高斯平面坐标换算到测区平均高程面上的方法   总被引：5，自引：2，他引：5  

鲍建宽 《测绘工程》1997,6(3):46-49,55

依据高斯投影原理，提出了一种在高斯平面与任决高程平面间进行坐标转换的方法，并设计了相应的计算软件。  相似文献   

正常椭球内部场的内蕴几何与密度分布     

黄金水 《武汉大学学报(信息科学版)》1997,(4)

将重力场内蕴几何结构的研究引入到正常椭球内部场的研究中，深入探讨了内蕴几何量及其与内部物理量之间的关系，并据此建立了弱平衡条件下的基本微分方程，进而给出确定椭球内部内蕴几何量与场源密度分布的方法。研究表明，平衡形状理论中的Ｗａｖｒｅ公式和Ｃｌａｉｒａｕｔ方程可由内蕴几何与内部物理量之间的关系导出，它们是在平衡假设下取椭球近似的结果。  相似文献   

氯对测定化合水的影响及其校正研究     

李继乐 《岩矿测试》1997,16(2):81-86

用差热和热（失）重法、ｐＨ值检验、离子色谱等分析方法考察和证实了Ｃｌ－对平菲尔特管重量法测定化合水（Ｈ２Ｏ＋）的干扰，研究其影响规律，提出用系数校正方法可获得Ｈ２Ｏ＋的准确结果。方法用于含氯深海沉积物和大洋多金属结核标准物质中Ｈ２Ｏ＋的定值分析，取得满意结果  相似文献   

多金属结核中二氧化锰的测定   总被引：1，自引：0，他引：1  

夏月莲  毛海燕 《岩矿测试》1997,16(3):177-179

用过量的含有Ｈ２ＳＯ４的（ＮＨ４）２Ｆｅ（ＳＯ４）２溶液分解多金属结核的同时，还原了试样中的ＭｎＯ２，然后以Ｋ２Ｃｒ２Ｏ７标准溶液滴定测定了多金属结核中的ＭｎＯ２。就样品分解过程中的加热温度和时间对测定结果的影响及标准溶液的标定等问题进行了讨论，经多次测定，方法重现性好。应用此方法为新研制的多金属结核标准物质提供了ＭｎＯ２的定值数据，其结果与初定值相符，无剔除值，精密度（ＲＳＤ，ｎ＝８）小于０６％。  相似文献   

参数椭球表面的重力   总被引：10，自引：0，他引：10       下载免费PDF全文

郝晓光 《地球科学》1997,22(2):223-226

推导了带密度参数的界面深度参数的旋转椭球表面重力的封闭公式，提出了“参数椭球”的概念。  相似文献   

深基础护坡桩的设计与施工中的几个问题     

曹新明 《地质与勘探》1997,33(3):56-60

着重介绍了间隔式钻孔灌注桩在挡土护坡技术中的应用方法，设计时的主要参考依据，计算土压力理论的应用原则以及施工中需注意的几个问题，为进行深基础挡土护坡的工程提供了部分参考依据。  相似文献   

O(T2)精度下椭球界面Dirichlet边值问题的积分解     

于锦海 《地球物理学报》2004,47(1)

研究了边界是参考椭球面的Laplace方程Dirichlet边值问题的求解，在O(ε4·T)精 度下给出了参考椭球界面上扰动重力位Dirichlet外问题的积分解式. 该结果理论上优于目 前常用的球近似下的积分解式，从而为研究物理大地测量中边值问题的求解提供了新的依据  相似文献   

Analysis of Sediments and Soils by X-Ray Fluorescence Spectrometry Using Matrix Corrections Based on Fundamental Parameters   总被引：2，自引：0，他引：2  

Jacinta Enzweiler  Maria Aparecida Vendemiatto 《Geostandards and Geoanalytical Research》2004,28(1):103-112

Wavelength dispersive X-ray fluorescence spectrometry (WD-XRF) is widely used for the analysis of soils and sediments using well characterised procedures. However, difficulties can occur with samples such as unknowns containing small amounts of ore materials and samples collected from contaminated sites where trace elemental concentrations can exceed the concentration range for routine analysis. We studied the performance of a commercially available method, based on fundamental parameters (FP) to correct matrix effects. The spectrometer was originally calibrated with elemental or simple compound calibrants. Samples were analysed as pressed powder pellets. Eighteen sediment and soil reference materials, three of them with certified values for some of their constituents, were used to evaluate accuracy, by comparing results with recommended values and their standard deviations (RV ± 2s) or certified values and their confidence intervals (CV ± Cl). When results fell systematically outside these intervals, calibrations were refined with geochemical reference materials. The best agreement of results with recommended and certified values was obtained when the contents of H₂O and C in each sample were included as matrix constituents during calculations. The detection limits of trace elements tended to be relatively high, because the measuring conditions employed were not maximised for sensitivity. The main advantage of the method tested was that it enabled the analysis of samples with high concentrations of trace elements and the determination of elements such as F, Bi, Sb and W, which are not commonly included in quantitative XRF analysis of geological samples.  相似文献   

A Reflection on Mg, Cd, Ca, Li and Si Isotopic Measurements and Related Reference Materials   总被引：6，自引：1，他引：6  

Jean Carignan  Damien Cardinal  Anton Eisenhauer  Albert Galy  Mark Rehkamper  Frank Wombacher  Nathalie Vigier 《Geostandards and Geoanalytical Research》2004,28(1):139-148

This contribution aims to report the reflections we had with the scientific community during two international workshops on reference materials for stable isotopes in Davos (2002) and Nice (2003). After evaluating the isotopic homogeneity of some existing reference materials, based on either certificates, literature data or specific inter-laboratory rounds, we confirm these as primary reference materials or propose new ones relative to which stable isotope compositions should be reported. We propose DSM-3 for Mg, NIST SRM 915a for Ca, L-SVEC for Li and NBS28 for Si. Cadmium does not yet have a well identified delta zero material, although three commercial mono-elemental Cd solutions have yielded the same isotopic composition relative to one another. In order to scale the linearity of any mass spectrometer, some secondary reference materials are also proposed: Cambridge-1 solution for Mg, the "Münster-Cd" and JEPPIM Cd solutions for Cd and the "Big Batch" silicate for Si. The team from Nancy propose to prepare a mixed spike solution for Li isotopes. Well-characterised natural samples such as ocean or continental waters, diatoms, sponges, rocks and minerals are needed to validate the entire analytical procedure, particularly to take into account the effect of sample mineralisation and of chemical manipulations for elemental separation prior to analysis.  相似文献   

Precise/ Small Sample Size Determinations of Lithium Isotopic Compositions of Geological Reference Materials and Modern Seawater by MC-ICP-MS   总被引：6，自引：1，他引：6  

Alistair B. Jeffcoate  Tim Elliott  Alex Thomas  Claudia Bouman 《Geostandards and Geoanalytical Research》2004,28(1):161-172

The Li isotope ratios of four international rock reference materials, USGS BHVO-2, GSJ JB-2, JG-2, JA-1 and modern seawater (Mediterranean, Pacific and North Atlantic) were determined using multi-collector inductively coupled plasma-mass spectrometry (MC-ICP-MS). These reference materials of natural samples were chosen to span a considerable range in Li isotope ratios and cover several different matrices in order to provide a useful benchmark for future studies. Our new analytical technique achieves significantly higher precision and reproducibility (< ± O.3%o 2s) than previous methods, with the additional advantage of requiring very low sample masses of ca . 2 ng of Li.  相似文献