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激光剥蚀电感耦合等离子体质谱分析石笋样品中多元素比值及45种元素含量 总被引:1,自引:0,他引:1
石笋样品的微量元素含量及Mg/Ca、Sr/Ca比值为高分辨的古气候重建提供重要指标。针对现有溶液分析技术易混合多个石笋微层、误差大的缺点,本文利用激光剥蚀电感耦合等离子体质谱技术(LA-ICP-MS)原位线扫描和点剥蚀方式对比分析了石笋生长轴方向的Mg/Ca和Sr/Ca空间分布趋势,研究表明二者均展现出显著的周期性变化特征,且周期性变化一致,其中40 μm束斑线扫描更具有稳定性强、分辨率高、快速简便的优点。通过探讨碳酸盐标准样品MASC-3与玻璃标准样品NIST 610、NIST 612、KL2G、ATHO-G的相对灵敏度系数关系和元素分馏行为,确定基体效应是造成相对灵敏度系数变化的主要原因。同时建立了以MASC-3、NIST 610和NIST 612多外标结合内标Ca归一定量分析石笋中45种元素方法,针对石笋碳酸盐样品,将主量元素Ca、Mg变形为碳酸盐形式,与其他元素加和归一,不仅改变了国内外研究中需要预先采用其他分析技术来测定内标元素含量的计算方法,而且有效地避免了C元素无法准确检测的问题,能够实现与Ca内标法校正结果的吻合。 相似文献
105.
The regional climate correlation within the Northern Hemisphere in the cold/dry mid-Younger Dryas event (YD) remains elusive. A key to unraveling this issue is sufficient knowledge of the detailed climate variability at the low latitudes. Here we present a high-resolution (3-yr) δ18O record of an annually laminated stalagmite from central China that reveals a detailed Asian monsoon (AM) history from 13.36 to 10.99 ka. The YD in this record is expressed as three phases, characterized by gradual onsets but rapid ends. During the mid-YD, the AM variability exhibited an increasing trend superimposed by three centennial oscillations, well-correlated to changes in Greenland temperatures. These warming/wetting fluctuations show a periodicity of ~ 200 yr, generally in agreement with centennial changes in cosmogenic nuclides indicated by the 10Be flux from the Greenland ice. This relationship implies that centennial-scale climate changes during the mid-YD are probably caused by solar output and rapidly transported over broad regions through atmosphere reorganization. 相似文献
106.
Emile Rod 《Australian Journal of Earth Sciences》2013,60(1-2):89-95
The structural deformation which produced more than 80 Jura‐type folds each of an axial length exceeding 1 km, in the Redbank Area, N.T., involved only a 360‐to 400‐m thick blanket of sediments. This thin skin of sediments and volcanic rocks, belonging to the Lower Proterozoic Tawallah Group, consists from bottom to top of the Wollogorang Formation, Gold Creek Volcanics, and Pungalina beds. Folding did not involve the underlying Settlement Creek Volcanics or Aquarium Formation. It is postulated that the cause of this detachment and shearing off along the bottom of the thin blanket of sediments is the infiltration of carbonated, K‐rich hydrothermal fluids under high pressure. This occurred during a period of igneous activity related to a postulated deep‐seated alkaline magma thought to be responsible for the many breccia pipes in the area. Thus the folds result from a décollement triggered by high fluid pressure, and from the accompanying gravity gliding and gravitational induced deformation of the thin skin of sediments along a gentle slope. 相似文献
107.
对于已进入开发中后期的碳酸盐岩缝洞型油气藏,进行缝洞单元精细研究非常重要。盲目部署加密井,很容易导致因为所在单元的储量已被动用而失利。本文采用的碳酸盐岩缝洞单元多学科综合划分方法是:在有井控制的地区,首先分析井间连通性,然后结合生产动态、常规解析试井、流体性质、数值试井等多学科资料确定缝洞单元边界;在无井控制的地区,影响连通性最重要的主控因素是储层本身的相互连通性,其次才是断裂和裂缝,这时可在连通性约束下进行储层和裂缝预测,并以此为主要依据确定缝洞单元边界。对塔里木盆地轮古油气田轮古11井区划分出80个缝洞单元,其中有55个为储量未动用单元(潜力单元),并部署了一些加密井,已钻的XW1井获得了成功,投产初期日产油95t,不含水。 相似文献
108.
Little work has been undertaken on combined dating of sedimentary quartz grains using electron spin resonance (ESR) and optically stimulated luminescence (OSL) techniques in Australia. This study aims to assess the suitability of a combined ESR and OSL dating approach for establishing improved chronologies of Middle-Late Pleistocene deposits within the Naracoorte Cave Complex (NCC), South Australia. Here, we apply ESR and OSL dating in tandem to a series of samples collected from three different NCC sites: Whale Bone, Specimen and Alexandra cave. ESR quartz dating focuses on the multi-centre (MC) approach, which involves comparative evaluations of Al and Ti centre signals, while paired luminescence dating focuses on single-grain OSL analysis and includes examination of multi-grain averaging effects. The comparative ESR-OSL dating results exhibit broad agreement for deposits spanning 50–150 thousand years, with either the Ti–H or Al centre ages overlapping with paired OSL ages at 2σ in nearly all cases. MC ESR evaluations (Al v Ti–Li v Ti–H age assessments) indicate incomplete resetting of the bleachable Al centre signal for a small number of samples. Two-thirds of samples exhibit Ti–Li ages that are significantly older than corresponding Al centre ages, which is unexpected from a bleaching kinetics perspective and may indicate a broader reliability issue for Ti–Li palaeodose evaluation with these particular samples. Our findings: (i) support the applicability of both palaeodosimetric dating methods in this depositional setting; (ii) highlight the merits of applying combined ESR-OSL analyses in tandem, and; (iii) provide one of the first reliable evaluations of quartz ESR MC dating for samples with natural dose ranges as low as only a few tens of Gy. These results show that the Whale Bone, Specimen and Alexandra cave sites are temporally related and can be used to derive multi-site reconstructions of faunal assemblages and palaeoenvironmental history. 相似文献
109.
James U.L. Baldini Frank McDermott Dirk L. Hoffmann David A. Richards Nicholas Clipson 《Earth and Planetary Science Letters》2008,272(1-2):118-129
Cave air PCO2 at two Irish sites varied dramatically on daily to seasonal timescales, potentially affecting the timing of calcite deposition and consequently climate proxy records derived from stalagmites collected at the same sites. Temperature-dependent biochemical processes in the soil control CO2 production, resulting in high summer PCO2 values and low winter values at both sites. Large Large-amplitude, high-frequency variations superimposed on this seasonal cycle reflect cave air circulation. Here we model stalagmite growth rates, which are controlled partly by CO2 degassing rates from drip water, by considering both the seasonal and high-frequency cave air PCO2 variations. Modeled hourly growth rates for stalagmite CC-Bil from Crag Cave in SW Ireland reach maxima in late December (0.063 μm h− 1) and minima in late June/early July (0.033 μm h− 1). For well-mixed ‘diffuse flow’ cave drips such as those that feed CC-Bil, high summer cave air PCO2 depresses summer calcite deposition, while low winter PCO2 promotes degassing and enhances deposition rates. In stalagmites fed by well-mixed drips lacking seasonal variations in δ18O, integrated annual stalagmite calcite δ18O is unaffected; however, seasonality in cave air PCO2 may influence non-conservative geochemical climate proxies (e.g., δ13C, Sr/Ca). Stalagmites fed by ‘seasonal’ drips whose hydrochemical properties vary in response to seasonality may have higher growth rates in summer because soil air PCO2 may increase relative to cave air PCO2 due to higher soil temperatures. This in turn may bias stalagmite calcite δ18O records towards isotopically heavier summer drip water δ18O values, resulting in elevated calcite δ18O values compared to the ‘equilibrium’ values predicted by calcite–water isotope fractionation equations. Interpretations of stalagmite-based paleoclimate proxies should therefore consider the consequences of cave air PCO2 variability and the resulting intra-annual variability in calcite deposition rates. 相似文献
110.
Temporal and spatial variations in the discharge and dissolved organic carbon of drip waters in Beijing Shihua Cave,China 总被引:1,自引:0,他引:1
To detect the causal relationship between cave drip waters and stalagmite laminae, which have been used as a climate change proxy, three drip sites in Beijing Shihua Cave were monitored for discharge and dissolved organic carbon (DOC). Drip discharges and DOC were determined at 0 to 14‐day intervals over the period 2004–2006. Drip discharges show two types of response to surface precipitation variations: (1) a rapid response; and (2) a time‐lagged response. Intra‐annual variability in drip discharge is significantly higher than inter‐annual variability. The content of DOC in all drip waters varies inter‐ and intra‐annually and has good correlation with drip water discharge at the rapid response sites. High DOC was observed in July and August in the three years observed. The flushing of soil organic matter is dependent upon the intensity of rain events. The DOC content of drip water increases sharply above a threshold rainfall intensity (>50 mm d?1) and shows several pulses corresponding with intense rain events (>25 mm d?1). The DOC content was lower and less variable during the dry period than during the rainy period. The shape of DOC peak also varies from year to year as it is influenced by the intensity and frequency of rainfall. The different drip sites show marked differences in DOC response, which are dominated by hydrological behaviour linked to the recharge of the soil and karst micro‐fissure/porosity network. The results explain why not all stalagmite laminae are consistent with climate changes and suggest that the structure of the rainy season events could be preserved in speleothems. Copyright © 2008 John Wiley & Sons, Ltd. 相似文献