别稳定层结和不稳定层结大气边界层湍流特征的指标，对造成两者之间的差别做出了对应的解释。  相似文献   

黑龙江气候变暖的时空变化特征   总被引：15，自引：0，他引：15  

潘华盛  张桂华 《黑龙江气象》2002,(3):3-6,11

进入80年代以来，黑龙江气温明显变暖，近120年来年平均气温上升1.4℃，春季次之，气温突变在1990年前后，从年、各季平均气温变化趋势与全国北半球及全球气温变化进行比较，年及冬季我国增暖中心在黑龙江，春季增暖中心在内蒙古北部及黑龙江省；夏秋增暖不明显，但仍有上升趋势，近50年来，50～70年代黑龙江省及全国各大区域普遍增暖不明显，80年代开始黑龙江省增暖明显，三北地区次之，90年代黑龙江增暖更加明显，而全国及其他区域上升已达到80年代北方增温幅度，这里从黑龙江变暖的事实，突变时间，与全球、北半球、全国区域的气温及雪盖海温变化关系来揭示黑龙江气候变化的时空特点。  相似文献   

显式自由表面模型时间分裂格式的一个积分方案   总被引：5，自引：0，他引：5  

Zhou Weidong 《大气科学进展》2002,19(2):255-265

讨论了有关显式自由表面模型的时间分裂格式中的分裂误差。在传统的积分方案中，由于采用蛙跳格式，斜压动量方程具有三层的时间离散结构，但是，正压动量方程在相应的时间层上只有二层的离散结构。因此，正压方程与斜压方程的时间离散结构是不相容的。分析结果表明，这是导致分裂误差的原因。本提出一种能保持时间离散结构相容的正压和斜压方程的时间积分方案。该积分方案的分裂误差很小因此特别适合于需要长期积分的气候研究。该方案在北太平洋的一个自由表面模型中得到了应用。  相似文献   

Electrical aerosol spectrometer of Tartu University     

H. Tammet  A. Mirme  E. Tamm   《Atmospheric Research》2002,62(3-4)

The electrical aerosol spectrometer (EAS) of the parallel measuring principle at Tartu University is an efficient instrument for rapid measurement of the unstable size spectrum of aerosol particles. The measuring range from 10 nm to 10 μm is achieved by simultaneously using a pair of differential mobility analyzers with two different particle chargers. The particle spectrum is calculated and measurement errors are estimated in real time by using a least-squares method. Experimental calibration ensures reliability of measurement. The instrument is well suited for continuous monitoring of atmospheric aerosol.  相似文献   

Study on effects of damping in laminated rubber bearings on seismic responses for a ⅛ scale isolated test structure     

Bong Yoo  Yang‐Hann Kim 《地震工程与结构动力学》2002,31(10):1777-1792

The effects of damping in various laminated rubber bearings (LRB) on the seismic response of a ?‐scale isolated test structure are investigated by shaking table tests and seismic response analyses. A series of shaking table tests of the structure were performed for a fixed base design and for a base isolation design. Two different types of LRB were used: natural rubber bearings (NRB) and lead rubber bearings (LLRB). Three different designs for the LLRB were tested; each design had a different diameter of lead plug, and thus, different damping values. Artificial time histories of peak ground acceleration 0.4g were used in both the tests and the analyses. In both shaking table tests and analyses, as expected, the acceleration responses of the seismically isolated test structure were considerably reduced. However, the shear displacement at the isolators was increased. To reduce the shear displacement in the isolators, the diameter of the lead plug in the LLRB had to be enlarged to increase isolator damping by more than 24%. This caused the isolator stiffness to increase, and resulted in amplifying the floor acceleration response spectra of the isolated test structure in the higher frequency ranges with a monotonic reduction of isolator shear displacement. Copyright © 2002 John Wiley & Sons, Ltd.  相似文献   

Numerical Analysis of Space–Time Finite Element Formulations for Miscible Displacements     

Rigoberto G. Sanabria Castro  Sandra M. C. Malta  Abimael F. D. Loula  Luiz Landau 《Computational Geosciences》2002,5(4):301-330

A finite element formulation is proposed to approximate a nonlinear system of partial differential equations, composed by an elliptic subsystem for the pressure–velocity and a transport equation (convection–diffusion) for the concentration, which models the incompressible miscible displacement of one fluid by another in a rigid porous media. The pressure is approximated by the classical Galerkin method and the velocity is calculated by a post-processing technique. Then, the concentration is obtained by a Galerkin/least-squares space–time (GLS/ST) finite element method. A numerical analysis is developed for the concentration approximation. Then, stability, convergence and numerical results are presented confirming the a priori error estimates.  相似文献   

厚层覆盖区综合物化探方法找金试验研究——以广西兴安金石金矿为例     

胡云沪  罗先熔  王桂琴  杜建波  张小路 《矿产与地质》2002,(5)

在兴安金石金矿外围 4号分散流异常区 ,通过地电化学提取金测量法 ,查明测区存在 5个走向规模小于 5 0 m的金异常区 ,W( Au) 最大值为 72 .4× 10 - 9,高出背景值十几倍 ,并藉综合土壤吸附汞测量 ,高精度磁测和激发极化法等多种物化探方法来确定这些异常区的地质、地球化学和地球物理特征 ,提出金矿成矿的有利部位在金的地电提取高异常区、高汞量异常区、高磁性异常区、低视电阻率异常区和中等视极化率异常区的“三高一低一中”的找矿模式。确定测区的北北东角 (右下角 )一带具备有利的金矿成矿条件  相似文献   

震源时间函数与震源破裂过程   总被引：2，自引：0，他引：2  

许力生  陈运泰 《地震地磁观测与研究》2002,23(6):1-8

简要介绍了现代数字地震学的两个重要概念。一个是震源时间函数，另一个是地震震源的时空破裂过程。首先，从地震断层位移表示定量出发，介绍震源时间函数和震源破裂过程的基本概念。然后，分别介绍两种从远场地震记录中提取震源时间函数和获取有限断层面上时空破裂过程图像的反演方法。  相似文献