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84.
柱撑蒙脱石制备与表征 总被引:47,自引:2,他引:47
本文采用多种方法制备keggin离子,并探索出制备稳定keggin离子的适宜酸碱度,用此柱化剂制备出层间距为2.4~2.5nm的柱撑蒙脱石。应用X射线走向衍射技术、红外光谱、差热分析对往撑蒙脱石进行表征,用BET、吡啶吸附考察了其表面物理化学性质。结果表明,用Keggin离子制备出的柱撑蒙脱石其层间距在自然状态下为2.4~2.5nm,350C灼烧,层间距稳℃定在1.8nm,且具有耐热性能好、较大的比表面积和较强的Lewis酸位中心等特点. 相似文献
85.
矿物流体包裹体中的羧酸曾贻善刘家齐(北京大学地质系,北京100871)(地矿部宜昌地质矿产研究所,宜昌443003)关键词矿物包裹体浸取液羧酸离子色谱分析分子中含有羧基官能团(—COOH)的物质称为羧酸。Fein[1]和Shock[2]曾概述羧酸在自... 相似文献
86.
唐古拉山冬克玛底冰川雪层中淋溶作用的初步研究 总被引:7,自引:7,他引:7
利用唐古拉山冬克玛底冰川雪坑和表层积雪样品的实测资料,初步探讨本区雪层中离子淋溶作用的特征,影响因素及其对冰芯记录的干扰。研究发现淋溶作用能够对数周至数月时间尺度的雪层记录产生“平滑”作用,但不会影响冰芯记录的长期变化趋势。 相似文献
87.
宝鸡某场地污染土的分析评价 总被引:5,自引:0,他引:5
宝鸡某场地由于长期堆放食盐,造成地基上污染、通过勘察,查明了污染土层,进行了腐蚀性测试和评价,对场地污染区与非污染区土的物理力学性质指标进行了对比,并分析了土的污染机理,提出了防护措施。 相似文献
88.
The application of X-ray photoelectron spectroscopy (XPS) to coal surface characterisation for preparation research is described. Progress towards the acquisition of complementary surface chemical information by time-of-flight secondary ion mass spectrometry (ToF-SIMS) is also discussed. Surface-based beneficiation techniques such as flotation are assuming greater importance as the proportion of fines in raw coal increases due to the proliferation of high capacity mining methods. A necessary condition for the floatability of a coal particle is adequate hydrophobicity, and the degree of hydrophobicity of the flotation concentrate is one factor influencing the ease with which its dewatering can be affected. The hydrophobicity of a coal is very difficult to measure directly because of microporosity, and it is often necessary to deduce the degree of hydrophobicity from a knowledge of the surface chemistry. XPS is able to provide sufficient analytical data to allow relative levels of hydrophobicity to be estimated. In principle, ToF-SIMS should be able to supply additional information enabling refinement of such estimates; however, there are insufficient data at present to allow the ionic fragments detected to be related to specific functional groups at the coal surface. 相似文献
89.
探讨了45Mn2钻杆接头的各种热处理工艺降综合机械性能,应用断裂力学优选最佳热处理工艺,并已投入生产。 相似文献
90.
Estimation of groundwater evaporation and salt flux from Owens Lake, California, USA 总被引:3,自引:0,他引:3
S. W. Tyler S. Kranz M. B. Parlange J. Albertson G. G. Katul G. F. Cochran B. A. Lyles G. Holder 《Journal of Hydrology》1997,200(1-4):110-135
Groundwater evaporation and subsequent precipitation of soluble salts at Owens Lake in eastern California have created one of the single largest sources of airborne dust in the USA, yet the evaporation and salt flux have not been fully quantified. In this study, we compare eddy correlation, microlysimeters and solute profiling methods to determine their validity and sensitivity in playa environments. These techniques are often used to estimate evaporative losses, yet have not been critically compared at one field site to judge their relative effectiveness and accuracy. Results suggest that eddy correlation methods are the most widely applicable for the variety of conditions found on large playa lakes. Chloride profiling is shown to be highly sensitive to thermal and density-driven fluxes in the near surface and, as a result, appears to underestimate yearly groundwater evaporation. Yearly mean groundwater evaporation from the playa surface estimated from the three study areas was found to range from 88 to 104 mm year−1, whereas mean evaporation from the brine-covered areas was 872 mm year−1. Uncertainties on these mean rates were estimated to be ±25%, based on comparisons between eddy correlation and lysimeter estimates. On a yearly basis, evaporation accounts for approximately 47 × 106 m3 of water loss from the playa surface and open-water areas of the lake. Over the playa area, as much as 7.5 × 108 kg (7.5 × 105 t) of salt are annually concentrated by evaporation at or near the playa surface, much of which appears to be lost during dust storms in area. 相似文献