M17树脂对岩石中痕量硒碲的分离富集研究及应用     

林猷璧  朱玉伦 《岩矿测试》1993,12(2):81-84

M_(17)树脂在>6mol/L的HCl介质中能同时吸附Se和Te,Se和Te可用水和丙酮分别洗脱,也可用丙酮同时洗脱。从而建立了两个新的Se、Te分离富集体系,使原子荧光测定达到纳克量级。  相似文献   

锰矿石中硅酸锰的分离和测定方法对比     

耿学道  李维翰 《岩矿测试》1994,13(1):49-51

文章对几种分离测量硅酸锰的方法进行了对比。指出硅酸锰测定失真的缘由。选择了浸取分离伴生铁矿物的浸取剂及浸取分离条件。  相似文献   

P507负载泡塑反相色层富集岩石中的稀土元素   总被引：4，自引：0，他引：4  

漆亮 《岩矿测试》1994,13(1):52-55

研究了Ｐ５０７负载泡塑萃取柱色谱分离富集稀土元素的条件，并与Ｐ５０７萃淋树脂柱进行了对比；拟定了Ｐ５０７负载泡塑反相色属富集岩石中稀土元素的方法。在ｐＨ２．５介质中ＲＥＥ上柱率９８％，用５０ｍｌ２．５ｍｏｌ／ＬＨＮＯ３作洗脱液，ＲＥＥ总回收率达９６．１％，干扰测定的Ｔｈ，Ｕ，Ｔｉ，Ｚｒ，Ｈｆ等均被除法。方法用于标样分析验证，结果与推荐值相符。  相似文献   

M17树脂分离富集原子荧光测定岩矿中痕量碲   总被引：4，自引：1，他引：4  

林猷璧  朱玉伦 《岩矿测试》1991,10(4):283-286

本文研究了不同种类树脂对Te的吸附能力,提出了在3mol/L HCl介质中,用M_(17)二甲胺树脂吸附,然后用水洗脱的新途径,使Te有效且无污染地得到分离和富集,实现了原子荧光测定地质试样中ppb级痕量Te。经地矿部标准参考样GSR7-12考察,分析结果与推荐值相符。  相似文献   

Three　dimensional　velocity　structure　beneath　the　Kunming　Telemetered　Seismic　Network     

王椿镛  王溪莉  颜其中 《地震学报(英文版)》1994,(2)

Ｔｈｒｅｅ　ｄｉｍｅｎｓｉｏｎａｌ　ｖｅｌｏｃｉｔｙ　ｓｔｒｕｃｔｕｒｅ　ｂｅｎｅａｔｈ　ｔｈｅ　Ｋｕｎｍｉｎｇ　Ｔｅｌｅｍｅｔｅｒｅｄ　Ｓｅｉｓｍｉｃ　Ｎｅｔｗｏｒｋ（王椿镛）（王溪莉）（颜其中）Ｔｈｒｅｅｄｉｍｅｎｓｉｏｎａｌｖｅｌｏｃｉｔｙｓｔ...  相似文献   

光石沟花岗伟晶岩型铀矿小型重选试验及技术经济初步评价     

孙志富  冯明月 《铀矿地质》1994,10(6):334-342

光石沟花岗伟晶岩型铀矿小型重选试验为工业利用花岗伟晶岩铀矿床的矿石，特别是低品位矿石方面开拓了新的途径。试验证明重选法在回收花岗伟晶岩型铀矿床矿石的铀以及回收副产品和防止环境污染等方面均优于湿法冶炼，并有好的经济效益。  相似文献   

在地面三角网中布设卫星观测站的最低精度要求     

周忠谟 《武汉大学学报(信息科学版)》1986,(3)

本文从地面三角网和卫星同联合平差的原理出发,讨论了对卫星网的最低精度要求。指出,为改善地面三角网而布设卫星网时,卫星观测站的最低精度主要决定于以下因素: ——地面三角网的精度; ——对地面三角网精度改善程度的要求; 一卫星观测站之间的距离。这里通过模拟计算对卫星网的最低精度要求与上列因素之间的关系作了数字分析,并建立了估算卫星网最低精度的数学模型。预期,在一般情况下,该模型的估算误差将不会超过10％。  相似文献   

TBP－（X－5）反相色谱分离m－NPF分光光度法测定铀     

周发连  罗志远 《华东地质学院学报》1995,(1)

本文研究了以磷酸三丁酯为固定相，大孔聚乙烯苯（Ｘ－５型）为担体的浸渍树脂、垂直型反相色谱柱，对铀分离富集的基本性能，以及铀（Ⅳ）－间硝基苯基萤光酮（ｍ－ＮＰＦ）一氨三乙酸（ＮＴＡ）－吐温－８０显色体系的反应条件，提出了ＴＢＰ（Ｘ－５）分离，ｍ－ＮＰＦ－ＮＴＡ－吐温－８０光度法测定铀，经标准样品验证，结果满意。  相似文献   

Rainfall-runoff forecasting methods,old and new     

M. Karlsson  S. Yakowitz 《Stochastic Environmental Research and Risk Assessment (SERRA)》1987,1(4):303-318

Here we review the main thrusts of rainfall-runoff modelling with an eye toward the advantageous use of the massive date sets being accumulated and the modern computers capable of dealing effectively with such sets.More than a tutorial, this study is aimed at providing a unifying structure for analyzing available techniques. The closing section draws attention to the existence of an alternative methodology.  相似文献   

Efficiency of heavy liquid separation to concentrate magnetic particles     

Christine Franke  Thomas Frederichs  Mark J. Dekkers 《Geophysical Journal International》2007,170(3):1053-1066

Low-temperature rock magnetic measurements have distinct diagnostic value. However, in most bulk marine sediments the concentration of ferrimagnetic and antiferromagnetic minerals is extremely low, so even sensitive instrumentation often responds to the paramagnetic contribution of the silicate matrix in the residual field of the magnetometer. Analysis of magnetic extracts is usually performed to solve the problems raised by low magnetic concentrations. Additionally magnetic extracts can be used for several other analyses, for example electron microscopy or X-ray diffraction. The magnetic extraction technique is generally sufficient for sediments dominated by magnetite. In this study however, we show that high-coercivity components are rather underrepresented in magnetic extracts of sediments with a more complex magnetic mineralogy. We test heavy liquid separation, using hydrophilic sodium polytungstenate solution Na₆[H₂W₁₂O₄₀], to demonstrate the efficiencies of both concentration techniques. Low-temperature cycling of zero-field-cooled, field-cooled and saturation isothermal remanent magnetization acquired at room temperature was performed on dry bulk sediments, magnetic extracts, and heavy liquid separates of clay-rich pelagic sediments originating from the Equatorial Atlantic. The results of the thermomagnetic measurements clarify that magnetic extraction favours components with high spontaneous magnetization, such as magnetite and titanomagnetite. The heavy liquid separation is unbiased with respect to high- and low-coercive minerals, thus it represents the entire magnetic assemblage.  相似文献