Focused ion beam technique and transmission electron microscope studies of microdiamonds from the Saxonian Erzgebirge, Germany     

Larissa F. Dobrzhinetskaya  Harry W. Green  Matthew Weschler  Mark Darus  Young-Chung Wang  Hans-Joachim Massonne  Bernhard St  ckhert 《Earth and Planetary Science Letters》2003,210(3-4):399-410

A focused ion beam of Ga ions is a relatively new technique that has been developed for microelectronic industries. Now researchers of the Earth sciences find it to be a promising tool for studying various geological materials. Using the FIB technique and an FEI Strata DB 235 dual beam system, we have successfully prepared several electron-transparent foils, which crossed μm-sized diamonds included in host minerals such as zircon and garnet from quartzofeldspathic rocks of the Saxonian Erzgebirge, Germany. Scanning and transmission electron microscopy applied to these foils revealed that the diamonds contain crystalline nanometric inclusions. These inclusions consist of minerals of known stoichiometries such as SiO₂ and Al₂SiO₅, whereas others are characterized by different combinations of Si, K, P, Ti, and Fe in the presence of oxygen (stoichiometries are not clear at this stage of research). One suite of inclusions is assumed to be represented by archerite, KH₂PO₄, which is known to be stable at pressures of 4–22 GPa, and one nanocrystal containing Pb, oxygen and carbon is interpreted to be Pb_xO_y or PbCO₃. Along with solid crystalline inclusions, the diamonds contain cavities filled by liquid/gas that escaped during sample preparation. These are associated with dislocations of diamond growth. Our data are consistent with the concept of diamond crystallization from a COH-rich multicomponent supercritical fluid and suggest that the composition of such a fluid is more consistent with a local crustal source rather than that of a mantle origin.  相似文献   

Decoupled seismic analysis of an earth dam   总被引：2，自引：0，他引：2  

Ernesto Cascone  Sebastiano Rampello 《Soil Dynamics and Earthquake Engineering》2003,23(5):349-365

The seismic stability of an earth dam is evaluated via the decoupled displacement analysis using the accelerograms obtained by ground response analysis to compute the earthquake-induced displacements. The response analysis of the dam is carried out under both 1D and 2D conditions, incorporating the non-linear soil behaviour through the equivalent linear method. Ten artificial and five real accelerograms were used as input motions and four different depths were assumed for the bedrock.1D and 2D response analyses were in a fair agreement with the exception of the top third of the dam where only a 2D modelling of the problem could ensure that the acceleration field is properly described. The acceleration amplification ratio obtained in the 2D analyses was equal to about 2 in all the cases considered, consistently with data from real case histories.The maximum permanent displacements computed by the sliding block analysis were small, being less than 10% of the service freeboard; a satisfactory performance of the dam can then be envisaged for any of the seismic scenarios considered in the analyses.  相似文献   

Asymmetric one‐storey elastic systems with non‐linear viscous and viscoelastic dampers: Simplified analysis and supplemental damping system design     

Wen‐Hsiung Lin  Anil K. Chopra 《地震工程与结构动力学》2003,32(4):579-596

Investigated is the accuracy in estimating the response of asymmetric one‐storey systems with non‐linear viscoelastic (VE) dampers by analysing the corresponding linear viscous system wherein all non‐linear VE dampers are replaced by their energy‐equivalent linear viscous dampers. The response of the corresponding linear viscous system is determined by response history analysis (RHA) and by response spectrum analysis (RSA) extended for non‐classically damped systems. The flexible and stiff edge deformations and plan rotation of the corresponding linear viscous system determined by the extended RSA procedure is shown to be sufficiently accurate for design applications with errors generally between 10 and 20%. Although similar accuracy is also shown for the ‘pseudo‐velocity’ of non‐linear VE dampers, the peak force of the non‐linear VE damper cannot be estimated directly from the peak damper force of the corresponding linear viscous system. A simple correction for damper force is proposed and shown to be accurate (with errors not exceeding 15%). For practical applications, an iterative linear analysis procedure is developed for determining the amplitude‐ and frequency‐dependent supplemental damping properties of the corresponding linear viscous system and for estimating the response of asymmetric one‐storey systems with non‐linear VE dampers from the earthquake design (or response) spectrum. Finally, a procedure is developed for designing non‐linear supplemental damping systems that satisfy given design criteria for a given design spectrum. Copyright © 2003 John Wiley & Sons, Ltd.  相似文献   

A unified formulation of the piecewise exact method for inelastic seismic demand analysis including the P‐delta effect     

M. N. Ayd&#x;nolu  Y. M. Fahjan 《地震工程与结构动力学》2003,32(6):871-890

The non‐linear analysis of single‐degree‐of‐freedom (SDOF) systems provides the essential background information for both strength‐based design and displacement‐based evaluation/design methodologies through the development of the inelastic response spectra. The recursive solution procedure called the piecewise exact method, which is efficiently used for the response analysis of linear SDOF systems, is re‐formulated in this paper in a unified format to analyse the non‐linear SDOF systems with multi‐linear hysteresis models. The unified formulation is also capable of handling the P‐delta effect, which generally involves the negative post‐yield stiffness of the hysteresis loops. The attractiveness of the method lies in the fact that it provides the exact solution when the loading time history is composed of piecewise linear segments, a condition that is perfectly satisfied for the earthquake excitation. Based on simple recursive relationships given for positive, negative and zero effective stiffnesses, the unified form of the piecewise exact method proves to be an extremely powerful and probably the best tool for the SDOF inelastic time‐history and response spectrum analysis including the P‐delta effect. A number of examples are presented to demonstrate the implementation of the method. Copyright © 2003 John Wiley & Sons, Ltd.  相似文献   

A rooftop tuned mass damper frame     

Jerod G. Johnson  Lawrence D. Reaveley  Chris Pantelides 《地震工程与结构动力学》2003,32(6):965-984

This article documents the analytical study and feasibility of placing a tuned mass damper in the form of a limber rooftop moment frame atop relatively stiff structures to reduce seismic acceleration response. Six existing structures were analytically studied using a suite of time history and response spectra records. The analyses indicate that adding mass in conjunction with a limber frame results in an increase in the fundamental period of each structure. The fundamental period increase generally results in a decrease in seismic acceleration response for the same time history and response spectra records. Owing to the limber nature of the rooftop frames, non‐linear analysis methods were required to evaluate the stability of the rooftop tuned mass damper frame. The results indicate the addition of a rooftop tuned mass damper frame reduces the seismic acceleration response for most cases although acceleration response can increase if the rooftop frame is not tuned to accommodate the specific structure's dynamic behaviour and localized soil conditions. Appropriate design of the rooftop tuned mass damper frame can result in decreased seismic acceleration response. This translates to safer structures if used as a retrofit measure or a more economical design if used for new construction. Copyright © 2003 John Wiley & Sons, Ltd.  相似文献   

System identification of linear structures based on Hilbert–Huang spectral analysis. Part 2: Complex modes     

Jann N. Yang  Ying Lei  Shuwen Pan  Norden Huang 《地震工程与结构动力学》2003,32(10):1533-1554

A method, based on the Hilbert–Huang spectral analysis, has been proposed by the authors to identify linear structures in which normal modes exist (i.e., real eigenvalues and eigenvectors). Frequently, all the eigenvalues and eigenvectors of linear structures are complex. In this paper, the method is extended further to identify general linear structures with complex modes using the free vibration response data polluted by noise. Measured response signals are first decomposed into modal responses using the method of Empirical Mode Decomposition with intermittency criteria. Each modal response contains the contribution of a complex conjugate pair of modes with a unique frequency and a damping ratio. Then, each modal response is decomposed in the frequency–time domain to yield instantaneous phase angle and amplitude using the Hilbert transform. Based on a single measurement of the impulse response time history at one appropriate location, the complex eigenvalues of the linear structure can be identified using a simple analysis procedure. When the response time histories are measured at all locations, the proposed methodology is capable of identifying the complex mode shapes as well as the mass, damping and stiffness matrices of the structure. The effectiveness and accuracy of the method presented are illustrated through numerical simulations. It is demonstrated that dynamic characteristics of linear structures with complex modes can be identified effectively using the proposed method. Copyright © 2003 John Wiley & Sons, Ltd.  相似文献   

Evaluation of predictors of non‐linear seismic demands using ‘fishbone’ models of SMRF buildings     

Nicolas Luco  Yasuhiro Mori  Yosuke Funahashi  C. Allin Cornell  Masayoshi Nakashima 《地震工程与结构动力学》2003,32(14):2267-2288

Predictors (or estimates) of seismic structural demands that are less computationally time‐consuming than non‐linear dynamic analysis can be useful for structural performance assessment and for design. In this paper, we evaluate the bias and precision of predictors that make use of, at most, (i) elastic modal vibration properties of the given structure, (ii) the results of a non‐linear static pushover analysis of the structure, and (iii) elastic and inelastic single‐degree‐of‐freedom time‐history analyses for the specified ground motion record. The main predictor of interest is an extension of first‐mode elastic spectral acceleration that additionally takes into account both the second‐mode contribution to (elastic) structural response and the effects of inelasticity. This predictor is evaluated with respect to non‐linear dynamic analysis results for ‘fishbone’ models of steel moment‐resisting frame (SMRF) buildings. The relatively small number of degrees of freedom for each fishbone model allows us to consider several short‐to‐long period buildings and numerous near‐ and far‐field earthquake ground motions of interest in both Japan and the U.S. Before doing so, though, we verify that estimates of the bias and precision of the predictor obtained using fishbone models are effectively equivalent to those based on typical ‘full‐frame’ models of the same buildings. Copyright © 2003 John Wiley & Sons, Ltd.  相似文献   

A Linear Programming Approach to Determine the Normative Composition of Sedimentary Rocks     

V. N. Podkovyrov  O. V. Graunov  R. L. Cullers 《Mathematical Geology》2003,35(4):459-476

The analysis of modal and normative composition of sedimentary rocks is widely used for studying their sources and tectonic settings. The normative calculation of the mineral composition of rocks in this study is formulated as a linear programming problem and is solved by means of the simplex method. This enables both simultaneous and successive subtraction of a set of basic minerals from a rock sample represented by its chemical composition {SiO₂...LOI}. Such an approach provides a more exact calculation of the contribution of basic minerals in the rock. This mathematical approach is used to study two representative sets of sandstones and fine-grained rocks from a Meso- to Neoproterozoic marginal basin of southeastern Siberia (Uchur–Maya region, Yakutia) and a Pennsylvanian-Lower Permian uplifted continental block in Colorado, USA. The calculated normative mineral compositions of the Siberian sandstones are consistent with the observed modal compositions. These sandstones vary from K- Feldspar rich arkoses at the base of the sequence (the Uchur Group, lower Riphean) to quartz arenites or lithic sandstones and wacke in transgressive successions of the middle-upper Riphean. Arkoses and quartz arenites are dominant in Meso- to Neoproterozoic Siberia. These samples represent craton interior uplifted basement and quartzose, recycled orogen provenance of a stable craton in Rodinia. There are higher but consistent discrepancies between the calculated and observed compositions for the Pennsylvanian to Lower-Permian arkoses and quartz arenites (Sangre de Cristo, Belden, and Maroon Formations). The differences between the predicted and observed mineralogy may be due to uncertainties in the modes in the matrix and cement of the sandstones. This normative program should supplement modal calculations and provide better genetic constructions, especially in case of matrix-rich sandstones.  相似文献   

Smoothing and Change Point Detection for Gamma Ray Count Data   总被引：1，自引：0，他引：1  

Daniela Leonte  David J. Nott  William T. M. Dunsmuir 《Mathematical Geology》2003,35(2):175-194

Gamma ray detectors are used to measure the natural radioactivity of rocks. For a number of boreholes drilled at a site the gamma ray detector is lowered into each borehole and counts of gamma ray emissions at different depths are recorded as the instrument is gradually raised to ground level. The profile of gamma counts can be informative about the geology at each location. The raw count data are highly variable, and in this paper we describe the use of adaptive smoothing techniques and change point models in order to identify changes in the geology based on the gamma logs. We formulate all our models for the data in the framework of the class of generalized linear models, and describe computational methods for Bayesian inference and model selection for generalized linear models that improve on existing techniques. Application is made to gamma ray data from the Castelreagh Waste Management Centre which served as a hazardous waste disposal facility for the Sydney region between March 1974 and August 1998. Understanding the geological structure of this site is important for further modelling the transport of pollutants beneath the waste disposal area.  相似文献   

Determination of Halogens (F, Cl, Br, I), Sulfur and Water in Seventeen Geological Reference Materials   总被引：5，自引：0，他引：5  

Agnès Michel  Benoît Villemant 《Geostandards and Geoanalytical Research》2003,27(2):163-171

Fluorine, chlorine, bromine, iodine and sulfur were determined in seventeen geological reference materials after extraction by pyrohydrolysis. Fluorine, Cl and S (as sulfate ions) were determined in the extraction solution by ion chromatography with detection limits of around 0.2 mg l⁻¹. Bromine and I were measured by ICP-MS with detection limits of 1 μg l⁻¹ for Br and 0.1 μg l⁻¹ for I. For rock samples, using normal extraction conditions (500 mg of sample and 100 ml of final solution) detection limits were 40 mg kg⁻¹ for F and Cl, 15 mg kg⁻¹ for S, 0.2 mg kg⁻¹ for Br and 0.02 mg kg⁻¹ for I. These detection limits may be improved by increasing the amount of sample and hence the concentration of the final solution. Water was also determined using an extraction technique based on H₂O degassing, reduction on zinc at 1000 °C and H₂ manometry. Our results for fluorine, chlorine, sulfur and water are in good agreement with literature data. Very few reference materials have recommended values for bromine and especially for iodine. Among the analysed samples, three are new reference materials: BHVO-2, BCR-2 and AGV-2.  相似文献