排序方式: 共有53条查询结果,搜索用时 703 毫秒
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采用原子吸收法对肉类样品微量铜铅锌镉进行测定,重点对样品的前处理进行实验,拟订测试操作规程和仪器测量最佳条件,实验证明本法操作简便,准确快速,结果满意。 相似文献
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Janet M. Hergt Ricardo Arevalo Jr L. Paul Bèdard Jeremy Bellucci Jacinta Enzweiler Klaus Peter Jochum Kathryn L. Linge William F. McDonough Regina Mertz-Kraus Michael Wiedenbeck Xiaohong Wang Jon D. Woodhead 《Geostandards and Geoanalytical Research》2010,34(4):325-326
This collection of articles represents the fourth in a series of reviews in which authors have aimed at capturing the key advances in a range of analytical fields ( Hergt et al. 2005, 2006, 2008 ). The publication period under review is 2008–2009 and the intention here is to provide readers with a summary of the most influential developments published during this period, across a broad range of topics appropriate to the Earth and environmental sciences. Most authors comment on the ways in which the emphases of research in their specific fields of examination have changed over time. All note an increase in rigour and focus on data quality. Whether advances have taken place in instrumentation, sample manipulation or data deconvolution, there are a large number of dedicated scientists out there contributing to the high quality of geochemical data employed in geological and environmental research. 相似文献
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Neutron Activation Analysis, Atomic Absorption and X-Ray Fluorescence Spectrometry Review for 2003 总被引:1,自引:0,他引:1
This review for the year 2003 deals with three relatively well-established, mature, analytical techniques (neutron activation analysis, atomic absorption spectrometry and X-ray fluorescence spectrometry) that nevertheless remain very important for the characterisation of geological and environmental samples. Developments in neutron activation analysis included modification to the technique in relation to the determination of platinum-group elements, as well as consideration of sample size in ore grade estimation. A considerable body of literature was published on the application of atomic absorption spectrometry in the analysis of environmental samples. Many of these proposed technical and methodological improvements, notably in extraction procedures. X-ray fluorescence spectrometry saw developments in in situ analysis, synchrotron micro-XRF (μ-SRXRF) and a confocal X-ray set-up for 3D elemental imaging. XRF technologies were used in the analysis of geological samples, reference materials, glasses, solutes and environmental materials. 相似文献
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原子吸收法测定炼银炉渣中的金 总被引:6,自引:1,他引:6
采用HF-H2SO4除硅,萃取-原子吸收法测定炼银炉渣中的金。样品加标回收率为92.0%-104.0%,相对标准偏差为3.8%(n=11)。将该法应用到炼银炉渣中金的测定,结果符合分析质量要求。 相似文献
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聚氨酯泡塑对不同价态金吸附性能的研究及应用 总被引:7,自引:0,他引:7
研究了聚氨酯泡沫塑料对不同价态金的吸附行为,选择了泡塑吸附和硫脲解脱以及用原子吸收法测定的最佳条件。方法已应用于黄铁矿和毒砂单矿物中价态金的测定,黄铁矿中各价态金的加和与总金量相符,加标回收实验Au(Ⅲ),Au(Ⅰ),Au(0)的回收率分别为98=5%,98.8%和104%,为矿样中痕量金的价态分析提供了一个可靠的方法。 相似文献
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小锍试金-无火焰原子吸收法测定地质样品中超痕量金铂铑钯 总被引:1,自引:1,他引:1
将锍试金改成小锍试金,用小锍扣捕集法把分解样品同富集贵金属与分离基体成份结合在一起进行,炼得的锍扣经酸处理除去贱金属硫化物,富集的贵金属采用无火焰原子吸收光谱测定。取一份样可以测定Au、Pt、Rh和Pd。测定方法的特征质量(g):Au1.1×10 ̄(-11),Pt1.3×1O ̄(-10),Pd1.3×10 ̄(-11),Rh1.2×10 ̄(-11);线性范围(g/ml):Au0~0.040,Pd和Rh为0~0.050,Pt为0~0.50。方法用于超基性岩标样的测定,结果与推荐值相符。 相似文献
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