ICP-AES测定海洋生物体中13种元素的微波消解条件优化   总被引：3，自引：1，他引：2  

孙玲玲  宋金明  林强  孙萱  于颖 《海洋科学》2014,38(8):26-33

报道了微波密闭消解正交试验条件优化电感耦合等离子体发射光谱法(ICP-AES),同时测定8种海洋生物体中硒、铁、锰、锌、钙、镁、锶、砷、镉、铬、铜、铅和镍等13种元素含量的实验结果。优化后的样品消解条件为加入的HNO3V:H O2 2V=6.0 mL:1.0 mL,第二步程序升温温度为170℃,消解时间20 min;测定标准曲线相关系数大于0.999,相对标准偏差为0.30%~2.55%,加标回收率为92.0%~104.8%,方法检出限为0.0010~0.0468μg/g。结果表明,优化后方法测定操作简便、具有高的灵敏度、准确度和精密度,且能多元素同时测定,适合于海洋生物样品中这些元素含量的准确测定,并可为评估海产品食用安全提供科学依据。  相似文献   

地理国情普查 DOM 的制作及检查     

陈姝 《东北测绘》2014,(6):149-150,153

DOM是国情普查内容的重要组成部分,是地理国情普查中调查的重要数据源。本文通过卫星影象纠正,控制点选取,全色波段影像正射纠正,多光谱影像与全色波段影像配准,多光谱影像与全色波段影像融合等技术手段,确保了DOM的精度,为国情普查的后续工作提供精确的基础资料。  相似文献   

Evaluation of the mussel Perna perna as a biomonitor of polycyclic aromatic hydrocarbon (PAH) exposure and effects     

Francioni E  de L R Wagener A  Scofield AL  Depledge MH  Cavalier B 《Marine pollution bulletin》2007,54(3):329-338

The mussel Perna perna was used to monitor and assess areas suspected of oil contamination by transplanting animals from unimpacted to impacted sites and vice versa. The deployment lasted for three months during which total PAH were measured in seawater samples collected every 15 days. PAH concentrations were determined in mussel tissue monthly. The lysosomal neutral red assay and the condition index were used as biomarkers of the adverse biological effects. The PAH concentration in mussels at unimpacted sites, prior to deployment was ca. 100 microg kg(-1) but increased to 300 microg kg(-1) after three months at the contaminated site. Mussels transplanted to the uncontaminated site showed a decrease from 380 to 80 microg kg(-1). Significant changes in lysosomal stability occurred within one month of the beginning of the transposition; in contrast condition indexes were not correlated with the observed changes in PAH concentration.  相似文献   

市政管道状况评价技术研究     

张飘平  沈华  马保松 《岩土钻凿工程》2010,(1):127-132

本文首先对管道缺陷状况进行了总结分类,并对管道缺陷状况评价方法进行了探讨,以此为基础,用VB6．0开发了相应的管道状况评价软件,然后,采用层次分析法对管道各类缺陷严重性进行了分析,得出管道修复优先次序,为市政管道的评价与维护提供了一定的参考意见。  相似文献   

模拟地震环境土钉墙基坑支护设计研究     

李瑞琪  罗建鸿  张国林 《云南地质》2010,29(3):338-340,337

根据土体边坡滑动面破坏模式,拟静力法,在稳定性模型的假定条件下,建立地震作用下土钉支护边坡稳定性模型,并对云南映象中水处理厂的基坑土钉墙支护进行了计算,得到满意结果。  相似文献