微波炉在重量法测定硫中的应用     

姜锋  江荣燕 《岩矿测试》1993,12(2):135-136

采用玻璃砂芯坩埚过滤BaSO_4沉淀,微波炉代替马弗炉恒重坩埚、沉淀,重量法测定了矿石中的硫。方法准确,精密度好。微波炉不需预先升温,加热6min可达恒重,省时、省电。  相似文献   

Thermal analysis in the laser-heated diamond anvil cell     

Jeffrey S. Sweeney  Dion L. Heinz 《Pure and Applied Geophysics》1993,141(2-4):497-507

A new technique actively controls thermal radiation and monitors sample properties during laser-heating in a diamond anvil cell. The technique can be described as a qualitative application of thermal analysis. Discontinuities in temperature, laser power, visible thermal radiation, or in their derivatives as functions of time can be associated with the enthalpy of phase transitions (such as melting) or with changes in maternal properties (such as emissivity).The technique is illustrated with melting experiments on iron-magnesium-silicate perovskite. Temperature corrections associated with these experiments are discussed and the results are briefly reviewed.  相似文献   

基于地基微波辐射计资料对成都双流机场两次雷雨过程的分析     

宋静  傅文伶  张杰 《沙漠与绿洲气象(新疆气象)》2020,14(2):61-67

利用地基微波辐射计资料,比较了2017年7月成都双流机场的两次雷雨过程,根据天气形势分为"两高切变"和"东高西低"2类,在此基础上分析微波辐射计要素变化特征,结果表明:在垂直方向0～10 km,以相对湿度达到80%来区分干区和湿区,则两次过程前3 h,相对湿度在垂直方向均呈现"上下干、中间湿"三层结构,并早于近地层前2 h达到饱和状态;过程期间相对湿度呈现"上干、下湿"两层结构;过程结束后湿层抬高,低层变干。两次过程水汽含量充沛,保持在70 kg/m~2以上,峰值超过85 kg/m~2。每一次中阵雨发生后水汽含量都会短暂回落,但仍高于过程前的数值,不足2 h后再次发生中阵雨。由0℃线高度变化可知,降水过程中,暖区(温度≥0℃)内相对湿度≥90%;云中液态水含量主要分布于6 km以下,温度在0℃以上的液态水占比很高,故两次过程以暖云降水为主。雷雨前1 h左右有"低层气温上升,0℃层抬升,K指数、CAPE指数也明显增大"的典型特征。降水发生在相对湿度、水汽总含量、云中液态水含量和稳定度指数快速增长的波峰中。  相似文献   

Spectral index determination between 408 MHz and 5 GHz in the northern sky     

A.W. Jones  R.J. Davis  A. Wilkinson  G. Giardino  S.J. Melhuish  H. Asareh  R.D. Davies  A.N. Lasenby 《Monthly notices of the Royal Astronomical Society》2001,327(2):545-551

We present the joint analysis of two 5-GHz interferometric surveys of the northern sky, taken with different baselines. The two surveys were carried out on the Jodrell Bank 5-GHz interferometer based at Manchester. The Maximum Entropy Method is used to check the consistency of the two surveys and the final two-dimensional maps are used, together with low-frequency full sky surveys, to put constraints on the Galactic spectral index. It is found that synchrotron emission is the dominant process at high Galactic latitudes below 5 GHz.  相似文献   

Cases-97: Late-Morning Warming And Moistening Of The Convective Boundary Layer Over The Walnut River Watershed     

Margaret A. LeMone  Robert L. Grossman  Robert T. Mcmillen  Kuo-Nan Liou  S.C. Ou  Stuart Mckeen  Wayne Angevine  Kyoko Ikeda  Fei Chen 《Boundary-Layer Meteorology》2002,104(1):1-52

Aircraft, radiosonde, surface-flux, and boundary-layer windprofiler data from the Cooperative Atmosphere Surface Exchange Study's 1997 field project, CASES-97, are combined with synoptic data to study the evolution of the vertically-averaged mixed-layerpotential temperature []and mixing-ratio [Q] onthree nearly-cloudless days from 1000 CST to 1200CST (local noon is approximately 1230 CST). This was achieved through examination of the terms in the time-tendency (`budget')equations for []and [Q]. We estimate three of the terms –local time rate of change, vertical flux divergence, andhorizontal advection. For the [Q]-budget, vertical flux divergence usually dominates, buthorizontal advection is significant on one of the three days. The [Q]-budget balances for two of the three days to within the large experimental error. For the -budget,vertical flux divergence accounts for most of the morningwarming, with horizontal advection of secondary importance.The residual in the -budget has the same sign for all three days, indicating that not all the heating is accounted for. We can balance the []-budgets to within experimental error on two of the three days by correcting the vertical-flux divergence for apparent low biases in the flux measurements of one of the aircraft and in the surface fluxes, and accounting for direct heating of the mixed layer by radiative flux divergence allowing for the effects of carbonaceous aerosols. The [];-budget with these corrections also balances on the third day if horizontal gradients from synoptic maps are used to estimate the horizontal advection. However, the corrected budget for this day does not balance if the horizontal gradient in the advection term is estimated using CASES-97aircraft and radiosondes; we suggest that persistent mesoscale circulations led to an overestimate of the horizontal gradient andhence horizontal advection.  相似文献   

地面感热对青藏高原低涡流场结构及发展的作用   总被引：31，自引：9，他引：22  

李国平  赵邦杰  杨锦青 《大气科学》2002,26(4):519-525

考虑热带气旋类青藏高原低涡为受加热和摩擦强迫并满足热成风平衡的轴对称涡旋系统,通过求解线性化的柱坐标系中涡旋模式的初值问题,分析了地面感热对高原低涡流场结构及发展的影响,给出了高原低涡眼壁内、外侧水平流场和垂直流场的结构特征,讨论了低涡发展与其水平尺度、垂直厚度、所处纬度以及热量总体输送系数和加热强度的关系.结果表明:地面感热对低涡的生成及发展具有重要作用,但这种作用是否有利于低涡的发展与低涡中心和感热加热中心的配置有关.  相似文献   

Space-time soil wetness variations monitoring by a multi-temporal microwave satellite records analysis     

T. Lacava  E.V. Di Leo  V. Tramutoli 《Physics and Chemistry of the Earth》2006,31(18):1274-1283

In the last few years, remote sensing observations have become a useful tool for providing hydrological information, including the quantification of the main physical characteristics of the catchment, such as topography and land use, and of its variables, like soil moisture or snow cover. Moreover, satellite data have also been largely used in the framework of hydro-meteorological risk mitigation.Recently, an innovative Soil Wetness Variation Index (SWVI) has been proposed, using data acquired by the microwave radiometer AMSU (Advanced Microwave Sounding Unit) which flies aboard NOAA (National Oceanic and Atmospheric Administration) satellites.SWVI is based on a general approach for multi-temporal satellite data analysis (RAT - Robust AVHRR Techniques). This approach exploits the analysis of long-term multi-temporal satellite records in order to obtain a former characterization of the measured signal, in term of expected value and natural variability, providing a further identification of signal anomalies by an automatic, unsupervised change-detection step. Such an approach has already demonstrated, in several studies carried out on extreme flooding events which occurred in Europe in the past few years, its capability in reducing spurious effects generated by natural/observational noise. In this paper, the proposed approach is applied to the analysis of the flooding event which occurred in Europe (primarily in NW Spain) in June 2000. Results obtained, in terms of reliability as well as efficiency in space-time monitoring of soil wetness variation, are presented. Future prospects, in terms of exportability of the methodology on the new dedicated satellite missions, like ESA-SMOS and NASA-HYDROS, are also discussed.  相似文献   

微波消解-等离子体发射光谱法同时测定水中硅铁钠   总被引：1，自引：0，他引：1  

李明利  袁园 《岩矿测试》2006,25(3):279-281

讨论使用电感耦合等离子体发射光谱法测定水样中si、Fe、Na时，四种水样前处理方法对测试结果的影响。提出采用HNO3^-HF体系微波消解、H3BO3掩蔽HF的方法前处理水样，用等离子体发射光谱法可同时准确快速地测定水中Si、Fe、Na三种元素的含量。5次测定的相对标准偏差小于4％，加标回收率为89．2％-106％。  相似文献   

微波辅助化学反应制备纳米高岭石     

费进波  田熙科杨起  罗东岳裴芳罗红玉  皮振邦 《岩石矿物学杂志》2006,25(4):335-337

为提高高岭石比表面积、孔隙率和吸附容量，利用微波辅助化学反应制备了尿素-高岭石复合物，进一步微波辐射使层状高岭石完全剥离并粉碎，经分散后得到了纳米高岭石。利用傅立叶红外光谱仪（FT-IR）、X射线粉晶衍射仪（XRD）、扫描电镜（SEM）和透射电镜（硎）进行了过程中样品结构、形貌和尺寸方面的表征。结果表明：同等条件下，通过微波辅助剥离并粉碎层状高岭石，时间只需30min，约为单一球磨的1／20，分散后的纳米高岭石平均粒径约为150nm。  相似文献   

多频率多极化地表辐射参数化模型   总被引：5，自引：2，他引：5  

施建成  蒋玲梅  张立新 《遥感学报》2006,10(4):502-514

发展了针对对地观测系统被动微波辐射计AMSR-E应用的裸露地表辐射模型。首先，利用1993年法国INRA地面试验数据对AIEM在宽波段高频率和大角度的辐射信号模拟能力进行评价。验证结果表明，AIEM模型模拟值与地面实测数据吻合很好，说明AIEM模型能很好模拟宽波段和大角度的辐射信号。在此基础上，用AIEM模型建立了一个针对AMSR-E传感器参数配置．包含各种地表粗糙度和介电特性的裸露地表辐射模拟数据库。利用AIEM模拟数据和地面实测数据对目前人们使用的半经验地表模型进行了比较和分析，发展了多频率多极化的地表辐射参数化模型——Qp模型。该模型中，地表粗糙度对辐射信号的影响通过粗糙度参数Qp来表示。参数Qp可简单表示为均方根高度与相关长度的比值（s／l）。从Qp模型与AIEM模型模拟的发射率比较结果来看，它们之间的绝对误差很小，不超过10^-3因而，本文发展的参数化模型可用作模拟地表辐射的前向模型，如用于估算AMSR-E传感器的亮温值，同时模型的发展有利于提高人们对辐射机制的理解和认识。  相似文献