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Taeko Shinonaga Helmuth Aigner Dilani Klose Peter Spinder Heinz Fröschl David Donohue 《Geostandards and Geoanalytical Research》2008,32(1):93-101
The recommended concentrations of 239Pu, 240Pu and 239+240Pu in reference material IAEA‐315 (marine sediment) were estimated by three analytical methods: isotope dilution thermal ionisation mass spectrometry (TIMS), isotope dilution inductively coupled plasma‐mass spectrometry (ICP‐MS) and alpha spectrometry. The determination of 239Pu and 240Pu (239+240Pu by alpha spectrometry) was carried out with samples from randomly selected bottles using each method. Plutonium‐238 was also measured by alpha spectrometry. A plutonium‐242 reference material was used as a spike for the quantitative analysis. The influence of 242Pu in the samples was therefore calculated; however, this contribution was less than the range of uncertainty and did not influence the final results. The obtained data were statistically analysed using variance component analysis and paired comparison. The combined standard uncertainties from “method/measurement”, “bottle” and “sub‐sample” were in the order of 3 to 6%. The main contributions to the uncertainty were from the material heterogeneity and from systematic differences between methods. Based on this study with twenty‐seven analyses using 10–14 g sample mass, concentrations of (38 ± 3) Bq kg?1, (28 ± 3) Bq kg?1 and (66 ± 4) Bq kg?1 are proposed as recommended values for 239Pu, 240Pu and 239+240Pu, respectively, and (9.5 ± 0.4) Bq kg?1 for 238Pu as an information value in reference material IAEA‐315. In mass concentration units, these amount to (16.4 ± 1.2) ng kg?1, (3.3 ± 0.4) ng kg?1 and (0.015 ± 0.003) ng kg?1 for 239Pu, 240Pu and 238Pu, respectively. The certified reference materials NIST 4350B and NIST 4354 were also analysed by TIMS for quality assurance of the method used in this study. 相似文献
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作为GPS/重力边值问题理论及方法的应用,在对GPS/重力方法确定(似)大地水准面的原理进行简要介绍与分析的基础上,利用收集到的N区的600个GPS/重力数据和48个高精度GPS水准数据,计算出该区域的(似)大地水准面。通过拟合法和系统差直接改正法进行的精度分析表明,应用GPS/重力数据结合水准方法确定的该地区(似)大地水准面的精度达到厘米级精度。 相似文献
45.
Extreme value analysis provides a semiparametric method for analyzing the extreme long tails of skew distributions which may be observed when handling mining data. The estimation of important tail characteristics, such as the extreme value index, allows for a discrimination between competing distribution models. It measures the thickness of such long tailed distributions, if only a limited sample is available. This paper stresses the practical implementation of extreme value theory, which is used to discriminate a lognormal from a mixed lognormal distribution in a case study of size distributions for alluvial diamonds. 相似文献
46.
关于海平面上升及其环境效应 总被引:12,自引:0,他引:12
沿海地区地质环境复杂。由于国民经济的迅速发展,人类活动日益增多,对地质环境进一步造成严重的不利影响。特别是“温室效应”引发的海平面上升,使各种地质灾害更加激化。文章详细探讨了海平面上升的影响因素,理论海平面与相对海平面升降幅度的评估,以及海平面上升所造成的地质环境效应与相应的防治对策,特别强调控制沿海城市地面沉降,以减轻海平面相对上升造成的危害,具有特殊而重要的意义。 相似文献
47.
Darren G. Bos Brian F. Cumming Christine E. Watters John P. Smol 《International Journal of Salt Lake Research》1996,5(1):1-15
Zooplankton collected from vertical net tows were related to the environmental variables from 98 lakes from the Interior Plateau of British Columbia. Canonical correspondence analysis showed that both salinity and ionic composition (pH and Mg) of the lake-water made major and significant contributions to the first two ordination axes (=0.42 and 0.11 respectively,P<0.05). BothArtemia franciscana andMoina hutchinsoni had their highest relative abundance in meso-hypersaline waters. However,Artemia franciscana preferred waters that were higher in Mg and Ca, whileMoina hutchinsoni was found in waters that were lower in Mg and Ca. Similarly, at intermediate salinities,Daphnia pulex and the calanoid copepods preferred waters slightly lower in Mg and Ca, whereasCeriodaphnia laticaudata andSimocephalus spp. were relatively more common in waters higher in Mg and Ca. Because the freshest lakes studied varied much less in ionic composition, the zooplankton in these lakes did not show a preference to ionic composition. As expected, multi-generic groups, such as the calanoid copepods, cyclopoid copepods and nauplii, had wider tolerances to conductivity than groups identified to lower taxonomic levels. Significant weighted-averaging regression and calibration models of conductivity were developed based on zooplankton species composition from the study lakes (r
2=0.56,P<0.05). Samples composed largely of multi-generic taxa yielded the worst estimates of salinity in the reconstruction model. This study suggests that zooplankton community composition may be developed into a useful proxy for paleosalinity reconstruction. 相似文献
48.
浙闽山区茶叶生产基地评价的探讨 总被引:6,自引:0,他引:6
茶叶基地的评价包括对基地的自然和经济条件的评估,应用系统分析方法,将自然和经济条件进行定量的综合评估,用综合评价值区分基地间的差异,最后定性与定量相结合,提出茶叶生产基地的合理布局. 相似文献
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