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31.
样品在分解过程中 ,亚铁易被空气部分氧化 ,致使测试结果偏低 ,采用在HF H2 SO4溶矿过程中加入邻菲卟罗啉 ,与亚铁形成络合物 ,对保护亚铁具有较好的效果。拟定了在塑料坩埚中加邻菲卟罗啉、H2 SO4及HF ,中高温电热板溶矿 ,容量法测定样品中的亚铁 ,方法精密度为 0 .2 3% ,样品加标准回收率 98.8%~ 10 1.9%。此方法具有较好的应用效果  相似文献   
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Man Hoi Lee  S.J. Peale 《Icarus》2006,184(2):573-583
Two small satellites of Pluto, S/2005 P1 (hereafter P1) and S/2005 P2 (hereafter P2), have recently been discovered outside the orbit of Charon, and their orbits are nearly circular and nearly coplanar with that of Charon. Because the mass ratio of Charon-Pluto is ∼0.1, the orbits of P2 and P1 are significantly non-Keplerian even if P2 and P1 have negligible masses. We present an analytic theory, with P2 and P1 treated as test particles, which shows that the motion can be represented by the superposition of the circular motion of a guiding center, the forced oscillations due to the non-axisymmetric components of the potential rotating at the mean motion of Pluto-Charon, the epicyclic motion, and the vertical motion. The analytic theory shows that the azimuthal periods of P2 and P1 are shorter than the Keplerian orbital periods, and this deviation from Kepler's third law is already detected in the unperturbed Keplerian fit of Buie and coworkers. In this analytic theory, the periapse and ascending node of each of the small satellites precess at nearly equal rates in opposite directions. From direct numerical orbit integrations, we show the increasing influence of the proximity of P2 and P1 to the 3:2 mean-motion commensurability on their orbital motion as their masses increase within the ranges allowed by the albedo uncertainties. If the geometric albedos of P2 and P1 are high and of order of that of Charon, the masses of P2 and P1 are sufficiently low that their orbits are well described by the analytic theory. The variation in the orbital radius of P2 due to the forced oscillations is comparable in magnitude to that due to the best-fit Keplerian eccentricity, and there is at present no evidence that P2 has any significant epicyclic eccentricity. However, the orbit of P1 has a significant epicyclic eccentricity, and the prograde precession of its longitude of periapse with a period of 5300 days should be easily detectable. If the albedos of P2 and P1 are as low as that of comets, the large inferred masses induce significant short-term variations in the epicyclic eccentricities and/or periapse longitudes on the 400-500-day timescales due to the proximity to the 3:2 commensurability. In fact, for the maximum inferred masses, P2 and P1 may be in the 3:2 mean-motion resonance, with the resonance variable involving the periapse longitude of P1 librating. Observations that sample the orbits of P2 and P1 well on the 400-500-day timescales should provide strong constraints on the masses of P2 and P1 in the near future.  相似文献   
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Photographic spectra of SN1987A in the LMC have been obtained from 1987 February 25 to 1988 June 30. Microdensitometer tracings of these have been reduced to intensity and corrections for instrumental response have been applied to the spectra. This paper presents these data in an atlas format, discusses the reduction procedures in detail, and presents radial velocity measurements of selected lines in the spectra  相似文献   
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The Tamtsag Basin is located in the extreme eastern portion of the Mongolia. The Basin and its counterpart in China (the Hailar Basin) are united a whole basin on the structural setting. In recent years, the Tamtsag Basin attracts more and more attention with the important exploration discovered in the 19th block by SOCO and in Hailar Basin of China. This paper discusses the exploration potential of Tamtsag Basin from the viewpoint of petroleum geology.  相似文献   
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bdAbstract The open cluster NGC 2818 containing a planetary nebula has been observed inVRI bands using the CCD system at prime focus of the 2.3-metre Vainu Bappu Telescope. The study extending to starsV ∼ 21 magnitude establishes the distance modulus as(m-M) 0 = 12.9 ±0.1 for the cluster. Based on the fitting of theoretical isochrones computed for solar metallicity, an age of 5(±1) × 108 years has been assigned to the cluster. Association of the planetary nebula with the cluster indicates that the progenitor mass of the planetary nebula on the main sequence is ≥2.5M Based on observations obtained with the Vainu Bappu Telescope.  相似文献   
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