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Sandro Fadda 《Geostandards and Geoanalytical Research》2005,29(1):143-156
Major concentrations of Al2O3, Fe2O3, MgO, CaO, Na2O and K2O, minor levels of TiO2, P2O5 and thirty petrologically, geochemically and environmentally significant trace elements have been determined in microwave oven acid leachates of whole powdered coal samples by direct current plasma‐atomic emission spectrometry (DCP‐AES). A single sample preparation procedure was suitable for all the determinations with no additional dilution step for major elements solution. Dried samples (0.5 g) were treated in low‐pressure PFA digestion vessels with HF/HCl/HNO3/HClO4 acids to quantitatively extract the analytes from the bulk material, while leaving the major part of organic matrix as a residue. The major constituents of geological samples, in particular the easily ionised elements (EIEs) such as alkali and alkaline earths, may complicate the instrumental determinations in DCP‐AES because of differential enhancements of elemental emission intensities and stray light interferences. Taking account of these factors, the coal matrix is considered to have very low major oxide totals as compared to many other common geo‐environmental and related materials (rocks, sediments, soil, ashes etc.). The sample size employed here, while yielding a relatively concentrated solution to cover a wide range of elemental determinations, provided a sample matrix that significantly diminished interferences for DCP measurements. The need for closely matching the unknowns and calibrators was eliminated except for overall acidity and an excess quantity of caesium for EIE buffering. Calibration of the spectrometer was accomplished by simple aqueous single element solutions as high concentration calibrators in addition to a reagent blank as a low concentration calibrator. Two point working curves were established to allow for the maximum concentrations of each element expected in the unknowns. The precision of determinations under routine conditions as well as the reproducibility of the leaching and precision of instrumental measurements have been evaluated. Relative standard deviations (RSD) were of 1–2% for those elements whose concentrations in solid samples were well above the limits of quantification. Method detection limits in the buffered solutions were also evaluated. To evaluate the accuracy of the microwave oven‐DCP method a suite of eight certified coal reference materials of differing rank, were analysed with good agreement with the certified and/or available published data. Results are presented for the uncertified major oxides in the AR series reference materials. 相似文献
185.
对薄壁金刚石钻头胎体进行了性能分析和配方设计探讨,尤其根据被钻切介质对钻头胎体性能的要求作了较详细的分析,从理论分析结合实践经验筛选出了钻切建筑石材和各种钢筋砼的钻头胎体配方,在生产中满足了钻头工作条件的要求。 相似文献
186.
Naïma AbouAli Mohamad Hafid El Hassane Chellaï Mohamed Nahim Mahmoud Zizi 《Comptes Rendus Geoscience》2005,337(14):1267-1276
Seismic reflection profiles from the Ifni/Tan-Tan Atlantic margin of southern Morocco, interpreted in the light of well data and field geology from the Western Anti-Atlas, allowed us to establish the seismostratigraphic framework of the syn-rift series and to reveal (i) a compressional structural style in the pre-Triassic basement similar to that established in the adjacent outcropping onshore basement but with an opposed western vergence, (ii) the importance of inherited anterior structures in the formation of Triassic-Liassic rift structures and (iii) an east–west propagation of these rift structures. To cite this article: N. AbouAli et al., C. R. Geoscience 337 (2005). 相似文献
187.
Transient seepage analysis in zoned anisotropic soils based on the scaled boundary finite‐element method 下载免费PDF全文
The scaled boundary finite‐element method, a semi‐analytical computational scheme primarily developed for dynamic stiffness of unbounded domains, is applied to the analysis of unsteady seepage flow problems. This method is based on the finite‐element technology and gains the advantages of the boundary element method as well. Only boundary of the domain is discretized, no fundamental solution is required and singularity problems can be modeled rigorously. Anisotropic and non‐homogeneous materials satisfying similarity are modeled with no additional efforts. In this study, firstly, formulation of the method for the transient seepage flow problems is derived followed by its solution procedures. The accuracy, simplicity and applicability of the method are demonstrated via four numerical examples of transient seepage flow – three of them are available in the literature. Homogenous, non‐homogenous, isotropic and anisotropic material properties are considered to show the versatility of the technique. Excellent agreement with the finite‐element method is observed. The method out‐performs the finite‐element method in modeling singularity points. Copyright © 2014 John Wiley & Sons, Ltd. 相似文献
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在对极化干涉SAR森林树高反演的DEM差值算法、相干相位-幅度综合反演算法进行分析的基础上,对基于极化干涉相干优化方法的改进算法进行了探讨。利用黑龙江大兴安岭地区的一对ALOS全极化干涉SAR数据进行实验,并对比分析各算法的反演结果。结果表明,在使用改进的算法进行森林树高反演时可以获取精度较高的反演结果,并且在一定程度上提高了森林树高反演的稳定性,为森林树高反演工作的业务化运行提供一定的依据。 相似文献
189.
设计了一种采用基础矩阵的立体像对核线影像制作方法,由基础矩阵来描述影像间的相对方位关系,避免了相对定向过程中复杂的迭代过程。通过稀疏匹配获取高精度的同名点,由基础矩阵确定每组同名点对应的同名核线,根据核线必相交于核点的原理,采用最小二乘法确定左右影像的核点坐标;然后根据核点坐标完成影像间核线的快速映射,沿核线方向采用双线性内插法进行核线重采样,完成核线影像制作。采用多组影像进行核线影像制作实验,对生成的核线影像进行同名特征点提取与匹配,结果表明采用该方法制作的核线影像上下视差较小,验证了方法的有效性。 相似文献
190.
以LandSat多时相影像为数据源,采用基于规则的面向对象分类方法,监测会理县2000~ 2015年地表覆盖变化.结合1∶50 000 DEM数据,分析了会理县地表覆盖构成与转移、变化动态度及潜在退耕地情况.监测分析结论能为会理县加强空间管制、促进土地资源集约利用、指导生态文明建设等提供决策信息支撑. 相似文献