减压微色谱柱在矿石分析中的应用研究——P350萃淋树脂分离光度法测定痕量金     

龚治湘  宋金如  罗静 《岩矿测试》1993,(3)

研究了甲基膦酸二甲庚酯(P350)减压微色谱柱对Au的萃取性能。减压条件下,2mol/LHCI或浓度<25％的王水介质中的Au被萃取在P350(Φ3mm)微色谱柱上,再用小体积的1％Na_2SO_3定量洗脱。与常规柱相比,减压微色谱柱分离具有柱效高、洗脱体积小、速度快、节省大量试剂等优点。经标准样品验证,方法可用于含Au 0.025～200g/t地质样品的分析。  相似文献   

FIVE RED TIDE SPECIES IN GENUS PROROCENTRUM INCLUDING THE DESCRIPTION OF PROROCENTRUM DONGHAIENSE LU SP. NOV. FROM THE EAST CHINA SEA   总被引：22，自引：0，他引：22  

陆斗定  JeanetteGoebel 《中国海洋湖沼学报》2001,19(4):337-344

A new planktonic dinoflagellate, Prorocentrum donghaiense I_a sp. nov., is described in the present paper. The water sample was collected from the Changjiang Estuary, the East China Sea. The species identification is based on shape, size, surface micro-morphology, ornamentation of thecal plates and the architecture of the pel‘iflagellar area and the intercalary bands as seen by fight and scanning electron microscope. Prorocentrum donghaiense Lu sp. nov. is compared with other prorocentrum species with respect to morphological characteristics and bloom behavior. It is not known whether Prorocentrum donghaiense Lu sp. nov produces phycotoxins like some other Prorocentrum species. Four other red tide species in the family Prorocentraceae (Dinophyceae), namely P. balticum, P. minimum, P.micans, P. triestinum, were examined and identified by light and scanning electron microscope. They have been recorded as bloom-forming species. Some aggregates of Prorocentrum are observed at the end of blooms. An event of strong discoloration caused by P. donghaiense could be detected by satellite sensor in the East China Sea in the late spring, of 1995.  相似文献   

陆相汕藏中砂泥岩互层时移地震遮掩效应及其对时移地震资料解释的影响     

王大伟  刘震  赵伟  夏庆龙 《现代地质》2006,20(4):635-640

从差异波形特征的角度出发,分析时移地震差异波形特征与砂泥岩互层油藏中油层速度变化的关系.通过建立由5层地层组成的楔形地质模型,运用褶积公式及时移地震求差公式,得到泥岩速度为2 400 m/s和砂岩速度为2 700 m/s条件下,互层中砂岩速度变化±150 m/s的时移地震响应.研究结果表明砂泥岩互层的差异波形是一个多峰复合波,泥岩夹层的厚度是决定差异波形特征的一个主要因素,并且存在一个临界值,即四分之一主波长;如果泥岩夹层的厚度小于这一临界值,就会发生遮掩效应,即顶部油层的时移地震响应可以掩盖中、下部油层的时移地震响应.  相似文献   

万丰路桥大吨位矩形截面桩成孔施工技术     

王宏坤 《探矿工程》2007,34(2):10-12

针对在卵石及基岩地层中桩孔施工时成孔难、渗漏大的问题，以液压抓斗为成孔设备，采用合理的机械结构、钻进方法、泥浆配方进行矩形截面桩的施工。  相似文献   

利用赤泥制备钙铝榴石微晶玻璃的实验研究     

邢净  李金洪  张凯 《矿物岩石地球化学通报》2007,26(2):181-184

在1300℃下将赤泥和石英砂熔制成基础玻璃,经粉磨、筛选后,通过二次热处理工艺获得了以钙铝榴石为主晶相的微晶玻璃。采用XRD和SEM等研究赤泥和微晶玻璃后表明,赤泥主要由方解石和霰石等钙质成分组成;热处理温度对微晶玻璃性能和钙铝榴石晶体结构的影响较大。优化的制备条件为:核化900℃,1h,晶化1105℃,2h,该条件下所得的微晶玻璃晶相含量较高,晶体发育完整,性能良好,相应的体积密度为2.79g/cm3,显微硬度为6.52。  相似文献   

依兰矿区钻探施工泥浆选型的研究     

魏臣 《中国煤田地质》2007,19(2):72-74

依兰矿区第三系上部的砂泥岩段,因泥岩的水敏水化作用及粗砂岩易坍塌等原因造成,区内钻孔孔壁极不稳定,经常发生粘卡钻具事故。为抑制泥岩的水敏水化,阻止泥岩水化和井壁岩石剥落,增强其防塌能力,在选择腐植酸钾做主剂的基础上选择CMC作降失水增粘剂,选择分子量为300万～500万、水解度30%的聚丙烯酰胺(PAM)作絮凝剂,以加速岩屑沉降,控制固相侵入,降低失水。在钻遇半胶结泥岩时,为防止缩径、坍塌,采用在泥浆中加入重晶石粉,把泥浆比重调整到1.15～1.20g/cm~3,利用泥浆液柱压力控制泥岩缩径和孔壁坍塌。通过实验及现场应用,为该区选择的KHM-CMC-PAM高聚物泥浆配方,能有效地防止水敏性易塌地层的粘卡钻事故,具有护壁防塌、提高钻效等技术效果。  相似文献   

武乡区块山西组泥页岩孔隙结构及分形特征研究     

曹磊  郭英海 《岩石矿物学杂志》2020,39(3):283-290

沁水盆地东部煤系伴生泥页岩广泛发育,页岩气资源潜力大,开展该区泥页岩孔隙结构特征的研究对页岩含气性评价及实现煤层气、页岩气合探共采具有重要意义。本文以盆地内武乡区块Y井二叠系山西组泥页岩为研究对象,通过XRD、高压压汞和低温液氮吸附等实验手段对泥页岩孔隙结构特征及分形特征进行了研究。结果表明,Y井山西组泥页岩的矿物组成以黏土矿物和石英为主;泥页岩中小于50 nm的孔隙大量发育,结构形态上以狭缝平板型孔隙和"细瓶颈"孔隙为主;泥页岩样品吸附曲线呈倒S型,属于Brunauer分类方案中的Ⅱ型曲线,其脱附曲线属于IUPAC分类方案中的H2型(兼具H1型及H3型),属De Boer分类方案中的B型(兼具E型及C型); Y井山西组泥页岩分形维数接近3,非均质性较强,矿物成分、总孔体积、平均孔径和TOC含量是影响泥页岩分形维数的重要因素。  相似文献   

有益微生物改善养殖生态研究──Ⅰ.复合微生物分解有机底泥及对鱼类的促生长效应   总被引：3，自引：0，他引：3  

李卓佳  张庆  陈康德 《广东海洋大学学报》1998,(1)

应用以芽孢杆菌为主导菌的微生物复合制剂进行分解养鱼池有机污泥的试验,菌剂合活菌数为109个／g．用量为1.5～4．5mg·L－1。经一个月的试验,池底原有厚3～5cm的有机污泥被分解,并对鱼类有明显的促生长作用。说明应用以芽孢杆菌为主导菌的微生物复合制剂净化养殖池塘底质是一种有效的措施。  相似文献   

Development of a river delta: a case study of Cimanuk river mouth,Indonesia     

Nita Yuanita  Tawatchai Tingsanchali 《水文研究》2008,22(18):3785-3801

This paper describes delta development processes with particular reference to Cimanuk Delta in Indonesia. Cimanuk river delta, the most rapidly growing river delta in Indonesia, is located on the northern coast of Java Island. The delta is subject to ocean waves of less than 1 m height due to its position in the semi‐enclosed Java Sea in the Indonesian archipelago. The study has been carried out using a hydrodynamic model that accounts for sediment movement through the rivers and estuaries. As an advanced approach to management of river deltas, a numerical model, namely MIKE‐21, is used as a tool in the management of Cimanuk river delta. From calibration and verification of hydrodynamic model, it was found that the best value of bed roughness was 0·1 m. For the sediment‐transport model, the calibration parameters were adjusted to obtain the most satisfactory results of suspended sediment concentration and volume of deposition. By comparing the computed and observed data in the calibration, the best values of critical bed shear stress for deposition, critical bed shear stress for erosion and erosion coefficient were 0·05 N m^?2, 0·15 N m^?2, and 0·00001 kg m^?2 s^?1, respectively. The calibrated model was then used to analyse sensitivity of model parameters and to simulate delta development during the periods 1945–1963 and 1981–1997. It was found that the sensitive model parameters were bed shear stresses for deposition and erosion, while the important model inputs were river suspended sediment concentration, sediment characteristics and hydrodynamic. The model result showed reasonable agreement with the observed data. As evidenced by field data, the mathematical model proves that the Cimanuk river delta is a river‐dominated delta because of its protrusion pattern and very high sediment loads from the Cimanuk river. It was concluded that 86% of sediment load from the Cimanuk river was deposited in the Cimanuk delta. Copyright © 2008 John Wiley & Sons, Ltd.  相似文献   

The journal Communications in Numerical Methods in Engineering with Biomedical Applications becomes the International Journal for Numerical Methods in Biomedical Engineering (IJNMBE) from 1st January 2010     

Perumal Nithiarasu  Rainald Löhner 《国际地质力学数值与分析法杂志》2009,33(16):1769-1770

Communications in Numerical Methods in Engineering, founded by Roland W. Lewis in 1985, will change its title to the ‘International Journal for Numerical Methods in Biomedical Engineering’ and has a revised Aims and Scope. Copyright © 2009 John Wiley & Sons, Ltd.  相似文献