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21.
作者以 Sm Cl3 与 (CH3 Cp) Na反应分离得到了三价稀土有机配合物 [(CH3 Cp) 2 Sm Cl·THF]2 的单晶 ,X-射线四圆衍射测定 ,该配合物属正交晶系 ,Pbna空间群 ,晶胞参数 a=9.6 6 2 (2 ) ,b=16 .4 76 (9) ,c=2 0 .582 (9) ;α=β=γ=90°,Z=4。并分析比较 [(CH3 Cp) 2 Sm Cl· THF]2 与其他三价稀土一氯化物的结构特点 相似文献
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报道一种新的有效催化剂-碘-钒盐和在一定条件下合成四溴邻苯二甲酸酐的方法。探讨催化剂的组成配比、用量、温度及废酸循环使用等因素对合成方法的影响。该催化剂的催化效果和常用的碘、碘-铁催化剂相同,适用于四溴邻苯二甲酸酐的合成。 相似文献
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A. Mascle R. Vially E. Deville B. Biju-Duval J.P. Roy 《Marine and Petroleum Geology》1996,13(8):941-961
The Southeast Basin of France is the thickest onshore French sedimentary basin which contains locally as much as 10 km of Mesozoic-Cenozoic sediment. Basin development occurred in several stages between late Carboniferous and late Cretaceous times. Partial tectonic inversion took place during two compressive events, the so-called ‘Pyrenean’ and ‘Alpine’ phases of late Cretaceous-early Tertiary and late Tertiary ages respectively. They are separated by an intervening stretching event of Oligocene age, which further south resulted in the opening of the western Mediterranean oceanic basin. As a result of this complex tectonic history, structural traps were difficult to image on the seismic data shot during the first phase of exploration prior to 1980. Oil and gas natural seeps, and shows in several wells, indicate that some petroleum systems are, or have been active, at least in some places.The present erosional western margin of the basin is more or less superimposed on the initial Triassic-Jurassic margin. Margin subsidence and Tertiary inversion are discussed using regional sections on which the polyphase history of the entire basin is well shown. These sections are located on three major segments where the Mesozoic margin is either partly preserved (Ardèche), or has been partly inverted in late Tertiary times (Vercors-Chartreuse), or has been completely inverted in early Tertiary times (Corbières-eastern Pyrenees). 1-D ‘Genex’ basin modelling on the Ardèche segment, and 2-D ‘Thrustpack’ structural-maturity modelling in the Vercors-Chartreuse segment are used to further assess the remaining petroleum plays. 相似文献
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This paper investigates the use of data assimilation in coastal area morphodynamic modelling using Morecambe Bay as a study site. A simple model of the bay has been enhanced with a data assimilation scheme to better predict large-scale changes in bathymetry observed in the bay over a 3-year period. The 2DH decoupled morphodynamic model developed for the work is described, as is the optimal interpolation scheme used to assimilate waterline observations into the model run. Each waterline was acquired from a SAR satellite image and is essentially a contour of the bathymetry at some level within the inter-tidal zone of the bay. For model parameters calibrated against validation observations, model performance is good, even without data assimilation. However the use of data assimilation successfully compensates for a particular failing of the model, and helps to keep the model bathymetry on track. It also improves the ability of the model to predict future bathymetry. Although the benefits of data assimilation are demonstrated using waterline observations, any observations of morphology could potentially be used. These results suggest that data assimilation should be considered for use in future coastal area morphodynamic models. 相似文献
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碳水化合物的组合合成是一项新兴技术,该技术可以在短时间内合成大量用于进行生物活性筛选的寡糖及拟糖物。液相与固相合成技术可以极大地加快药物研究与开发进程。作者针对该技术在碳水化合物合成方面的研究进展情况进行讨论。 相似文献
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The sediments of the eastern Mediterranean basin contain a series of organic-rich sapropels intercalated with organic-poor nannofossil oozes. Until recently the timing of the onset of sapropel formation was not known accurately because of the low resolution achievable by conventional radiocarbon dating. Compilation of all available 14C-AMS dates show that the base of S-1 (the most recent sapropel) was initiated 8800 years B.P. (14C age corrected by 400 years for reservoir effect) under a 500 m water column and moved progressively into deeper water reaching depths of 3500 m at 8200 years B.P. The linear correlation between the age of S-1 onset and water depth suggests that formation of sapropels moved into deeper water at a rate of 1000 m/200 year. A model is suggested in which export production which sank below the well-mixed surface layers (500 m) was respired consuming dissolved oxygen in the Levantine deep water until a threshold value was reached when sapropels began to be preserved in the sediment. This resulted in a progressively deepening oxygen minimum zone with time until eventually the entire deep water in the basin was oxygen depleted. Assuming that the threshold value for sapropel formation was complete anoxia, it was calculated that primary productivity in the basin during the deposition of S-1 was a factor of 5 greater than that found at present. 相似文献
30.
Accelerated relative sea-level rise and rapid coastal erosion:: testing a causal relationship for the Louisiana barrier islands 总被引:1,自引:0,他引:1
Jeffrey H. List Asbury H. Sallenger Jr. Mark E. Hansen Bruce E. Jaffe 《Marine Geology》1997,140(3-4):347-365
The role of relative sea-level rise as a cause for the rapid erosion of Louisiana's barrier island coast is investigated through a numerical implementation of a modified Bruun rule that accounts for the low percentage of sand-sized sediment in the eroding Louisiana shoreface. Shore-normal profiles from 150 km of coastline west of the Mississippi delta are derived from bathymetric surveys conducted during the 1880s, 1930s and 1980s. An RMS difference criterion is employed to test whether an equilibrium profile form is maintained between survey years. Only about half the studied profiles meet the equilibrium criterion; this represents a significant limitation on the potential applicability of the Bruun rule. The profiles meeting the equilibrium criterion, along with measured rates of relative sea-level rise, are used to hindcast shoreline retreat rates at 37 locations within the study area. Modeled and observed shoreline retreat rates show no significant correlation. Thus, in terms of the Bruun approach, relative sea-level rise has no power for hindcasting (and presumably forecasting) rates of coastal erosion for the Louisiana barrier islands. 相似文献